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Preface - kmutt

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94<br />

application of these skills in their work. The<br />

learning structure of C-ChEPS exposes the<br />

learners every year to all the following 5<br />

components: project-based learning, background<br />

knowledge (Chemical Engineering), learning<br />

tools, mindfulness and learning support. Thus,<br />

the key performance indicators (KPI) for<br />

learners' development are: 1) Learning skill, 2)<br />

Chemical Engineering Knowledge, and 3)<br />

General Skill.<br />

Four classes (a total of 45 people) have<br />

graduated from the C-ChEPS program. The<br />

learning results have shown significant<br />

development in the learners' self-confidence at<br />

work, information seeking, communication, and<br />

presentation skills. Moreover, they can apply<br />

chemical knowledge to make reasonable<br />

decisions in problem solving.<br />

The company benefits from productivity<br />

improvement, energy and cost savings a total<br />

value of about 108 MBaht from a 4-year<br />

operation of C-ChEPS program.<br />

The effectiveness of C-ChEPS can be<br />

seen from an increase in the participating<br />

companies which now includes the following<br />

four: Thai Plastic and Chemical Public Co. Ltd.,<br />

Bangkok Synthetic Co. Ltd, The Aromatics<br />

(Thailand) Public Co. Ltd, and National Petrochemical<br />

Public Co. Ltd. as well as CCC.<br />

Clearly, these companies appreciate the<br />

development their employees get from the C-<br />

ChEPS program.<br />

The indirect result of the C-ChEPS<br />

program has led the KMUTT and the Petrochemical<br />

Industry into establishing a University<br />

of Learning and learning being applied in the<br />

workplace.<br />

IC-051 ADSORPTION OF METALLIC IONS<br />

FROM A METAL PLATING PROCESS ON<br />

ACTIVATED CARBON<br />

Suwassa Pongamphai, Supaporn Douglas,<br />

Wittaya Teppaitoon, Peter L. Douglas<br />

The 55 th Canadian Chemical Engineering<br />

Conference, October 16-19, 2005, Metro<br />

Toronto Convention Centre, Toronto, Ontario,<br />

Canada<br />

A shrinking core model was applied to<br />

metallic ion adsorption on compacted particles<br />

of coconut shell activated carbon. The model is<br />

based on the shrinking core formulation for<br />

catalytic reactions. The analysis of the external<br />

liquid film mass transfer and intraparticle<br />

KMUTT Annual Research Abstracts 2005<br />

diffusion on the adsorption kinetics with<br />

nonlinear adsorption and diffusion in a single<br />

particle is presented.<br />

The model was solved numerically and<br />

optimized using nonlinear parameter estimation<br />

to determine the film mass transfer coefficient<br />

and internal effective diffusivity. Using the<br />

estimated parameters, a parametric study was<br />

carried out to study the effects of initial mass<br />

and concentration of the adsorbate and adsorbate<br />

particle size on the system kinetics.<br />

The accuracy of the model will be<br />

demonstrated by comparison with experimental<br />

data on the adsorption of heavy metals from the<br />

effluent stream from a metal plating process.<br />

IC-052 EXTRACTION OF NIMBIN FROM<br />

NEEM SEEDS USING SUPERCRITICAL<br />

CARBON DIOXIDE WITH MODIFIER<br />

Pathumthip Tonthubthimthong,<br />

Supaporn Douglas, Suwassa Pongamphai,<br />

Peter L. Douglas<br />

The 55 th Canadian Chemical Engineering<br />

Conference, October 16-19, 2005, Metro<br />

Toronto Convention Centre, Toronto, Ontario,<br />

Canada<br />

The objective of this research was to<br />

study the extraction of nimbin from neem seeds<br />

(Azadirachta indica var siamensis valeton) using<br />

supercritical carbon dioxide and modifier. Our<br />

previous work, which focused on the extraction<br />

of nimbin from neem seeds using pure<br />

supercritical carbon dioxide, indicated that the<br />

optimum extraction pressure was about 20 MPa.<br />

In this paper, the effect of extraction<br />

pressure, temperature, and the type of modifier<br />

on extraction yield were studied using the Latin<br />

Square technique to plan the experiments.<br />

Extraction pressures were 10, 15, 20, 25 MPa;<br />

extraction temperatures were 30, 35, 40, 45 °C<br />

and methanol, ethanol, ethyl acetate and<br />

dichloromethane modifiers were investigated.<br />

The nimbin extraction experiments were<br />

performed using 2 g of neem seed kernels with<br />

an average size of 850 nm and 10% modifier for<br />

an extraction time of 1 hour.<br />

The results indicated that the extraction<br />

yield depends significantly on the extraction<br />

modifier. The maximum extraction yield was<br />

0.099 mg/g neem seeds kernel, (fractional yield<br />

of 97.17 %), obtained at P = 25 MPa, T = 45°C<br />

using methanol. The maximum extraction yield<br />

using methanol and a soxhlet was 0.1004 mg/g<br />

International Conference

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