SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />
Analyte / Extraction<br />
Matrix Literature Reference Conditions Instrument<br />
in drugs Zasshi 16: 251 (1996)<br />
Yakugaku<br />
473 Residual solvents<br />
Headspace <strong>SPME</strong> method optimization for<br />
residual solvent analysis 65µm DVB/PDMS GC<br />
pharmaceutical Acta pharm. Hung., 1999, 69(2), 77-84 30 min headspace<br />
samples Camarasu, C., Mezei, M., Szabo, A 2gm NaCl,<br />
919 Residual solvents<br />
Headspace <strong>SPME</strong> method development for the analysis of<br />
volatile polar residual solvents by GC-MS<br />
pharmaceutical J. Pharm. & Biomediecal Aanlysis 2000, 23(1) 197-210<br />
samples Camarasu, C.<br />
Verapamil drug metabolism studies by automated in-tube solid phase<br />
microextraction.<br />
1002 Verapamil Jnl of Pharmaceutical and Biomedical Analysis (2002) 30 (2), 307-319. LC-MS<br />
Walles, M.; Mullett, W. M.; Levsen, K.; Borlak, J.; Wuensch, G.; Pawliszyn, J.<br />
New trends in sample preparation for clinical and pharmaceutical analysis<br />
1006 Trends TrAC-Trends in Analytical Chemistry (2003) 22 (4), 232-244.<br />
Kataoka, Hiroyuki<br />
1024 clenbuterol<br />
Solid-phase micro extraction (<strong>SPME</strong>) and headspace derivatization of<br />
clenbuterol followed by GC-FID and GC-SIMMS quantification.<br />
Analytical and Bioanalytical Chemistry (2003) 375 (3), 460-464.<br />
Wenclawiak, B. W.; Engelmann, M. D.; Hinz, D.<br />
85 µm polyacrylate GC-FID, GC-SIMMS<br />
Residual solvent testing: A review of gas-chromatographic and alternative<br />
techniques.<br />
1032 Review Pharmaceutical Research (Dordrecht) (2003) 20 (3), 337-344.<br />
B'Hymer, Clayton<br />
New designer drug 4'-methyl-alpha-pyrrolidinohexanophenone: Studies on its<br />
metabolism and toxicological detection in urine using gas chromatographymass<br />
spectrometry.<br />
1101 MPHP in urine Journal of Chromatography B (2003) 789 (1), 79-91. GC-MS<br />
Maurer, Hans H.; Fritschi, Giselher; Peters, Frank T.; Springer, Dietmar<br />
1107 Residual solvents<br />
Use of solid-phase microextraction coupled with gas chromatography for the<br />
determination of residual solvents in pharmaceutical products<br />
Journal of Chromatography A (2003) 999 (1-2), 195-201.<br />
Dugay, Jose; Legrand, Stephanie; Vial, Jerome<br />
Various<br />
1133<br />
1142<br />
Residual solvents in<br />
drug products<br />
Unknown residual solvents identification in drug products by headspace solid<br />
phase microextraction gas chromatography-mass spectrometry.<br />
Chromatographia (2002) 56(supplement), S131-S135 headspace GC-MS<br />
Camarasu, C. C.<br />
Determination of volatile residual solvents in traditional Chinese medicines by<br />
headspace solid-phase microextraction and cryogenic gas chromatography with<br />
flame ionization detection<br />
Volatile residual<br />
solvents in Chinese<br />
medicines. Journal of AOAC International (2003) 86 (3), 461-466. PDMS/DVB GC-FID<br />
Jiang, Guibin; Liu, Jiemin; Liu, Jingfu; Liu, Jiyan; Wen, Meijuan; Zhou, Qunfang<br />
Determination of methylmalonic acid and glutaric acid in urine by<br />
2608 Methylmalonic & aqueous-phase derivatization followed by headspace <strong>SPME</strong>-GC-MS 100 µm PDMS GC/MS<br />
glutaric acid J. Sep. Sci. 30, #2, 266-271 (2007-02) 55°C for 30 min,<br />
in urine Li, N.; Deng, C. H.; Zhang, X. M. diethyl sulfate<br />
derivatives<br />
Development of <strong>SPME</strong>-GC method to determine<br />
2324 Methylformamide N-hydroxymethyl-N-methylformamide and N-methylformamide in urine 65µm DVB/PDMS GC-NPD<br />
in urine J. Chromatogr. B, 828 #1-2, 103-107 (2005) headspace<br />
Knupp, V.; Alvarez Leite, Edna Maria; de Lourdes Cardeal, Zenilda 80°C for 15 min,<br />
Ambient temperature, unless otherwise indicated. 92
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