SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
soymilk J of Food Science 72, #7, S481-S486 (SEP 2007)
Yuan, S. H.; Chang, S. K. C.
Quantification of naltrexone and 6,beta-naltrexol in plasma and milk using gas
chromatography-mass spectrometry. Application to studies in the lactating
sheep.
Naltrexone, 6,beta-
1413 naltrexol Journal of Chromatography B (2001) 761(1), 85-92.
Ilett, Kenneth F.; Bencini, Roberta; Chan, Chooi Fen; Chiswell, Gregory M.;
GC-MS
in milk
Dusci, Leon J.; Hackett, L. Peter
Monitoring and fast detection of mycotoxin-producing fungi based on
headspace solid-phase microextraction and headspace sorptive extraction of
the volatile metabolites.
1225 Journal of Chromatography, A (2003) 985 (1-2), 127-135. GC-MS
Demyttenaere, J. C. R.; Morina, R. M.; Sandra, P.
1159 Phthalates from toys
Determination of bis(2-ethylhexyl) phthalate of plastic toys leached in stimulant
saliva by gas chromatography with solid-phase microextraction
Fenxi Ceshi Xuebao (2003) 22 (2), 34-36.
Yang, Z. J.; Zhang, W. Y.; Pan, K. Y.; Yu, J. X.; Wu, C. Y.; Wang, C. Y.
PDMS-fullerene GC
1210
Volatile fatty acids in
rumen.
Characterizing volatile fatty acids and other gases in a rumen closed in vitro
fermentation system using solid phase microextraction
Transactions of the American Society of Agricultural Engineers (2003) 46 (2),
585-588.
Chirase, Norbert K.; Koziel, Jacek A.; Spinhirne, Jarett P.
DVB/Carboxen/PDMS GC-MS
2798 Crude oil
A comparison of results obtained using liquid injection and
headspace SPME for crude oil analysis by GC-MS
J of Chrom Sci. 46, #4, 332-338 (APR 2008)
D'Auria, Maurizio; Racioppi, Rocco; Velluzzi, Vincenzina
headspace GC-MS
Volatile hydrocarbon biodegradation by a mixed-bacterial culture during growth
on crude oil.
1412 Volatile hydrocarbons Journal of Industrial Microbiology & Biotechnology (2001) 26(6), 356-362.
Van Hamme, J. D.; Ward, O. P
1311
Production of flavoured volatile organic compounds (VOCs) by Candida
oleophila GK10: Optimisation using factorial design and response surface
analysis
Enzyme and Microbial Technology (2003) 33 (5), 668-675.
Buzzini, Pietro; Davoli, Paolo; Martini, Alessandro; Pagnoni, Ugo Maria
GC-MS
2791 Bromocyclen
Enantioselective determination of the organochlorine pesticide
bromocyclen in spiked fish tissue using SPME-GC-ECD and ICP-MS
GC-ECD
in fish tissue Talanta 75, #3, 710-716 (May 15 2008) ICP-MS
1443 Organochlorine
pesticides in fish
1456
1468
Pheremones in mouse
urine
Sufentanil in human
plasma
Blanco-Gonzalez, E.; Fidalgo-Used, N.; Montes-Bayon, M.; Sanz-Medel, A
Solid-phase microextraction as a clean-up and preconcentration procedure for
organochlorine pesticides determination in fish tissue by gas chromatography
with electron capture detection
Journal of Chromatography A (2003) 1017(1-2), 35-44 GC-ECD
Blanco-Gonzalez, Elisa; Centineo, Giuseppe; Fidalgo-Used, Natalia; Sanz-
Medel, Alfredo
Identification of pheromones in mouse urine by head-space solid phase
microextraction followed by gas chromatography-mass spectrometry.
Journal of Chromatography B (2003) 796(1), 55-62 85um Carboxen PDMS GC-MS
Kayali-Sayadi, M. N.; Bautista, Jose M.; Polo-Diez, L. M.; Salazar, Ignacio
Solid-phase microextraction of human plasma samples for determination of
sufentanil by gas chromatography-mass spectrometry.
Therapeutic Drug Monitoring (2002) 24(6), 768-774
Ambient temperature, unless otherwise indicated. 100
65um PDMS DVB,
10mins, immersion
GC-MS