Dissertation Klaus Heitkamp 1999

162 6 Anhang3. Optimierungsschrittlfd. x A in x B in x C in x D in x E in X A X B X C X D X ENr. mg DPC/100 ml % m ml/min °C1 20 10 7,0 0,25 45 -1 -1 -1 -1 -12 20 10 7,0 0,45 45 -1 -1 -1 +1 -13 20 10 7,0 0,25 65 -1 -1 -1 -1 +14 20 10 7,0 0,45 65 -1 -1 -1 +1 +15 20 10 11,0 0,25 45 -1 -1 +1 -1 -16 20 10 11,0 0,45 45 -1 -1 +1 +1 -17 20 10 11,0 0,25 65 -1 -1 +1 -1 +18 20 10 11,0 0,45 65 -1 -1 +1 +1 +19 20 20 7,0 0,25 45 -1 +1 -1 -1 -110 20 20 7,0 0,45 45 -1 +1 -1 +1 -111 20 20 7,0 0,25 65 -1 +1 -1 -1 +112 20 20 7,0 0,45 65 -1 +1 -1 +1 +113 20 20 11,0 0,25 45 -1 +1 +1 -1 -114 20 20 11,0 0,45 45 -1 +1 +1 +1 -115 20 20 11,0 0,25 65 -1 +1 +1 -1 +116 20 20 11,0 0,45 65 -1 +1 +1 +1 +117 40 10 7,0 0,25 45 +1 -1 -1 -1 -118 40 10 7,0 0,45 45 +1 -1 -1 +1 -119 40 10 7,0 0,25 65 +1 -1 -1 -1 +120 40 10 7,0 0,45 65 +1 -1 -1 +1 +121 40 10 11,0 0,25 45 +1 -1 +1 -1 -122 40 10 11,0 0,45 45 +1 -1 +1 +1 -123 40 10 11,0 0,25 65 +1 -1 +1 -1 +124 40 10 11,0 0,45 65 +1 -1 +1 +1 +125 40 20 7,0 0,25 45 +1 +1 -1 -1 -126 40 20 7,0 0,45 45 +1 +1 -1 +1 -127 40 20 7,0 0,25 65 +1 +1 -1 -1 +128 40 20 7,0 0,45 65 +1 +1 -1 +1 +129 40 20 11,0 0,25 45 +1 +1 +1 -1 -130 40 20 11,0 0,45 45 +1 +1 +1 +1 -131 40 20 11,0 0,25 65 +1 +1 +1 -1 +132 40 20 11,0 0,45 65 +1 +1 +1 +1 +1Tabelle 41Versuchsplan für den 3. Optimierungsschritt