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Chapter – 5 Synthesis and Characterization….. 14. After C4-N19 bond cleavage, cleavage of the bonds C17-C18, C15-N16 gave characteristic peak at 217 m/e. [13] 15. C14-C15 bond cleavage gave characteristic peak at 204 m/e. [14] Department of Chemistry, <strong>Saurashtra</strong> <strong>University</strong>, Rajkot – 360 005 299
5.10.1.1 FRAGMENTATION PATTERN FOR DNJ-1013 8 7 6 O 1 2 O 11 9 5 3 10 4 12 22 23 F 29 8 9 22 23 F 29 21 24 28 F 30 7 10 21 24 28 F 30 20 25 F 31 6 5 20 25 NH 19 F 31 316 m/e 8 9 22 23 18 17 H3C 27 431 m/e 7 10 21 24 [8] 6 5 O 1 4 NH 19 [9] 20 25 248 m/e O 1 4 2 3 NH 19 N 13 N 16 26 O 11 14 15 CH 3 12 18 17 + . H3C 27 113 m/e 2 3 H N 13 N 16 26 O 11 8 7 6 O 1 2 + . O 11 8 7 6 O 1 2 O 11 + . 8 7 6 O 1 2 + . O 11 [1] 9 10 5 4 3 12 [2] 9 10 5 4 3 12 [3] 9 10 5 4 3 12 [4] + . + . CH 3 12 14 15 [11] [10] 22 23 F 29 21 24 28 F 30 20 25 F 31 NH 19 18 17 N 13 14 N 16 CH 3 26 15 22 23 F 29 21 24 28 F 30 20 25 F 31 NH 19 416 m/e 403 m/e 389 m/e 8 9 22 23 + . 8 7 6 O 1 2 O 11 9 5 3 10 4 12 22 23 F 29 7 10 21 24 21 24 28 F 30 6 5 20 25 20 235 m/e NH 2 19 O 1 4 + . NH 19 18 17 25 H3C 27 F 31 145 m/e 2 3 8 9 N 13 N 16 26 O 11 14 15 288 m/e 7 10 + . 6 5 204 m/e O 1 4 [12] 2 3 H3C 18 O 11 12 18 17 N 13 N H 16 14 15 8 7 6 O 1 2 O 11 9 5 3 10 4 12 8 9 220 m/e + . N 13 CH3 14 18 17 H3C 27 272 m/e 7 10 [14] 6 5 O 1 4 N 13 N 16 26 + . [13] 2 3 H3C 18 14 15 O 11 12 N 13 22 23 F 29 + . 14 21 24 28 F 30 CH 3 15 20 25 F 31 NH 19 8 9 22 23 F 29 18 CH 3 17 7 10 21 24 28 F 30 N 13 6 5 20 25 F 31 331 m/e 14 CH 3 15 O 1 4 NH 19 2 3 O 11 12 NH 2 13 + . + . 8 7 6 O 1 2 O 11 9 5 3 10 4 12 21 22 20 23 25 24 F 29 8 9 28 F 30 7 10 24 6 5 F 31 25 NH 19 O 1 4 18 CH 3 17 2 3 N 13 CH3 14 O 11 12 21 NH N 22 20 19 13 H3C CH3 18 14 23 F 29 8 9 22 23 F 29 28 F 30 7 10 21 24 28 F 30 [5] 6 5 20 25 F 31 [6] F 31 [7] 374 m/e O 1 4 359 m/e NH 19 2 3 O 11 12 + . + . HN 13 CH3 14 346 m/e
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Saurashtra University Re - Accredit
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Statement under O. Ph. D. 7 of Saur
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ACKNOWLEDGEMENT It is a moment of g
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Jignesh Lunagariya, Hitesh Sarvaiya
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CONTENT Content General Remarks 6 A
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Content 3.2 Reaction scheme 149 3.3
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5.14 Conclusion 313 5.15 Spectral r
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MF Molecular Formula MW Molecular W
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GABA Gamma Amino Butyric Acid MES M
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PART - A STUDIES ON 2-METHYL INDOLI
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Part-A Studies on 2-methyl indoline
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CHAPTER - 1 PREPARATION AND YIELD O
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Chapter - 1 Preparation and Yield o
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Chapter - 2 Microwave assisted simp
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Part - B Studies on isatin derivati
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CHAPTER - 3 PREPARATION OF SMALL LI
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Chapter - 3 Preparation of small li
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CHAPTER - 4 STUDIES ON DIFFERENT TY
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Chapter - 4 Studies on different ty
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Summary Synthesis and biological pr
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Conferences / Seminar / Workshop At
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