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Chapter – 1 Preparation and Yield optimization..... acquire Mannich bases having desired scaffolds. These interesting Mannich bases derived from 2-methyl indoline are not only structurally novel but the biological evaluation is reported here for the first time. Biological importance of such an important scaffold is the rational behind the current work done in this chapter. Department of Chemistry, Saurashtra University, Rajkot-360 005 35
Chapter – 1 Preparation and Yield optimization..... 1.2 REACTION SCHEMES 1.2.1 PREPARATION OF 2 – METHYL INDOLINE STEP – 1 Reagents / Reaction Condition (a): Phenyl hydrazine, Acetone / Addition at RT. STEP – 2 Reagents / Reaction Condition (b): Polyphosphoric acid / 120°C. STEP – 3 NH NH N H NH 2 + CH 3 C H 3 N CH 3 CH 3 O NH a N CH3 CH 3 c Reagents / Reaction Condition (c): TFA, 1 M BH3.THF / 0-5°C. (Method – A) Zinc dust, 85% phosphoric acid. (Method – B) Department of Chemistry, Saurashtra University, Rajkot-360 005 36 b N H N H CH 3 CH 3 CH 3
Page 1 and 2: Saurashtra University Re - Accredit
Page 3 and 4: Statement under O. Ph. D. 7 of Saur
Page 6 and 7: ACKNOWLEDGEMENT It is a moment of g
Page 8 and 9: Jignesh Lunagariya, Hitesh Sarvaiya
Page 10 and 11: CONTENT Content General Remarks 6 A
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Page 14 and 15: 5.14 Conclusion 313 5.15 Spectral r
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Page 22 and 23: Part-A Studies on 2-methyl indoline
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Chapter - 2 Microwave assisted simp
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Part - B Studies on isatin derivati
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CHAPTER - 3 PREPARATION OF SMALL LI
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Chapter - 3 Preparation of small li
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CHAPTER - 4 STUDIES ON DIFFERENT TY
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Chapter - 4 Studies on different ty
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Chapter - 5 Synthesis and Character
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Chapter - 6 Biological evaluation o
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Summary Synthesis and biological pr
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Summary Synthesis and biological pr
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Conferences / Seminar / Workshop At
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