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Online proceedings - EDA Publishing Association

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Sub-micronic features with a final dimension of 400 nm<br />

wide, 570 nm height and 50 µm long were produced in SU-<br />

8 on silicon after exposure, development, PEB and hard<br />

bake as shown in Fig.5. For the 400 nm feature array,<br />

exposure dose of 4 µC/cm² was selected. However, with<br />

larger feature size less exposure dose is required.<br />

11-13 <br />

May 2011, Aix-en-Provence, France<br />

<br />

m/min as shown in Fig.7. Reduction of feed rate in PMMA<br />

case shows difference as it is inversely proportional to<br />

holding time of applied pressure and allows polymer filling.<br />

Also, its value directly affects the production rate. Good<br />

pattern transfer is obtained by changing only the number of<br />

passes compared with the micronic features replication.<br />

Fig.5 SU-8/Si mould with submicronic features of 400 nm wide and 570<br />

nm height. Inset: Magnification view of SU-8 feature cross-section 40KX<br />

First set of trials for roll embossing with 400 nm wide<br />

features was conducted in Topas 8007 COC. Embossed fine<br />

features of 400 nm width and 570 nm depth were produced<br />

in three passes at a temperature of 133–137 °C for upper<br />

and lower rolls, using a pressure of 4 bars and a feed rate of<br />

0.4 m/min as shown in Fig.6. However, an incomplete<br />

filling problem at sharp edges appears (see inset of Fig.6).<br />

Fig.7. PMMA replica embossed from SU-8/Si mould with submicronic<br />

features of 400 nm wide and 570 nm deep. Inset: Magnification view of the<br />

channel section Mag. 40KX<br />

C. Mould defects after replication<br />

The SU-8/Si mould has been used for roll embossing in<br />

COC foils without facing any problem. However, after<br />

using the SU-8/Si mould to emboss in PMMA, a complete<br />

de-lamination at the 300 nm features and partial delamination<br />

at the 400 nm features were observed on the<br />

stamp as shown in Fig.8 and its inset.<br />

Fig.6. Topas COC 8007 replica embossed from SU-8/Si mould with<br />

submicronic-features of 400 nm wide and 570 nm deep. Inset:<br />

Magnification view of the channel section Mag. 40KX<br />

It was expected that by increasing the embossing<br />

temperature and pressure, as well as decreasing feed rate,<br />

this problem could be resolved. But comparing these results<br />

with another COC embossed replica produced in three<br />

passes at the higher temperature of 166 °C for both rollers<br />

and a higher pressure of 6 bars and a feed rate of 0.3 m/min,<br />

shows no big difference at the sharp edges.<br />

Submicronic features replicated in PMMA in four passes<br />

at a temperature of 166 °C for both upper and lower rollers<br />

while applying a pressure of 6 bars and a feed rate of 0.1<br />

Fig.8. SU-8/Si mould with submicron features of 400 nm wide and 570 nm<br />

height after embossing. Inset: Magnification view of feature cross-section<br />

Mag. 40KX<br />

This de-lamination could be explained by the relatively<br />

high adhesive forces between the master patterns in SU-8<br />

and the PMMA foil to be embossed. These adhesive forces<br />

could be reduced if an anti-sticking layer is deposited before<br />

starting the embossing process. This anti-sticking layer<br />

could be a deposited layer of Teflon-like octo-fluoro-butane<br />

(C 4 F 8 ) gas.<br />

Also, the adherence between patterned SU-8 resist and<br />

the silicon wafer could be increased by optimizing the<br />

282

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