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1997 Swinburne Higher Education Handbook

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SCE502 Reactor Design<br />

10 credit points 4 hours per week Hawthorn<br />

Instruction: lectures, tutorials Assessment: examination<br />

70%, assignments 30% Prerequisites: SCE206 Fluid<br />

Mechanics, SCE302 Chemical Engineering ~modynamics,<br />

SCE402 Fluid Particle Systems and Advanced Fluid Mechanics<br />

- or demonstrated equivalent knowledge.<br />

A fifth year subject in the Bachelor of Chemical Engineering<br />

Ob jedives<br />

To provide students with the skills necessary to understand<br />

the complexities of industrial chemical reactors and the<br />

reactions carried out in them. The analysis and design of<br />

reactors will also be studied, as well as the fundamentals of<br />

reacting systems.<br />

Content<br />

Review of basic chemistry necessary to study reactors<br />

Stoichiometry, order of reaction, thermodynamic<br />

considerations, especially effect of temperature on heats<br />

of reaction and heat capacity data, van't Hoff equation,<br />

Chemical Kinetics and the effect of temperature on rate<br />

of reaction, Definition of reaction rate, other variables<br />

affecting reaction rate, kinetics of homogeneous<br />

reactions.<br />

Interpretation of batch reactor design<br />

Constant volume batch reactor and analysis of data,<br />

Variable volume batch reactor and analysis of data.<br />

Types of ideal reactors<br />

Definition of ideal reactors, continuous stirred tank<br />

reactors, plug flow reactors, mixed flow reactors,<br />

reactors in series and parallel<br />

Design for single reactions<br />

Size comparisons of single reactors, CSTR versus PFR<br />

for first and second order reactions.<br />

Tem~erature and Pressure effects<br />

Heats of reactions and equilibrium constants - the effect<br />

of temperature and pressure, general design procedure,<br />

optimum temperature progression, heat effects, adiabatic<br />

operation, non adiabatic operation.<br />

Non ideal flow in reactors<br />

residence time distribution in reactors, age distribution<br />

curves, use of tracer information, diagnostics for poorly<br />

rn<br />

performing equipment,<br />

-.<br />

Heterogeneous reaction systems.<br />

0 Fluid/particle reactions, shrinking core model for<br />

3<br />

particles of unchanging size and associated controlling<br />

8.<br />

mechanisms, reaction rates for shrinking particles and<br />

associated control mechanisms, non spherical particles,<br />

fluidised bed reactors<br />

Application of the above concepts to the solution of<br />

problems.<br />

Recommended reading<br />

Levenspiel, O., Chemical Reaction Engineering 2nd ed., John<br />

Wiley and Sons 1972<br />

Coulson, J.M., and Richardson, J.F., Chemical Engineering<br />

Volume 3,2nd edition, Pergamon Press 1990<br />

Denbigh, K.G., and Turner, J.C.R., Chemical Reactor Theory -An<br />

Introduction 3rd ed., Cambridge University Press 1984<br />

SCE503 Process Control<br />

10 credit points 3 hours per week Hawthorn<br />

Instruction: lectures, tutorials Assessment: examination<br />

70%, assignments 35%<br />

A fifth year subject in the Bachelor of Chemical Engineering<br />

0 bjedives<br />

To develop skills in control design and implementation of<br />

systems for chemical (including biochemical and food)<br />

plants. Provide the mathematical tools to analyse process<br />

dynamics, investigate system stability and understand the<br />

implications of these for chemical plant design.<br />

Content<br />

Introduction to process control<br />

Steady state, process dynamics, process modelling,<br />

closed-loop, process stability<br />

Chemical process Models<br />

continuity equations, energy equations, transport<br />

equations, equations of state, chemical kinetics<br />

Chemical Process Models<br />

CSTR (series, isothermal, variable hold up), batch<br />

reactor, distillation<br />

Process Dynamics<br />

Time-domain, laplace domain, frequency domain,<br />

Nyquist, Bode, Nichols plots<br />

Feed Back Control<br />

Proportional, integral, derivative, tuning, stability,<br />

Routh stability, criterion, Nyquist stability criterion<br />

Feed Forward Control<br />

Principle of invariance, linear/non-linear systems,<br />

dynamic compensatory tuning.<br />

Fuzzy Logic Control Principles<br />

Recommended reading<br />

Process Modelling, Simulation and Control for Chemical Engineers.<br />

Luyben McGraw Hill 1973.<br />

Shinskey, F.G., Process Control Systems, Application, Design and<br />

Tuning 3rd Ed. McGraw Hi11,1988<br />

Palm, W.J., Control Systems Engineering, W.J. Wiley N.Y. 1986<br />

Ogata, K., Modern Control Engineering 2nd Ed. Prentice Hall<br />

1990.<br />

SCE504 Process Equipment Design<br />

10 credit points fi hours per week Hawthorn<br />

Instruction: lectures, tutorials Assessment: examination<br />

70%, tests 15%, assignments 15% Prerequisites: CE102<br />

Enginewing Design, SCE201 Basic Process Cakculations,<br />

SCE40fi Fluid Particle Systems and Advanced Fluid<br />

Mechanics, SCE400 Heat transfw, SCE401 Mass Transfer,<br />

SCE305 Separation Processes, MM235 Enginewing Materials<br />

A fifth year subject in the Bachelor of Chemical Engineering<br />

0 bjedives<br />

To apply scientific and economic principles in selecting and<br />

specifying major equipment required to carry out particular<br />

processes: heat and mass transfer equipment, equipment for<br />

storage and transport of fluids. Apart from the physical and<br />

chemical principles of the processes, other factors are also

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