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SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />

Analyte / Extraction<br />

Matrix Literature Reference Conditions Instrument<br />

443 Organophosphate (<strong>SPME</strong>) Before Capillary Gas Chromatography GC-NPD, -MS<br />

pesticides Hochudoku 13 (2): 122-123 (1995)<br />

in water Lee, X., Kumazawa, T., Taguchi, T., Sato, K., Suzuki, O.<br />

167 Organophosphorus<br />

Analysis of Organophosphorus Insecticides from<br />

Environmental Samples Using <strong>SPME</strong> 85µm polyacrylate GC-NPD<br />

insecticides J. Chromatogr. A 736: 219-228 (1996) 60°C, 60 min<br />

in water Magdic, S., Boyd-Boland, A., Jinno, K., Pawliszyn, J.<br />

Solventless sample preparation procedure for<br />

immersion<br />

salt added<br />

861 Organophosphorus organophosphorus pesticides analysis using <strong>SPME</strong> and HPLC<br />

pesticides on-line supercritical fluid extraction/HPLC technique.<br />

in water Analytica Chimica Acta (2001) 433(2) 207-215<br />

Jinno, K; Kiso, Yoshiaki; S, Yoshihiro; S, Shamsul H<br />

93 Organophosphorus<br />

Matrix Effects on <strong>SPME</strong> of Organophosphorus<br />

Pesticides from Water 85µm polyacrylate GC-NPD<br />

pesticides J. Chromatogr. A 767: 195-203 (1997) 60°C, 45 min<br />

in water Valor, I., Molto, J., Apraiz, D., Font, G.<br />

<strong>SPME</strong> of 52 pesticides and polychlorinated biphenyls:<br />

immersion<br />

stirring<br />

839 52 Pesticides, PCBs efficiencies of the <strong>SPME</strong> coatings PDMS, polyacrylate,<br />

PDMS/DVB, Carboxen/PDMS, and Carbowax/DVB<br />

J. Sep. Sci. 2001) 24(1), 39-48<br />

Valor, I; Perez, M; Cortada, C; Apraiz, D; Molto, J; Font, G<br />

65µm PDMS/DVB<br />

118 Organophosphorus<br />

Solid Phase Microextraction of Organophosphorus<br />

Pesticides from Water 65µm PDMS/DVB<br />

pesticides J. Chromatogr. A 759: 225-230 (1997) 30 min<br />

in water Sng, M., Lee, F., Lakso, H. immersion<br />

524 Organophosphorus<br />

Determination of organophosphorus pesticides in water<br />

using GC-MS 100µm PDMS GC-MS<br />

pesticides Qim. Nova (1999), 22(2), 197-200<br />

in water Silva, F., Cardeal, Z., De Carvalho, C. Portuguese<br />

Headspace solid-phase microextraction for the gas chromatographic<br />

2579 Organophosphorus analysis of organophosphorus insecticides in vegetables 100µm PDMS GC-FPD<br />

pesticides J AOAC Int 90, #6, 1677-81 (2007 Nov-Dec) headspace<br />

in vegetables Fytianos, K.; Drimaropoulou, G.; Raikos, N.; Theodoridis, G.; Tsoukali, H.<br />

350 Organophosphorus<br />

The Application of <strong>SPME</strong> in the Analysis of<br />

Organophosphorus Pesticides in a Food Plant 100µm PDMS GC-FPD<br />

pesticides Environ Sci. Technol. 1998, 32, 3816-820 90 min<br />

in food plant Chen, W., Poon, K., Lam, M. immersion (water)<br />

525 Pyrethrins in<br />

Heterogenic catalytic hydrolysis and analysis of natural<br />

pyrethrins in subcritcal water coupled w/<strong>SPME</strong>-GC-MS 100µm PDMS GC-FID or<br />

insect spray, Fresenius'J. Anal. Chem. 1999, 364(7), 625-630 20 min @ pH 2 MSD<br />

shampoo, flowers Krappe, M, Hawthorne, S., Weclawiak, B. immersed<br />

705 Pyrethroids<br />

<strong>SPME</strong> of pyrethroid pesticides from water at low and<br />

sub-ppt levels at different temperature 100µm PDMS GC-ECD<br />

in water J.High Resolut.Chromatogr. (2000), 23(7/8), 485-488 5 min<br />

Barrionuevo, W., Lancas, F. 40-90°C<br />

837 Pyrethroids<br />

Solid-phase extraction (SPE) and solid-phase microextraction<br />

( <strong>SPME</strong> ) of pyrethroids in water<br />

in water Quim. Nova (2001), 24(2), 172-175<br />

Barrionuevo, W., Lancas, F.<br />

299 Organophosphorus<br />

Online Determination of Organophosphorus Pesticides in<br />

Water by <strong>SPME</strong> and GC with Thermionic-Selective Detection 30µm PDMS GC-TCD<br />

pesticides J. High Resolut. Chromatogr. 20 (9): 487-492(1997 30 min<br />

in water Lopez-Avial, V., Young, R., Becker, W. immersion<br />

Ambient temperature, unless otherwise indicated. 185

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