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OHM RemediationServices Corp. SAMPLING AND ANALYSIS PLANSamples will be logged in <strong>and</strong> screened upon arrival at the on-<strong>site</strong> laboratory. Manufacturer’sinstructions will be followed <strong>for</strong> each kit. Detection <strong>and</strong> quantitation limits, accuracy, <strong>and</strong>precision studies will also be per<strong>for</strong>med <strong>for</strong> each kit. Results will be recorded in the laboratorynotebook <strong>and</strong> submitted in the pilot study report Time required <strong>for</strong> testing will be carefullymonitored <strong>and</strong> recorded.Samples will be analyzed at an off-<strong>site</strong> laboratory <strong>for</strong> the parameters listed in Appendix A.Laboratory services will be procured on a competitive bid basis.Results from both on-<strong>site</strong> <strong>and</strong> off-<strong>site</strong> laboratories will be reviewed, summarized <strong>and</strong> evaluatedby the Regional Senior Project Chemist <strong>and</strong> Regional Chemical QA/QC Coordinator. Eachscreening method <strong>and</strong> kit will be evaluated based on criteria such as the correlation to st<strong>and</strong>ardmethod results, sensitivity, selectivity, possible matrix interferences, per<strong>for</strong>mance, time <strong>and</strong>cost. Recommendations will be made as to the use <strong>and</strong> validity of each screening technique.Results from the off-<strong>site</strong> laboratory will also be evaluated by the Regional Transportation <strong>and</strong>Disposal Coordinator <strong>for</strong> disposal options.3.1.1 Segregation of Excavated SoilsAs excavation is being per<strong>for</strong>med <strong>and</strong> each truck loaded with approximately 17 cubic yards of<strong>soil</strong>, a compo<strong>site</strong> sample consisting of 5 grabs will be collected. These 5 grab samples will becollected as the truck is being loaded, using a clean SS spoon. The grab samples will becollected in a clean SS bowl or bucket <strong>and</strong> homogenized. A compo<strong>site</strong> sample will beprepared <strong>and</strong> placed into the appropriate containers as listed in Appendix A, Table A-l.Sampling equipment will be thoroughly cleaned between samples using decontaminationprocedures described in section 3.5. Field <strong>sampling</strong> personnel will wear disposable glovesduring <strong>sampling</strong> <strong>and</strong> will change gloves between truckloads to minimize the potential <strong>for</strong>cross-contamination.The sample will be screened using a TPH immunoassay field-screening kit. If TPH is greaterthan 100 mg/lcg, the truckload of <strong>soil</strong> will be taken to a lined holding area designated as“contaminated”. If TPH is less than 100 m@kg, the truckload of <strong>soil</strong> will be taken to a linedholding area designated as “clean”.3.1.2 Characterization of the “Contaminated” Soil PilesOne compo<strong>site</strong> sample of all “contaminated ” <strong>soil</strong> piles will be collected <strong>and</strong> sent to the off-<strong>site</strong>laboratory <strong>for</strong> the analyses listed in Appendix A, Table A- 1. The compo<strong>site</strong> sample will beprepared by collecting 6 r<strong>and</strong>om grab samples from the surface, middle <strong>and</strong> center of all the<strong>soil</strong> piles using a clean SS spoon. The grabs are then collected into a clean SS bowl or bucketOHM Project 16487SAP Sampling <strong>and</strong> Analysis Ran May 1995In<strong>for</strong>mation herein is pmprietary <strong>and</strong> confidential <strong>and</strong> to be used or released to others only with explicit writtea permission of OHM RemcdLtionService4 Colp.3-2

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