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Preface - kmutt

Preface - kmutt

KMUTT Annual Research

KMUTT Annual Research Abstracts 2005 respectively. Deionized water at 100 o C could elute gold adsorbed onto WSFW to 71%. The effect of the increasing temperature of water, 30, 60, and 100 o C, implied that the adsorption mechanism was mainly physical adsorption. The negative values of enthalpy change (∆H) and free energy change (∆G) indicated an exothermic and spontaneous process, respectively. The positive values of entropy change (∆S) indicated increasing disorder of the system. The advantages of wood shaving fly ash are the purification of gold and the easier recycling of gold from the gold-adsorbed adsorbent. IJ-106 ADSORPTION MECHANISM OF SYNTHETIC REACTIVE DYE WASTEWATER BY CHITOSAN Niramol Sakkayawong, Paitip Thiravetyan, Woranan Nakbanpote Journal of Colloid and Interface Science, Vol. 286, No. 1, 2005, pp. 36-42 Chitosan was able to remove the color from synthetic reactive dye wastewater (SRDW) under acidic and caustic conditions. The effect of the initial pH on SRDW indicated that electrostatic interaction occurred between the effective functional groups (amino groups) and the dye under acidic conditions. Moreover, SRDW adsorption under caustic conditions was also affected by the covalent bonding of dye and hydroxyl groups of chitosan. In addition, elution tests confirmed that chemical adsorption occurred under acidic conditions, while both physical and chemical adsorption appeared under caustic conditions. The spectra of attenuated total reflectance Fourier transform infrared spectrometry confirmed the functional groups of chitosan that affected the SRDW adsorption. However, the maximum adsorption capacities of chitosan increased when the temperature increased. The maximum adsorption capacity of chitosan obtained from the Langmuir model was 68, 110, and 156 mg g −1 under a system pH of 11.0 at 20, 40, and 60 o C, respectively. The negative values of enthalpy change (∆H), free energy change (∆G), and entropy change (∆S) indicated an exothermic, spontaneous process and decreasing disorder of the system, respectively. Therefore, the mechanism of SRDW adsorption by chitosan was probably by chemical adsorption for a wide range of pH's and at high temperatures. 39 IJ-107 VOLTAMMETRIC DETECTION OF ORGANOHALIDES BY REDOX CATALYSIS: IMPROVED SENSITIVITY BY IMMOBILISATION WITHIN A CUBIC PHASE LIQUID CRYSTAL Wisitsree Wiyaratn, Mithran Somasundrum, Werasak Surareungchai Analyst, Vol. 130, No. 5, 2005, pp. 626-631 Two combined strategies are reported for improving the sensitivity of organohalide detection by redox catalysis. These are, improvement of the second order rate constant (k) for catalytic reduction of the organohalide, and improvement of the rate of substrate diffusion. Values of k are calculated for both alkyl and aryl halides, from slow scan rate cyclic voltammograms in homogeneous solution. It is shown that a Zn(II) porphyrin exhibits higher catalytic rates than the previously used Co(II) porphyrin or Co(I) salen. Amperometric and rotating disk electrode studies of electropolymerised films of the Zn(II) porphyrin, reveal that at optimum thickness, mediator–substrate reaction and substrate diffusion are the rate limiting steps. Hence, immobilisation of the Zn(II) porphyrin within the more open structure of a cubic phase liquid crystal produces an increase in sensitivity of approx. 10 times, and lowers the limit of detection by one order of magnitude. The optimised sensor responds linearly to seven organohalides in the range 0.1 µM to 1.0 µM with a sensitivity of 6.95 A M –1 cm –2 . Chronoamperometric experiments with a microdisk electrode show that the rate of charge transport in the cubic phase films (apparent diffusion coefficient, D E = 5.65 x 10 –10 ± 0.11 x 10 –10 cm 2 s –1 ) is faster than in the electropolymerised films (D E = 3.64 x 10 –11 ± 0.02 × 10 –11 cm 2 s –1 ). The variation of D E with the concentration of Zn(II) in the cubic phase suggests that diffusion of charge is predominantly by electron self-exchange, rather than by physical movement. IJ-108 LIGHT-ASSISTED SYNTHESIS OF PT- ZN PORPHYRIN NANOCOMPOSITES AND THEIR USE FOR ELECTROCHEMICAL DETECTION OF ORGANOHALIDES Wisitsree Wiyaratn, Sabahudin Hrapovic, Yali Liu, Werasak Surareungchai, John H.T. Luong International Journal

40 Analytical Chemistry, Vol. 77, No. 17, 2005, September, pp. 5742-5749 Pt-Zn porphyrin nanocomposites have been synthesized using zinc porphyrin and dihydrogen hexachloroplatinate in the presence of light and ascorbic acid. TEM and AFM imaging revealed that Pt nanoparticles with an average diameter of ~3.5 nm were embedded within the Zn porphyrin matrix. The glassy carbon electrode was modified with Nafionstabilized Pt-Zn porphyrin nanocomposites and used for dehalogenation of carbon tetrachloride, chloroform, pentachlorophenol, chlorobenzene, and hexachlorobenzene as five test models. The Pt-Zn porphyrin nanocomposite-modified electrode exhibited catalytic activity for the reduction of organohalides at -1.0 V versus Ag/AgCl. Raman signatures confirmed the dehalogenation of chlorobenzene by the nanocomposite-modified electrode. The above two aliphatic and three aromatic organohalides had detection limits of 0.5 µM with linearity up to 8 µM. The modified electrode was good for at least 80 repeated measurements of 4 µM chlorobenzene with a storage stability of 1 month at room temperature. The deactivation of the electrode activity was associated with the loss of platinum nanoparticles from the nanocomposite structure. IJ-109 TAURA SYNDROME VIRUS (TSV) IN THAILAND AND ITS RELATIONSHIP TO TSV IN CHINA AND THE AMERICAS Linda Nielsen, Wiwat Sang-oum, Supapon Cheevadhanarak, Timothy W. Flegel Diseases of Aquatic Organisms, Vol. 63, No. 2- 3, 2005, pp. 101-106 The cultivation of exotic Penaeus vannamei in Thailand began on a very limited scale in the late 1990s, but a Thai government ban on the cultivation of P. monodon in freshwater areas in 2000 led many Thai shrimp farmers to shift to cultivation of P. vannamei. Alarmed by the possibility of Taura syndrome virus (TSV) introduction, the Thai Department of Fisheries required that imported stocks of P. vannamei be certified free of TSV by RT-PCR (Reverse Trasciption Polymerase Chain Reaction) testing. During the interval of allowed importation, over 150000 broodstock shrimp were imported, 67% of these from China and Taiwan. Despite the safeguards, TSV outbreaks KMUTT Annual Research Abstracts 2005 occurred and we confirmed the first outbreak by RT-PCR in early 2003. This resulted in a governmental ban on all shrimp broodstock imports from February 2003, but TSV outbreaks have continued, possibly due to original introductions or to the continued illegal importation of stocks. To determine the origin of the TSV in Thailand, the viral coat protein gene VP1 was amplified by RT-PCR from several shrimp specimens found positive for TSV by RT-PCR from January to November 2003. These included 7 samples from P. vannamei disease outbreaks in Thailand, 3 other nondiseased shrimp samples from Thailand and Burma and 6 samples including P. vannamei and P. japonicus from China. Comparison revealed that the Thai, Burmese and Chinese TSV types formed a clade distinct from a clade of TSV types from the Americas. IJ-110 USE OF AN ALTERNATIVE ARCHAEA- SPECIFIC PROBE FOR METHANOGEN DETECTION Wiwat Jupraputtasri, Nimaradee Boonapatcharoen, Supapon Cheevadhanarak, Pawinee Chaiprasert, Morakot Tanticharoen, Somkiet Techkarnjanaruk Journal of Microbiological Methods, Vol. 61, No. 1, April 2005, pp. 95-104 An alternative 16S rRNA-targeted oligonucleotide probe specific for Archaea was developed and used for detection of methanogens in anaerobic reactors. The designed probe was checked for its specificity by computer-aided comparative sequence analysis. For in situ application, optimal stringency conditions were adjusted by performing whole cell hybridization using target and nontarget organisms. Anaerobic sludge samples were examined by in situ hybridization for methanogenic populations. The relative abundance of methanogens was monitored with epifluorescence microscopy. Individual cells could be visualized with strong fluorescence signals after hybridization with the newly developed probe. IJ-111 HIGHER PLANT-LIKE FLUORESCENCE INDUCTION AND THERMOLUMINESCENCE CHARACTERISTICS IN CYANOBACTERIUM, Spirulina MUTANT DEFECTIVE IN PQH 2 OXIDATION BY CYTB 6 /F COMPLEX Marasri Ruengjitchatchawalya, László Kovács, International Journal

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    National Conferences

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    210 จอมเทียนปา

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    212 การสกัดสาร

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    214 ไดแก อุณหภู

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    216 โดยกลไกของ

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    218 เคลือบเมื่

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    220 สําเริง จัก

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    222 ลดเวลาตลอด

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    224 อุณหภูมิสู

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    226 NC-043 การวิเคร

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    228 เกิดพฤติกร

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    230 เดียว เพื่อ

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    232 มากนอยเพีย

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    234 หลักที่พบใ

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    236 NC-073 การออกแบ

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    238 บทความนี้น

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    240 นําเอาเวคเ

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    242 งานวิจัยนี

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    244 การอบแหงลด

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    246 แยกเฟสต่ํา

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    248 กลบ โดยเปรี

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    250 นํามาใช คือ

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    252 วิเคราะหหา

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    254 NC-123 การวิเคร

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    256 NC-129 เครื่องผ

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    258 สามารถขยาย

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    260 ครั้งที่ 43, 1-

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    262 calculated with the use of the

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    264 Version 1.3.1 และ Softwar

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    266 ขนไกได จากก

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    268 โครงสรางขอ

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    270 การปลูกพืช

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    272 ระดับพึงพอ

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    274 ของแกสโซฮอ

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    276 1) สภาพทั่วไ

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    278 อนุปริญญา แ

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    280 อาชีวศึกษา

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    282 กระทบตอคุณ

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    284 ตั้งกลไกแข

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    286 นุชจรินทร เ

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    288 โดยรวมผูบร

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    290 แนนกระแสไฟ

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    292 NC-222 ผลงานตีพ

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    294 NC-227 เตาเผาไห

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    296 จําเพาะรวม

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    298 NC-238 จลนพลศาส

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    300 ทนงเกียรติ

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    302 ดีเซลนั้นม

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    304 NC-254 การใชเทค

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    306 อาคารศูนยก

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    308 กระบวนการร

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    310 บรรยากาศขอ

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    312 metal ions on 2-AP biosyntheis

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    314 total clones while the ethanol

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    316 การประชุมท

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    318 BioThailand (The 16 th Annual M

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    320 สูงที่สุดพ

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    322 นัยสําคัญท

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    324 ความเขมขนร

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    326 ปลูกแบบพรา

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    328 นี้ทําใหทร

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    330 ดุลชาติ มาน

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    332 ไมโครเมตร ส

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    334 In this study, we collected seq

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    336 กนกรัตน นาค

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    338 การพัฒนาสื

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    340 one of the causes of difficulty

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    342 ทวีรัตน วิจ

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    344 program, Cytoscape. This model

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    346 production demand. Nevertheless

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    348 อุลตราไวโอ

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    350 นี้อยูในชว

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    352 เพื่อนําสว

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    354 trichloroacetic acid (TCA) ม

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    356 ทรัพยากรที

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    358 ในประเทศสห

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    360 8-9 ธันวาคม 2548,

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    362 ซึ่งเกิดขอ

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    364 NC-391 การวิเคร

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    366 การประชุมว

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    368 2547) พบวามหาว

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    370 กนกพร ลีลาเ

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    Authors Index

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    376 จงจิตร หิรั

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    378 ธ ธนธร ทองส

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    380 พยุงศักดิ์

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    382 วรรณพ วิเศษ

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    384 สุดารัตน จิ

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    386 อุลาวัณย กุ

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    388 138, 141, 142 Jarunya Narangaja

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    390 Panida Kongsawadworakul 191 Pan

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    392 Sorakrich Maneewan 124, 136 Sor

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    394 KMUTT Annual Research Abstracts

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