SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 2908 Pesticides in contaminants and pesticides in environmental waters 10min immersion GC-MS water J. Chromatogr. A 1190, #1-2, 27-38 (May 9 2008) Cela, R.; Garcia-Jares, C.; Garcia-Monteagudo, J.; Llompart, M.; Regueiro, J. Strategies for the microextraction of polar organic contaminants in 2172 Polar organics water samples GC-MS in water Anal. Bioanal. Chem. 384, #7-8, 1447-1461 (2006) Quintana, Jose Benito; Rodriguez, Isaac Photochemical studies of a polybrominated diphenyl ethers (PBDES) 2268 Polybrominated technical mixture by SPME diphenyl ethers Chemosphere 60 #7, 922-928 (2005) from water Sanchez-Prado, L.; Gonzalez-Barreiro, C.; Lores, M.; Llompart, M.; Garcia-Jares, C.; Cela, R. Development of a SPME-GC-MS method for poly- 1974 Polybrominate brominated diphenyl ethers and polybrominated headspace GC-MS diphenyls/ biphenyls in water sample biphenyls Analytical Chemistry, 76, #4, 1054-1062 in water Polo, M.; Gomez-Noya, G.; Quintana, J. B.; Llompart, M.; Garcia-Jares, C.; Cela, R. Photochemical studies of a polybrominated diphenyl 1975 Polybrominate ethers (PBDES) technical mixture by SPME GC diphenyl ether Chemosphere, 60, #7, 922-928 from water Cela, R.; Garcia-Jares, C.; Gonzalez-Barreiro, C.; Llompart, M.; Lores, M.; Sanchez-Prado, L. Determination of PDMS-seawater distribution 1976 PCBs in coefficients for PCBs and chlorinated biphenyls 100µm PDMS GC-MS water and chlorinated pesticides by SPME-GC-MS 12 day extraction J. Chromatogr. A,1066, #1-2, 165-175 immersion Zeng, E; Tsukada, D; Noblet, J.; Peng, J Multivariate optimization of a SPME method for the 1977 Phthalate analysis of phthalate esters in environmental waters Various fibers GC-MS esters in J. Chromatogr. A,1072, #1, 63-72 direct immersion & water Cela, R; Garcia-Jares, C; Llompart, M Polo, M headspace New approach of SPME improving the extraction 1978 Tin compounds yield of butyl and phenyltin compounds by combining Ethylate derivatives GC in water the effects of pressure and type of agitation headspace J. Chromatogr. A,1072, #1, 19-27 agitated Bueno, M; Darrouzes, J; Holeman, M; Pecheyran, C; Potin-Gautier, M Determination of aliphatic amines using N-succinimidyl 1979 Aliphatic benzoate as a new derivatization reagent in 60min @ 80°C GC-MS amines GC combined with SPME headspace GC-FID in water J. Chromatogr. A,1021, #1-2, 175-181 succinimidyl benzoate Zhao, Y.; Cai, L.; Jing, Z.; Wang, H.; Yu, J.; Zhang, H. derivatives Analytical methods applied to the determination of heterocyclic 2834 Aromatic aromatic amines in foods Review article amines in J. Chromatogr. B,862, #1-2, 15-42 (Feb 1 2008) food Afonso, A.M.; Ayala, J.H.; Gonzalez, V.; Sanz Alaejos, M. In situ derivatization/SPME determination of polar 1980 Aromatic aromatic amines. 65µm PDMS-DVB GC-MS amines in Analytical Chemistry, 76, #4, 1028-1038 diazotation/ iodination water Zimmermann, T.; Ensinger, W. J.; Schmidt, T. C.* Determination of aromatic amines in waste water by 1981 Aromatic SPME-GC GC amines in Fenxi Ceshi Xuebao, 23, #3, 18-21 water Peng, J. G.; Wang, D. H.; Wu, C. Y. Comparative study of the use of flow-through 1982 Phenols in systems with and without air segmentatio 80µm polyacrylate GC water determination of phenols by SPME-GC 100µm PDMS Chromatographia, 59, #5-6, 387-391 immersed Nome, R. C.; Carasek, E. * 1983 Aldehydes Determination of low-molecular mass aldehydes by automated headspace spme with in-fibre derivatisation headspace GC-FID Ambient temperature, unless otherwise indicated. 174
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument in water J. Chromatogr. A, 1071, #1-2, 147-154 PFBHA derivatives O'Reilly, John; Pawliszyn, Janusz; Wang, Qing Determination of low-molecular mass aldehydes by automated 1984 Aldehydes in headspace SPME with in-fibre derivatization PFBHA derivatives GC-FID water J. Chromatogr. A, 1071, #1-2,147-154 headspace Wang, Qing; O'Reilly, John; Pawliszyn, Janusz Concentration and fate of persistent organochlorine pesticides 2197 Organochlorine in estuarine sediments using headspace SPME headspace pesticides in Chemosphere 62, #11,1869-1878 (2006) sediments Chang, Sue-Min; Doong, Ruey-An Determination of organochlorine pesticides in ground water samples 2388 Organochlorine using SPME by GC-ECD 50/30µm DVB/CAR GC-ECD pesticides in Talanta 72, #5, 1833-1841 (2007-07-31) immersion water Raposo, J. L., Jr.; Re-Poppi, N. Analysis of organochlorine pesticides in water by 1985 Organochlorine novel activated carbon fiber SPME coupled w/GC-MS GC-MS pesticides J. Environ. Sci. Health Part B, 39, #2, 235-248 in water Fang, N; Jia, J; Sun, T; Wang, Y; Yu, J Development and validation of a methodology for the determination 2240 Tebuthiuron and of pesticides in water by SPME-LC/DAD 85µm polyacrylate LC/DAD diuron in water J. Liq. Chromatogr. 28 #18, 2909-2919 (2005) 50 minutes, Brondi, Silvia H. G.; Lancas, Fernando M.; Rodrigues Da Silva, Jose C. Optimization of a methodology for the determination 1986 Organochlorine of organochlorine pesticides in surface water by 85µm polyacrylate GC-MS pesticides SPME-GC-MS 40min @ >20°C in water J. Environ. Sci. Health Part B, 40, #4, 513-523 agitation Brondi, Silvia Helena G.; Lancas, Fernando M. immersed sampling GC-MS methodology using SPME for the multiresideu 1987 Pesticides in determination of pesticides in surface waters. 65µm PDMS-DVB GC-SIM-MS surface water Intl J Env Analytical Chem, 84, #14-15, 1079-1092 Albanis, T; Hela, D.; Lambropoulou, D.; Sakkas, V. Pesticides in Esteros del Ibera (AR): Evaluation of 1988 Endosulfan, impacts and proposal of guidelines for water immersed sampling GC-MS carbofuran quality protection in water Ecol. Model., 86, #1, 85-97 Boia, C; Borrego, C; Silva, C; Valente, J Optimization and application of SPME for the GC 1989 Endosulfan, determination of endosulfan and its major metabolites 100µm PDMS GC-ECD in water in the ng L/sup-1 / range in aqueous solutions 30% NaCl GC-MS Anal. Bioanal. Chem., 376, #1, 61-68 Deger, A.B.; Frimmel, F.H.; Gremm, T.J.; Mendez, L. Determination of membrane permeability without calibration 2306 PAHs in using (SPME) PDMS GC water J. Membr. Sci. 68 #1, 65-73 (2005) Liu, Xinyu; Pawliszyn, Janusz Application of membrane techniques to water 1990 Phthalates purification. Removal of phthalates 65µm CW/DVB GC-FID in water Desalination, 162, #1-3, 121-128 Bodzek, M; Dudziak, M; Luks-Betlej, K Degradation of PAHs in aqueous solutions by 1991 PAHs ultrasonic irradiation 20°C & 40°C GC-MS in water J. Hazard. Mater., 108, #1-2, 95-102 immersed sampling Goula,G; Kalogerakis,N; Mantzavinos,D; Psillakis, E sonicated Oxidative microbial transformation of vinyl chloride 1992 Vinyl chloride under anaerobic conditions in ground water headspace GC-MS in water Proc. of the Third Int. Conf. on Rem. of Chlorinated and Recalcitrant 2002, pp1571-1578 Banwart, S; Holliger, C; Morgan, Pl; Shah, N.; Szynalski, K. Determination of adipate in water with 1993 Adipate in headspace SPME and single ion monitoring GC-MS Headspace GC-MS water Fenxi Shiyanshi, 23, #4, 77-80 Ambient temperature, unless otherwise indicated. 175
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