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OHM RemediationServices Corp. SAMPLING AND ANALYSIS PLANThe final report is usually generated by use of computer. A back-up copy of the report ondiskette is filed along with the project file. The original report remains in the hard drive of thecomputer until such a time is required to download it on a diskette. This diskette is alsoarchived.All information under the corresponding project number is maintained in the archive system forfive years. All archives are accessed by the archives file master list which is maintained in aseparate location from the archives.OHM +jea 1+87.SAP Sampling and Aarlyb Plan %Y ,lqsS~&~orh~o$erem w proprietary and confidential and to be used or released to others only with explicit written permission of OHM Rancdmtmn5-6
6.0 DATA ASSESSMENT PROCEDURESReliability in analytical determination is maintained through strict adherence to quality controlprocedures. Procedures are designed to control both the accuracy and precision of analyticalresults. Depending on the level of certification of the data, a known method spike is routinelyanalyzed to ensure the accuracy of results. The procedure is to run the standard QA/QC andsample analysis with each lot of samples sent to the laboratory. If more than ten individualanalyses are made, additional standards will be analyzed at a rate of one standard per tenanalyses. Some procedures call for the use of either a surrogate spike or the standard additionof a known quantity of the analyte to a split of the sample being analyzed.Control charts will be prepared using an estimate of the spike recovery obtained from theliterature or determined by repeated analyses run in the laboratory. Each time the analyst runsa method spike, the results are entered on the control table. If a standard addition technique isused, a plot of instrument response versus added analyte concentration is made in order todetermine analyte concentration in the original sample. These are further explained in thelaboratory’s QAM.Replicate analyses will be performed on at least 10 percent of the samples processed by thelaboratory. A record of the precision of most analyses is kept by calculating and plotting theindustrial statistic I (which is equivalent to the coefficient of variation). Blanks are also runwith each batch of samples or individual sample analyzed regardless of the level of certificationof the data.The purpose of spikes, blanks, and replicates is to provide a sound scientific basis fi-om whichthe degree of certification of the resultant data can be objectively concluded. These are notmanagement decisions, but follow naturally from the results of the above QC procedures.6.1 AccuracyData accuracy is a reflection of the efficiency of the analytical procedure. It is determined byuse of spiked samples and standard reference materials or laboratory control samplesperformed at the rate of one set every 20 samples. A control chart is generated using historicallaboratory data where warning and control limits are established to assess data accuracy.The accuracy (check standards) samples will have concentration values of the mid-standard.During analysis, a minimum of 10 percent of samples must be accuracy samples. Theaccuracy samples must be staggered through the analysis, not placed one after another. After aminimum of seven accuracy samples are analyzed, the percent recovery is calculated for eachsample.OHM Project 16487SAp Sapling and Analysis plan May 1995Information herein is proprietary and confidential and to be used or released to othen only with explicit written pcmission of OHM Ram&&n&m&a Corp.6-1
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NOHM RemediationServices Corp.WORK
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1.0 INTRODUCTIONThis Work Plan (WP)
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2.0 SITE BACKGROUNDMCB Camp Lejeune
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..;/II'. 1i4\..\1 '*.XCAVATION \.AR
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A I B I CE I PI 0 I H I IPARK I NGA
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OHM RemediationServices Corp. WORK
Page 13 and 14: 5.0 SITE CONTROL PLANSOHM will impl
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Page 26 and 27: 7.0 SITE RESTORATION AND DEMOBILIZA
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Page 32 and 33: TABLE OF CONTENTS - CONTINUED6.0 DA
Page 34 and 35: 2.0 PROJECT MANAGEMENT2.1 Project B
Page 36 and 37: Program ManagerG. Krauter, P.E.Prog
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Page 48 and 49: A I 8 I P I 0 I EFI I 6 IH1 IPARKIN
Page 58 and 59: 4.0 DATA ACQUISITION4.1 Analytical
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Page 70 and 71: lWorking order of instruments and e
Page 72 and 73: 8.0 CORRECTIVE ACTIONCorrective act
Page 76 and 77: Table A-lSampling SummarySample Typ
Page 86 and 87: AppendixBSample LabelCustody SealCh
Page 88 and 89: 3 CHAIN-OF-CUSTODY RECORDOI IM Corp
Page 90 and 91: IA== B OHM Renmhtionavices Corp\&FC
Page 92 and 93: BOHM RemediationServices Corp.SITE-
Page 94 and 95: TABLE OF CONTENTS - CONTINUED6.0 DE
Page 96 and 97: This Health and Safety Plan (HASP)
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OHMRemediationconnection between th
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OHM RemediationServices Corp. HEALT
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OHMRemediationTask No. 4: SoilSampl
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OHM RemediatioaServices Corp. HEALT
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5.0 PROTECTIVE EQUIPMENTThis sectio
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6.0 DECONTAMINATION PROCEDURESThis
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. . . --..7.0 AIR MONITORINGAir mon
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OHMRemediationServices Corp. HEALTH
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ci@- OHM RemediationServices Corp.
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9.0 TRAINING REQUIREMENTSAs a prere
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HEALTH-AND-SAFETYPLAN CERTlFICATION
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APPENDIX B - OHM HAZARD COMMUNICATI
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8. Know what you are expected to do
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. Methods and observations that may
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msPhysical propertiesAcute/Chronic
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GPI Material Safety Data Sheets Col
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Material Safety Data Sheets Collect
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e5P (518)37%8854Genium Publishing C
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apSix.lion 1. Material Identificati
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Material Safety Data Sheets Collect
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Genium Publishing CorporationMateri
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.UrRPLS= ?UXiURE OF PARAFFIHTC, CTt
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APPxavg a5twfIc vAPUR'C!fE?!XCAL CA
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Fi reNF?A HAZARD RATING ’- Extten
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WITCO MATERIAL SAFETY .O A T A SHEE
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---------w.- -- ----F. FWSICAL DATA
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SECTION 5c- HEALTH HAZAROS4lllmsnol
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.--‘ AMALIE MULTI-PURPOSE LS GEAR
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We believe the statements, technica
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(Section III cmtinuei,)ffcsk=sint:
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i:.:::;:. ..-., \,’. .No. 68 Calc
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HATZ:P~A&,SXFETY DATA SHEET NC?. CO
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.w.N/AHAZAROOUS MIXTURES OF OTHER L
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.._ s1\1a.lZPage 4CHEMICAL FORMULA:
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. .SECTION 6. HEXLTH HAZARD. IfiFOR
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AJ 0. 14MSDS No. 324 Isopropyl Alco
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No. 14MSDS No. 324 Isopropyl Alcoho
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.;, -.-:-..: ..INo.44 Methane 8A9__
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. Materiaf Safety Data SheetFrom Gc
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:.I3 FlRsrBRANDSMaterial Safety Dat
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.nFIRSTBRANDSMaterial Safety Data S
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.. . DFIRSTBRANIlSMaterial Safety D
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Tdeshone:Infomation: (619) 275liu~C
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APPENDIXDHEALTH AND SAFETY FORMSAcc
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(Use Extra Pageif Needed).--%scribo
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*c= OH31 Remediation\m Services Cor
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IBAR MONTHLY INSbBCTIONCHECRLIBTBAR
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alme,-I sowica Corp.COMBUS’ITBLE
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DIRECT READING INSTUMENT LOGNAME:PR
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j% - -5 mi -omcorpo~Date:DAILY SA.F
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. ‘ISCUA MONIIILY INSFECA'ION CIi
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SITE SAFETY OFFICERDAILY REPORTDATE
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~.-’ - . .-Pm-.. -d-e..-L ArtEre
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HAZARD ANALYSISEM 38s i1 Ott 92nLll
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