SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument PAHs Luan, T.; Fang, S.; Zhong, Y.; Lin, L.; Chan, S. M. N.; Lan, C.; Tam, N. identification of gasoline soot in suspect arson 1909 PAHs in cases by using headspace SPME-GC-MS 100µm PDMS GC-MS gasoline soot Analytical Letters, 236, #7, 1373-1384 75µm Carboxen Wu, Chia-Hao; Chen, Chin-Lien; Huang, Ching-Te; heaspace Lee, Maw-Rong; Huang, Chih-Ming Quantification of propane in biological materials 1910 Propane in by headspace GC headspace GC-MS biological Forensic Science International, 151, #2-3, 165-170 materials Park, J; Min, Ji-Sook; Heo, S.; Lim, Mi-Ae; Park, S The study of fingerprint characteristics of the emanations 1911 Volatile from human arm skin using the original sampling headspace GC-MS organics system by SPME-GC-MS 30min sampling from human J. Chromatogr. B, 822, #1-2, 244-252 skin Cai, Ji-Jin; Li, Gong-Ke; Ruan, Gui-Hua; Zhang, Zhuo-Min Extraction of capsaicin in aerosol defense sprays from fabrics 1912 Capsaicin Talanta, 67, #2, 377-382 headspace GC from fabrics Almirall, Jose R.; Spicer Jr., Oliver Identification of dominant odor chemicals emanating from 1913 Odor explosives for use in developing optimal training aid headspace GC-MS chemicals in combinations and mimics for canine detection GC-ECD explosive Talanta, 67, #2, 313-327 Almirall, Jose R.; Furton, Kenneth G.; Harper, Ross J. Evaluation of sample recovery of malodorous gases from air 2235 Odorous gases sampling bags, SPME, and sampling canisters 75µmCarboxen GC/MS from livestock Annu. Int. Meet., (2004) p5547-5562 headspace operations Koziel, J.; Kuhrt, F.; Lloyd, J.; Parker, D.; Spinhirne,J.; Wright,D. Evaluation of sample recovery of malodorous livestock gases from 2265 Malodorous gases air sampling bags, SPME fibers, Tenax TA sorbent tubes, 75µm Carboxen GC/MS from livestock and sampling canisters headspace J. Air Waste Manage. Assoc. 55, #8, 1147-1157 (2005) Koziel, J.; Kuhrt, F.; Lloyd, J.; Parker, D.;Spinhirne, J.; Wright, D. 2657 Volatiles found Headspace-SPME preconcentration of phenols, indoles and on-fibre derivatised volatile fatty acids in liquid and gas samples from cow slurries DVB/Car 50/30µm GC/MS in cow slurry J. Sep. Sci. 30, #14, 2293-2304 (September 2007) headspace Arana, G,; Larreta, J.; Vallejo, A.; Bilbao, U.; Alonso, A.; Zuloaga, O. Optimisation of the on-fibre derivatisation of volatile fatty acids in the MTBSTFA derivative 2588 Volatiles found simultaneous determination together with phenols and DVB/Car 50/30µm GC in cow slurry indoles in cow slurries headspace Anal Bioanal Chem 389, #5, 1603-1609 (NOV 2007) MTBSTFA Larreta, J.; Usobiaga, A.; Etxebarria, N.; Arana, G.; Zuloaga, O. derivative Experimental design to optimise the analysis of organic volatile 2459 Volatiles found compounds in cow slurry by headspace SPME-GC-MS 100µm PDMS GC/MS in cow slurry J. Chromatogr., A 1136, #1, 1-9 (2006-12-08) 75µm Carboxen Larreta, J.; Vallejo, A.; Bilbao, U.; Alonso, A.; Arana, G.; Zuloaga, O. headspace Methylation 2477 Odor from Identification of volatile organic compounds in the manures of cow, hog and chicken by SPME-GC-MS 65µm PDMS-DVB GC-MS manures Se Pu 25, #3, 425-9 (2007 May) 30 min at 60°C Huang, Jun; He, Jin; Zhang, Jibin; Yu, Ziniu sat.NaCl headspace In chinese Multidimensional GC-olfactometry for the identification and 2221 Malodors of prioritization of malodors from confined animal feeding operations GC-MS livestock operations J Ag Food Chem, 53, #22, 8663-8672 (2005) Wright, D.; Eaton, D..; Nielsen, L.; Kuhrt, F.; Koziel, J.,. Spinhirne, J.; Parker, D 2316 Odor from Effect of ozonation on odor and the concentration of odorous organic compounds in air in a swine housing facility air sampling GC swine Trans. Am. Soc. Agric. Eng. 48 #6, 2297-2302 (2005) facilities Davies, S.H.; Hill, J.D.; Kim-Yang, H.; Von Bernuth, R.D. Ambient temperature, unless otherwise indicated. 134
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Analysis of odorous compounds in swine buildings and their 2144 Odor from relationship to thermal environment, management and Air sample GC/MS swine categories of pigs facilities Livestock Environ. Proc. Seventh Int. Symp 334-340 (2005) Dahl, P.; Johnsen, J.; Maahn, M.; Segaard, H.;Takai, H.; Tegersen, F. Simultaneous chemical and sensory characterization of volatile organic 2759 Odor from compounds and semi-volatile organic compounds emitted from swine 85µm Carboxen GC/MS swine manure manure using SPME and multidimensional GC-MS-olfactometry headspace J. Environ. Qual. 37, #2, 521-534 (2008) Cai, L.; Hoff, Steven J.; Jenks, W.; Koziel, Jacek A.; Lo, Yin-Cheung M.; Xin, Hongwei Characterization of volatile organic compounds and odorants 2161 Volatiles in associated with swine barn particulate matter using SPME-MS- 75µm Carboxen GC-MS swine particulate olfactometry headspace matter J. Chromatogr. A, 1102, #1-2, 60-72 (2006) Cai, Lingshuang; Koziel, Jacek A.; Lo, Yin-Cheung; Hoff, Steven J. Environmental 1914 Auto exhaust Formation and reaction of hydroxycarbonyls from the reaction of OH radicals with 1,3-butadiene and isoprene pentafluorobenzyl API-MS Environ. Sci. Technol., 39. #11, 4091-4099 hydroxyl amine GC/FID Arey, Janet; Atkinson, Roger; Baker, Jillian derivatives Photochemical sources of organic acids. 1. Reaction 1915 Carboxylic of ozone with isoprene, propene, and 2-butenes headspace GC-MS acids under dry and humid conditions using SPME in air J Phys Chem A, 109, #24, 5358-5365 Orzechowska, Grazyna; Paulson, Suzanne Rate coefficients for the gas-phase reaction of 1916 Byproducts isoprene with N0 3 and NO 2 headspace GC/FID of reactions Int J Chem Kinet, 37, #2, 57-65 Johnson, M.; Langer, S.; Stabel, J. 1,4-Hydroxycarbonyl products of the OH radical initiated 1917 Hydroxyl- reactions of C5-C8 n-alkanes in the prescence of NO on-fiber hydroxylamine GC-MS carbonyls Environ. Sci. Technol., 39. #12, 4447-4453 derivatives GC/FID in Air Arey, Janet; Aschmann, Sara M.; Atkinson, Roger; Reisen, F Occurrence and abatement of volatile sulfur 1918 Volatile sulfur compounds during biogas production headspace GC-MS from biogas J. Air Waste Manage. Assoc, 54, #7, 855-861. production Andersson, F.; Ejlertsson, J.; Karlsson, A.; Svensson, B. Headspace SPME followed by GC/PFPD for the analysis of 1920 Sulfur compd malodorous sulfur compounds liquid industrial effluents 65µm PDMS-DVB GC/PFPD industrial Anal and Bioanal Chemistry, 378, #1, 190-196 75µm Carboxen effluents Desauziers, V.; Fanlo, Jean-Louis; Lestremau, F. 5 or 60 min headspace Air/polymer distribution coefficients for 1921 PAHs in PAHs by SPME sampling. PDMS coated fibers GC-MS air J Chromatography, A, 1029, #1-2, 263-266 Kolar, K.; Ciganek, M.; Malecha, J. Selective extraction of trace levels of polychlorinated and 1922 Organo- polybrominated contaminants by supercritical fluid-SPME and GC/MS/MS halogenated determination by GC-MS. Application to aquaculture fish in fish feed feed and cultured marine species Anal. Chem., 77, #7, 2259-2265 Carro, A.M.; Lorenzo, R.A.; Rodil, R.; Torrijos, R. Cela Round-robin evaluation of a SPME-GC for reliable determination of 2389 Ethylene oxide trace level ethylene oxide in sterilized medical devices GC in air Biomed Chromatogr: 22, #2, 136-48 (-2008 Feb) Harper, T.; Cushinotto, L.; Blaszko, N.; Arinaga, J.; Davis, F.; Cummins, C.; Dicicco, M. Laboratory and field validations of a SPME 1923 Ethylene oxide device for the determination of ethylene oxide. 75µm Carboxen GC in air J Chromatogr A, 1026, #1-2, 25-30 HBr on-fiber derivative Ambient temperature, unless otherwise indicated. 135
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