SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Mullett, W.M.; Levsen, K.; Lubda, D.; Pawliszyn, J. Conditions Instrument Rapid diagnosis of ulcerative colitis and Crohns disease by the 2237 Volatiles from analysis of flatus headspace GC/MS stool samples Gastroenterology 126, #4 Suppl 2, A203 (2004) Probert, Christopher S. J.; Garner, C. E.; Ratcliffe, Norman Rapid diagnosis of GI infection from flatus. 1020 Gut (2003) 52 (Supplement 1), A93. Probert, C. S.; Jones, P.; Ratcliffe, N. 1036 Semi-volatiles in saliva Solid-phase micro-extraction-gas chromatography-mass spectrometry and headspace-gas chromatography of tetrahydrocannabinol, amphetamine, methamphetamine, cocaine and ethanol in saliva samples Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences (2003) 789 (1), 73-78. PDMS GC-MS Alves Silva, Ovandir; De Moraes Moreau, Regina Lucia; Tawil, Nadia; Yonamine, Mauricio Single hair analysis of methamphetamine and amphetamine by 2711 Amphetamines solid phase microextraction coupled with in matrix derivatization Journal of Chromatography B: Analytical Technologies in the Biomedical GC in hair. and Life Sciences 842 #2, 106-110. (2006-10-02) Nishida, M.; Yashiki, M.; Namera, A.; Kimura, K. N-propoxycarbonyl derivatives 1037 Amphetamines in hair. Determination of amphetamines in human urine by headspace solid-phase microextraction and gas chromatography Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences (2003) 789 (1), 59-63. 100 um PDMS GC-FID Christopoulou, Klio; Psaroulis, Dimitrios; Raikos, Nikolaos; Theodoridis, Georgios; Tsoukali, Heleni Investigation into the production of 2-Pentylfuran by Aspergillus 2869 2-Pentylfuran fumigatus and other respiratory pathogens in vitro and human headspace GC/MS in breath breath samples Medical Mycology 46, #3, 209-215 (2008) Syhre, Mona; Scotter, Jennifer M.; Chambers, Stephen T. Determination of aldehydes in human breath by on-fibre derivatization, 2743 Aldehydes in solid-phase microextraction and GC-MS 65µm PDMS/DVB GC/MS-SIM breath J Chromatogr B 860, #1, 86-91 (2007 Dec 1) headspace Svensson, S.; Larstad, M.; Broo, K.; Olin, A. -C. PFBHA derivative An optimized method for determination of benzene in exhaled 2785 Benzene in air by GC-MS using SPME as a sampling technique GC/MS breath J Chromatogr B, 865, #1-2, 141-146 (Apr 1 2008) Amorim, Leiliane C.A.; Cardeal, Zenilda L.; Carneiro, Joana P. 2647 Organics in Breath air analysis and its use as a biomarker in biological monitoring of occupational and environmental exposure to chemical agents. air sampling GC breath J Chromatogr B, 853, #1-2, 1-9 (2007 Jun 15) Amorim, Leiliane Coelho A; de L Cardeal, Zenilda Evaluation of the SPME technique for the analysis of human 2249 Aroma compounds breath during eating PDMS GC/MS in human breath Sciences des Aliments 25 #3, 193-206 (2005) headspace Pionnier, E.; Semon, E.; Chabanet, C.; Salles, C. Application of low-temperature glassy carbon-coated macrofibers for solidphase microextraction analysis of simulated breath volatiles 1038 Volatiles in breath Analytical Chemistry (2003) 75 (7), 1604-1614. PDMS-DVB Giardina, Matthew; Olesik, Susan V. The frequency of occurrence and discriminatory power of compounds 2501 VOCs in hand found in human scent across a population determined by SPME-GC/MS headspace GC/MS odor samples J. CHROMATOGR. B, 846, #1-2, 86-97 (01 FEB 2007) Curran, A. M.; Ramirez, C. F.; Schoon, A. A.; Furton, K. G. 2250 Volatile organic Comparison of the volatile organic compounds present in human odor using SPME-GC/MS headspace GC/MS in human odor Journal of Chemical Ecology 31 #7, 1607-1619 (2005) Ambient temperature, unless otherwise indicated. 96
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Curran, Allison M.; Rabin, Scott I.; Prada, Paola A.; Furton, K. A respiration-metabolism chamber system and a GC-MS method 2271 Perfluorobutane for studying exhalation of perfluorobutane in rats after intravenous 75µm Carboxen GC-MS from exhaled air injection of the ultrasound contrast agent Sonazoid Headspace J Pharma Biomedical Analysis, 39, #3-4, 746-751 (2005) Uran, S.; Landmark, K.; Normann, P.; Hals, P.l Toft, K.;Skotland, T. Urine from stressed rats increases immobility in receptor rats 2342 2-heptanone forced to swim: role of 2-heptanone headspace GC-MS from rat urine Physiol Behav 91, #1, 166-172 (2007 May 16) Gutioerrez-Garcoa, A; Contreras, C.; Mendoza-Loopez, M.; Garcoa-Barradas, O.; Cruz-Soanchez, J Metasternal gland volatiles and sexual communication in the 2872 Pheromones triatomine bug, Rhodnius prolixus headspace GC-MS from triatomine Journal of Chemical Ecology 34, #4, 450-457 (APR 2008) bugs Pontes, Gina B.; Bohman, Bjorn; Unelius, C. Rikard; Lorenzo, Marcelo G. Male bugs modulate pheromone emission in response to vibratory signals from conspecifics. Pheromones from male 1056 bugs. Journal of Chemical Ecology (2003) 29 (3), 561-574. Renou, Michel; Lasnier, Therese; Miklas, Nadege 1057 Review article New developments and applications of solvent-free sampling and sample preparation technologies for the investigation of living systems Australian Journal of Chemistry (2003) 56 (2-3), 155-158. Pawliszyn, Janusz LC-MS 1076 Organophosphorus pesticides in blood Simple determination of 22 organophosphorus pesticides in human blood using headspace solid-phase microextraction and gas chromatography with mass spectrometric detection. Journal of Chromatographic Science (2002) 40(1), 29-34 GC-MS Musshoff, F.; Junker, H.; Madea, B. Determination of phthalic monoesters in aqueous and urine samples by solidphase microextraction-diazomethane on-fibre derivatization-gas chromatography-mass spectrometry. Phthalic monoesters in 1060 urine. Journal of Separation Science (2003) 26 (1-2), 87-96. PDMS-DVB GC-MS Alzaga, R.; Pena, A.; Bayona, J. M.* 25 C, 20 minutes, headspace 1104 PAHs in urine. Determination of polycyclic aromatic hydrocarbons in urine of coke oven workers by headspace solid phase microextraction and gas chromatography-mass spectrometry. Chemico-Biological Interactions (2003) 145 (2), 165-174. Rappaport, Stephen M.; Waidyanatha, Suramya; Zheng, Yuxin GC-MS Rapid absorption of dietary 1,8-cineole results in critical blood 2326 1,8-cineole concentration of cineole and immediate cessation of eating in the headspace GC/MS in blood common brushtail possum (Trichosurus vulpecula) J Chemical Ecology 31 #12, 2775-2790 (2005) Boyle, Rebecca R.; McLean, Stuart; Brandon, Sue; Wiggins, Natasha 1158 1,8-cineole in blood Application of solid-phase microextraction to the quantitative analysis of 1,8cineole in blood and expired air in a Eucalyptus herbivore, the brushtail possum ( Trichosurus vulpecula ). Journal of Chromatography, B: Analytical Technologies in the Biomedical and Life Sciences (2002) 780 (2), 397-406. GC Boyle, R. R.; McLean, S.; Brandon, S.; Pass, G. J.; Davies, N. W. Fatty acid ethyl esters in neonatal hair: A possible biomarker for in utero ethanol exposure. Fatty acid esters in 1162 hair. Alcoholism Clinical and Experimental Research (2003) 27 (5 supp), 39A. Koren, G.; Klein, J.; Caprara, D. Headspace solid-phase microextraction (SPME) and gas chromatography-mass spectrometry (GC-MS) for the determination of 5alpha-androst-2-en-17-one and -17beta-ol in the female Asian elephant: Application for reproductive monitoring and prediction of parturition. Ambient temperature, unless otherwise indicated. 97
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SPME Literature Literature No. Titl
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