SPME Applications Guide - Overbrook Scientific

1522
1531
1554
1551
(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
Chlorinated pesticides
in water
Organophosphorus
pesticides in cherry
and strawberry juice
Determination of chlorinated pesticides in water by SPME/GC.
Water Research (2002) 36(7), 1909-1911 100µm PDMS GC-ECD
Boussahel, R.; Baudu, M.; Bouland, S.; Montiel, A.; Moussaoui, K. M.
Headspace solid phase microextraction applied to the analysis of
organophosphorus insecticides in strawberry and cherry juices.
Journal of Agricultural and Food Chemistry (2002) 50(12), 3359-3365 Various fibers compared GC-MS
Albanis, Triantafyllos A.; Lambropoulou, Dimitra A.
Evaluation of Solid Phase Microextraction-gas chromatography in the analysis o
some pesticides with different mass spectrometric techniques: Application to
environmental waters and food samples.
Pesticides in water and
Analytical Letters (2002) 35(2), 327-338
food
Benfenati, E.; Natangelo, M.; Tavazzi, S.
GC-ITMS
Pesticides in human
blood
Headspace solid-phase microextraction in combination with gas
chromatography and tandem mass spectrometry for the determination of
organochlorine and organophosphorus pesticides in whole human blood.
Journal of Chromatography B (2002) 769(1), 65-77 GC-MS
Hernandez, F.; Beltran, J.; Lopez, F. J.; Pitarch, E.
1386 Herbicides
Applications of solid-phase microextraction ( SPME ) in the determination of
residues of certain herbicides at trace levels in environmental samples.
Journal of Environmental Monitoring (2001) 49(9), 505-508.
Ramesh, A.; Ravi, P. E.
65µm Carobwax/DVB GC-ECD
Determination of tebufenpyrad and oxadiazon by solid-phase microextraction
and gas chromatography-mass spectrometry.
Tebufenpyrad and
1384 oxadiazon. Chromatographia (2001) 54(5-6), 377-382.
Navalon, A.; Prieto, A.; Araujo, L.; Vilchez, J. L.*
100µm PDMS GC-MS
2550 2-aminoaceto-
Analysis of 2-aminoacetophenone by direct-immersion SPME-GC-MS
and its sensory impact in Chardonnay and Pinot gris wines. immersion GC-MS
phenone Food Chemistry 105, #3, 1144-1150 (2007)
in wine Wenlai Fan; I-Min Tsai; Qian, M. C.
2815 Phthalates
Determination of phthalates in wine by headspace SPME followed
by GC-MS use of deuterated phthalates as internal standards headspace GC-MS
in wine J Chromatography A 1181, #1-2, 125-130 (FEB 15 2008)
Carrillo, J. D.; Martinez, M. P.; Tena, M. T.
2535 Phthalates
Determination of phthalates in wine by headspace SPME followed by .
GC-MS. Fibre comparison and selection 65µm PDMS-DVB GC-MS
in wine J Chromatography A 1164, #1-2, 248-261 (2007)
Carrillo, J. D.; Salazar, C.; Moreta, C.; Tena, M. T.
headspace
2746 guaiacols, phenols
Determination of Brett character responsible compounds in wines by
using multiple headspace solid-phase microextraction 65µm CW-DVB GC-MS
in wine J Chromatography A 1143, #1-2, 176-181 (2007)
Pizarro, C.; Perez-del-Notario, N.; Gonzalez-Saiz, J. M.
headspace
2526 Ethylphenols
Determination of ethylphenols in wine by in situ derivatisation and
headspace solid-phase microextraction-GC-MS 50/30 DVB/CAR GC-MS
in wine Anal Bioanal Chem 387, #7, 2547-2558 (2007) headspace
Carrillo, J. D.; Tena, M. T.
Automated analysis of 2-methyl-3-furanthiol and 3-mercaptohexyl .
70C for 70 min
acetic anhydride
2573 Polyfunctional acetate at ng L minus 1 level by headspace SPME with on-fibre . 65µm PDMS-DVB GC-MS
thiols in wine derivatisation.and GC-negative chemical ionization MS determination headspace
J. Chromatogr., A 1121, #1, 1-9 (2006-07-14) 5 min
Ambient temperature, unless otherwise indicated. 193