SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
pesticides, PCBs Chromatographia, 1999, 49(11/12), 686-690
from water Popp, P., Paschke, A.
904 pesticides
Analysis of fire ant pesticides in water by SPME and GC-MS
and LC-MS GC-MS &
in water Analytica Chimica Acta 2001, 436(1) 11-20
Reyzer, M., Brodbelt, J.
LC-MS
Optimisation and validation of a SPME method for simultaneous
2413 Pesticides determination of different types of pesticides in water by GC-MS 60µm PDMS/DVB GC-MS
in water J. Chromatogr., A 1141, #2, 165-173 (2007-02-09)
Beceiro-Gonzalez, E. ; Concha-Grana, E.; Guimares, A.; Goncalves, C.;
Muniategui-Lorenzo, S.; Alpendurada, M.
45 min @ 60°C
770 Chlorine, nitrogen
Multiresidual method for determination of chlorine,
nitrogen, and phosphorus containing pesticides in surface GC/ECD/NPD
phosphorus and drinking water by SPME and GC/ECD/NPD
pesticides Boll. Chim. Ig., Parte Sci. (2000) 51(S3), 99-103
in water de Luca, Giuseppe; Mura, Michele
(in Italian)
512 Iodinated THMs
SPME for the determination of iodinated trihalomethanes in
drinking water 65µm CW/DVB/PDMS GC-ECD
in drinking water J. Chromatogr., A (1999), 841(2), 197-206 10 min @ 20°C
Cancho, B., Ventura, G., Galceran, M. NaCl used
292 Iodinated organics
Solid Phase Microextraction and Analysis of Iodinated
Organic Compounds 85µm polyacrylate GC-ECD
in water Avail. UMI, Order No. DA9812871 from:
Diss. Abstr. Int., B 58 (10): 5364 (1998)
Frazey, P.
288 Iodinated volatiles
SPME with Temperature-Programmed Desorption for the
Analysis of Iodinated Disinfection Byproducts 85µm polyacrylate GC-ECD
in water Anal. Chem. 70 (3): 638-644 (1998) 15 min
Frazey, P., Barkley, R., Siever, R.
Simultaneous determination of cyanogen chloride and
immersion
stirring
694 Cyanogen chloride cyanogen bromide in treated water at sub-ug/L levels by a Carboxen/DVB/PDMS GC-ECD
in water new SPME-GC-ECD method 15 min, headspace
J. Chromatogr. A 897(2000) 307-315
Cancho, B., Ventura, F., Galceran, M.
2-3pH, 25% salt added
Determination of acetic acid in aqueous samples, by
695 Acetic acid water-phase derivatization, SPME, and GC 85µm Polyacrylate GC-FID
in water J. Chromatogr. A., (2000), 874(2), 225-234 headspace
Wittmann, G., Van Langenhove, H., Dewulf, J. benzenal bromide derv.
Determinationof Chlorinated Acetic Acids in Drinking
411 Chloroacetic acids Water by in-situ Derivatization-SPME
in water Interri J. Environ. Anal. Chem. 66: 215-224 (1997)
Aikawa, B., Burk, R.
SPME coupled with GC-ion trap mass spectrometry for the
520 Haloacetic acids analysis of haloacetic acids in water GC-Iontrap
in water J. Chromatogr., A 1999, 859(2), 159-172 MS
Sarridon, M., Santos, F., Galceran, M.
696 Haloacetic acids
In situ derivatization/SPME for the determination of
haloacetic acids in water Carboxen/PDMS GC-ITMS
in water Anal. Chem. 2000 Oct. 15, 72(20), 4865-4873
Sarrion, M. Santos, F., Galceran, M.
Using SPME to Determine Partition Coefficients to Humic Acids
headspace
dimethyl sulfate derv.
353 Chlorobenzenes and Bioavailable Concentrations of Hydrophobic Chemicals 7µm PDMS GC-FID
in water Environ.Sci Technol, 1998, 32, 3430-3435 20 min
Ramos, E., Meijer, S., Vaes, W., Verhaar, H., Hermens, J.
SPME-capillary GC determination of chlorobenzene
immersion
pH 7
Ambient temperature, unless otherwise indicated. 159