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24/06/2005 - Controller General of Patents, Designs, and Trade Marks

24/06/2005 - Controller General of Patents, Designs, and Trade Marks

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(21) Application No. 332/DEL/1999 A (22) Date <strong>of</strong> filing <strong>of</strong> Application: 25/02/1999<br />

(54) Title <strong>of</strong> the invention: “A PROCESS FOR PREPARATION OF SINTERING ADDITIVES IN<br />

POWDER FORM USEFUL FOR SINTERING OF SILICON CARBIDE.”<br />

(51) International Classification 7 :<br />

C04B 35/583; C08K 3/34<br />

(30) Priority Data :<br />

(31) Document No.:NIL<br />

(32) Date : NIL<br />

(33) Name <strong>of</strong> convention country : NIL<br />

(66) Filed U/s 5(2) : NIL<br />

(61) Patent <strong>of</strong> addition to application No. :<br />

NA<br />

(62) Filed on : NA<br />

(63) Divisional to Application No. :NIL<br />

(64) Filed on : NA<br />

Total No <strong>of</strong> Pages: 15<br />

(71) Name <strong>of</strong> the applicant:<br />

COUNCIL OF SCIENTIFIC INDUSTRIAL &<br />

RESEARCH<br />

Address <strong>of</strong> the Applicant:<br />

Rafi Marg New Delhi–110001<br />

(72) Name <strong>of</strong> the Inventor:<br />

SANKAR GHATAK<br />

AMIYASANKAR SANYAL<br />

KAJAL KUMAR DHARGUPTA<br />

SANTANU MANDAL<br />

(57) Abstract:<br />

The invention relates to a process for preparation <strong>of</strong> sintering additives in powder form<br />

useful for sintering <strong>of</strong> silicon carbide. The process steps comprises; mixing aluminum oxide <strong>and</strong><br />

aluminum nitride in attritor mill using alumina balls in the molar proportion <strong>of</strong> 5 to 95, separating<br />

the milled powder from alumina balls by sieving through 100 mesh B. S., preparing a slurry by<br />

known methods using organic solvents as herein described, drying the said slurry to obtain a<br />

powder, firing the said powder containing aluminum oxide <strong>and</strong> aluminium nitride at a temperature<br />

in the range <strong>of</strong> 1750–1850 0 C under nitrogen atmosphere for a period in the range <strong>of</strong> 1–5 hours,<br />

grinding the product by known methods in presence <strong>of</strong> organic solvents as defined above, drying<br />

the said slurry to obtain sintering additives in powder form.<br />

18170

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