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Chapter – 1 Preparation and Yield optimization.....
N-[(2-METHYL-2, 3-DIHYDRO-1H-INDOL-1-YL) METHYL] PYRIDIN-3-
AMINE (DNJ-208): IR (KBr, cm -1 ): 3341 (-NH), 3077 (Ar-H), 2945 (–CH3),
2862 (–CH2), 1560, 1500, 1470, 1462 (Ar-H), 1363 (C-N, Ar, 3°), 1325 (C-N,
Ar, 2°); MS m/z = 239 (M + ); Anal. Calcd. for C15H17N3: C, 75.28; H, 7.16; N,
17.56. Found: C, 75.32; H, 7.13; N, 17.55.
N-[(2-METHYL-2, 3-DIHYDRO-1H-INDOL-1-YL) METHYL] PYRIDIN-4-
AMINE (DNJ-209): 3292 (-NH), 3026 (Ar-H), 2941 (–CH3), 2866 (–CH2),
1558, 1496, 1470, 1460 (Ar-H), 1382 (C-N, Ar, 3°), 1323 (C-N, Ar, 2°); MS
m/z = 239 (M + ); Anal. Calcd. for C15H17N3: C, 75.28; H, 7.16; N, 17.56. Found:
C, 75.31; H, 7.16; N, 17.53.
(2-FURYL METHYL)[(2-METHYL-2, 3-DIHYDRO-1H-INDOL-1-YL) METHYL]
AMINE (DNJ-210): IR (KBr, cm -1 ): 3275 (-NH), 3020 (Ar-H), 2965 (–CH3),
2862 (–CH2), 1560, 1500, 1473, 1460 (Ar-H), 1371 (C-N, Ar, 3°), 1335 (C-N,
Ar, 2°), 1071 (C-O-C ); MS m/z = 242 (M + ); Anal. Calcd. for C15H18N2O: C,
74.35; H, 7.49; N, 11.56. Found: C, 74.31; H, 7.51; N, 11.59.
Department of Chemistry, Saurashtra University, Rajkot-360 005 57