Dissertation Klaus Heitkamp 1999

6 Anhang 1634. Optimierungsschrittlfd. x A in x B in x C in x D in x E in X A X B X C X D X ENr. mg DPC/100 ml % m ml/min °C1 25 20 11,0 0,25 65 -1 -1 ⎯ -1 ⎯2 25 20 11,0 0,45 65 -1 -1 ⎯ +1 ⎯3 25 10 11,0 0,45 65 -1 +1 ⎯ +1 ⎯4 25 10 11,0 0,25 65 -1 +1 ⎯ -1 ⎯5 45 20 11,0 0,25 65 +1 -1 ⎯ -1 ⎯6 45 20 11,0 0,45 65 +1 -1 ⎯ +1 ⎯7 45 10 11,0 0,45 65 +1 +1 ⎯ +1 ⎯8 45 10 11,0 0,25 65 +1 +1 ⎯ -1 ⎯Tabelle 42Versuchsplan für den 4. Optimierungsschritt5. Optimierungsschrittlfd. x A in mg DPC/100 x B in x C in x D in x E in X A X B X C X D X ENr. ml % m ml/min °C1 35 20 11,0 0,25 65 -1 -1 ⎯ -1 ⎯2 35 20 11,0 0,45 65 -1 -1 ⎯ +1 ⎯3 35 10 11,0 0,45 65 -1 +1 ⎯ +1 ⎯4 35 10 11,0 0,25 65 -1 +1 ⎯ -1 ⎯5 55 20 11,0 0,25 65 +1 -1 ⎯ -1 ⎯6 55 20 11,0 0,45 65 +1 -1 ⎯ +1 ⎯7 55 10 11,0 0,45 65 +1 +1 ⎯ +1 ⎯8 55 10 11,0 0,25 65 +1 +1 ⎯ -1 ⎯Tabelle 43Versuchsplan für den 5. Optimierungsschritt