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Chapter – 4 Studies on different types of reactions….. STEP – 2 Reagents / Reaction Condition (d): POCl3, Glacial acetic acid / Reflux, 30 min. 4.7.3 PREPARATION OF 1-(2, 6-DICHLOROPHENYL)-2-INDOLINONE STEP – 1 Reagents / Reaction Condition (e): ClCH2COCl / Reflux, 5 hours. STEP – 2 O O OH NH Cl Cl N Cl O Cl Cl O O Reagents / Reaction Condition (f): Anhydrous AlCl3 / 160°C, 2 hours. d e f Department of Chemistry, Saurashtra University, Rajkot – 360 005 219 N OH Cl O Cl Cl N O Cl Cl O CH 3
Chapter – 4 Studies on different types of reactions….. 4.7.4 SCHEME - 1 Reagents / Reaction Condition (g): 1-(2, 6-dichloro phenyl)-indolinone, Piperidine, Ethanol / Reflux, 5-7 hours. OR MW method: 1-(2, 6-dichloro phenyl)-indolinone, Piperidine, DMF / MW, 400 Watt. 4.7.5 SCHEME - 2 N N N N O R O R Reagents / Reaction Condition (h): 3-acetyl-4-hydroxycoumarin, Piperidine, Chloroform / Reflux, 4 hours. Where, R = 4-H, 4-Cl, 4-F, 4-NO2, 3-NO2 h g Department of Chemistry, Saurashtra University, Rajkot – 360 005 220 Cl R R N O O OH O O Cl N N N N
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Saurashtra University Re - Accredit
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Statement under O. Ph. D. 7 of Saur
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ACKNOWLEDGEMENT It is a moment of g
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Jignesh Lunagariya, Hitesh Sarvaiya
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CONTENT Content General Remarks 6 A
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Content 3.2 Reaction scheme 149 3.3
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5.14 Conclusion 313 5.15 Spectral r
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MF Molecular Formula MW Molecular W
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GABA Gamma Amino Butyric Acid MES M
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PART - A STUDIES ON 2-METHYL INDOLI
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Part-A Studies on 2-methyl indoline
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CHAPTER - 1 PREPARATION AND YIELD O
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Chapter - 1 Preparation and Yield o
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Chapter - 2 Microwave assisted simp
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Part - B Studies on isatin derivati
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CHAPTER - 3 PREPARATION OF SMALL LI
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Chapter - 3 Preparation of small li
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Chapter - 4 Studies on different ty
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Chapter - 5 Synthesis and Character
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Chapter - 6 Biological evaluation o
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Summary Synthesis and biological pr
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Summary Synthesis and biological pr
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Conferences / Seminar / Workshop At
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