SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
Nishikawa, M., Watanabe, K., Suzuki, O. stirring
142 Phenothiazines
Detection of Some Phenothiazines by Headspace SPME
and GC 100µm PDMS GC-FID
urine, blood Jpn. J. Forensic Toxicol. 14: 30 (1996) 40 min @ 140°C
Kumazawa, T., Seno, H.,, Ishii, A., Hattori, H., Sato, K., headspace
Watanabe, K., Suzuki, O. NaCl added
947 Propranolol
In-Tube Molecularly Imprinted Polymer SPME for the selective
Determination of Propranolol
Anal. Chem (2001) 73(11) 2383-2389
Mullett, Wayne M.; Martin, Paul; Pawliszyn, Janusz
Quantification of plasma and urinary levels of furan in healthy individuals
2480 Furan FASEB Journal. 21, #6, A1066 (APR 2007) GC-MS
in plasma, urine Jun, Hee-Jin; Chung, Mi Ja; Park, Young-Sik; Lee, Kwang-Geun; Lee, S.
Application of (SPME) technique for the detection of
946 Carbofuran carbofuran in serum
in seum J. Can. Soc. Forensic Sci(2001) 34(1), 23-26
Ameno, K.; Lee, S-K.; Ameno, S.; Kinoshita, H.; Kubota, T.;
Zhang, X.; Ijiri,
908 Dinitroaniline
Headspace SPME and GC determination of dinitroaniline
herbiciede s in human blood, urine and environmental water 100µm PDMS GC-ECD
in blood, urine J. Chromatogr. B. (1998), 714(2), 205-213 30 min @ 70°C
and water Guan, F., Watanabe, K., Ishii, A., Seno, H., Kumazawa, T., headspace
Hattori, H., Suzuki, O. NaSO4
2809 Pesticides
Reliable identification of pesticides using linear retention indices
as an active tool in GC-MS analysis
J. Chromatogr. A.1186 (1-2), 430-433 (Apr 4 2008)
Casilli, A.; Dugo, G.; Dugo, Paola; Mondello, L.; Salvatore, Angelo;
Tranchida, Peter Quinto
GC-MS
2636 Pesticides in
Evaluation of the pesticide contamination of groundwater sampledl
over two years from a vulnerable zone in Portuga GC-ECD
ground water J Agri Food Chem 55, #15, 6227-6235 (2007)
Goncalves, C. M.; Silva, J. C. G. E. da; Alpendurada, M. F
GC-MS
2412 Phenylurea and
Analysis of phenylurea and propanil herbicides by SPME-LC
combined with post-column photochemically induced 60µm PDMS/DVB HPLC-PIF-FD
propanil herbicides fluorimetry derivatization and fluorescence detection fluorimetry
in ground water Anal. Chim. Acta 593, #2, 157-163 (2007-06-19)
Mughari, A. R.; Parrilla Vazquez, P. ; Martinez Galera, M.
derivatization
183 Herbicides
SPME and GC-ECD Determination of Dinitroaniline Herbicides in
Surface Water and Biological Fluids 100µm PDMS GC-ECD
in water and Jpn. J. Forensic Toxicol. 15 (2): 151-153 (1997) 30 min @ 70°C water
biological fluids Prosen, F., Watanabe, K., Ishii, A., Seno, H., Suzuki, O.
Gas chromatographic determination of organochlorine and
@ 90°C blood
Na2SO4, headspace
860 Organochlorine & organophosphorus pesticides in human fluids using SPME GC/ECD/FPD
organophosphorus Analytica Chimica Acta (2001) 433(2) 217-226
pesticides in
biological fluids
Hernandez, F.; Beltran, J.; Egea, S.; Lopez, F. J.; Pitarch, E.
Detection of Organophosphate Pesticides in Human Body
66 Organophosphate Fluids by Headspace SPME and Capillary GC with 100µm PDMS GC-NPD
pesticides Nitrogen-Phosphorus Detection 100°C, 20 min
in urine, blood Chromatogrphia 42(3/4): 135-140 (1996)
Lee, X., Kumazawa, T., Taguchi, T., Sato, K., Suzuki, O.
pH 3 with HCl
875 Organophosphorus
Optimisation of SPME conditions for headspace analysis
of organophophorus pesticides in whole blood
pesticides in Z Zagadnien Nauk Sadowych, 42(2000) 47-59
whole blood Asri, K., Anderson, R.
Ambient temperature, unless otherwise indicated. 119