SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument in air Anal. Chem., 2001, 73(1), 47-54 Koziel, J., Odziemkowski, M., Pawliszyn, J. 10 sec 739 Aerosols, particulate Sampling and Raman Confocal Microspectroscopic Analysis of Airborne Particulate Matter Using Poly(dimethylsiloxane PDMS Raman in air Solid-Phase Microextraction Fibers Anal. Chem (2001) 73(13), 3131-3139 Odziemkowski, M.; Koziel, J.; Irish, D.; Pawliszyn, J. Study of preservation of polydimethylsiloxane/carboxen SPME fibres 2714 Volatiles in before and after sampling of volatile organic compounds in indoor air. 75µm Carboxen GC-MS Indoor air J. Chromatogr. A 1124, #1-2, 106-111 (2006-08-18) Larroque, V.; Desauziers, V. ; Mocho, P Volatile organic compounds in indoor environments 2236 Volatiles in HANDBOOK OF ENVIRONMENTAL CHEMISTRY, (2004) p1-35 book Indoor air Ayoko, Godwin A. 574 Solvents Application of SPME to monitoring indoor air quality. Fresenius'-J-Anal-Chem. Apr 1999; 363(7): 696-699 100µm PDMS GC-MS in air Gorlo,-D; Zygmunt,-B; Dudek,-M; Jaszek,-A; Pilarczyk,-M; Namiesnik,-J 15 min 542 Organic pollutants Application of SPME to monitoring indoor air quality Fresenius' J. Anal. Chem. (1999), 363(7), 696-699 100µm PDMS GC-MS in air Gorlo, D., Zygmunt, B., Dudek, M., Jaszek, A, Pilarczyk, M., Maniesnik, J. Time-weighted average water sampling with a SPME device 2293 PAHs in Anal. Chem. 77 #22, 7319-7325 (2005) PDMS GC water Chen, Yong; Ouyang, Gangfeng; Pawliszyn, Janusz 543 Organic vapors Time-Weighted Average Sampling with SPME Device; Implications for Enhanced Personal Exposure Monitoring to 100µm PDMS in Air Airborne Pollutants Anal. Chem. (1999), 71(8), 1513-1520 Martos, p. Pawliszyn, J. 932 Organic vapors Time-weighted average sampling of volatle and semivolatile airborne organic compounds by the SPME device in Air J. Chromatogr. A (2000), 892(1-2), 455-467 Khaled, A, Pawliszyn, J. 306 VOCs Application of Solid Phase Microextraction for Determination of Volatile Halogenated Hydrocarbons in Air and Water in water and air of an Indoor Swimming Pool Fresenius’ Environ. Bull. 5 (1+2): 55-60 (1996) Czerwinski, J., Zygmunt, B., Namiensnik, J. 307 Pollution A Case Study of Indoor Pollution by Chinese Cooking Toxicol. Environ. Chem. 65 (1-4): 217-224 (1998) in air Benfenati, E., Pierucci, P., Niego, A. 347 VOCs Nonequilbrium Quantitation of Volatiles in Air Stream by SPME Anal. Chem. Vol. 71, January 1, 1999, pg. 92-101 7µm, 30µm, 100µm GC-FID in air Bartelt, R., Zilkowski, B. PDMS 27°C, 30 min gas sampling 2605 Volatiles in High-molecular products analysis of VOC destruction in atmospheric pressure discharge 65µm CW/PDMS GC-FID atmosphere J. Phys., Conf. Ser. (UK) 63, #1, 6 (2007) Car/DVB 30/50µm Grossmannova, H.; Ciganek, M.; Krcma, F. gas sampling 544 Volatiles in The sampling and analysis of volatile organic compounds in the atmosphere Ambient temperature, unless otherwise indicated. 206
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument atmosphere React. Hudrocarbons Atmos. (1999), 119-157 Boob, Academic, Coden: 67ERAQ Cao, X, Hewitt, C. 851 Toluene diisocyanate Determination of gaseous toluene diisocyanate by use of solid-phase microextraction with on-fibre derivatisation. 65µm DVB/PDMS LC-MS-MS Fresenius' J. Anal. Chem. (2001), 369(6), 524-529 60min. Nilsson, U.; Batlle, R.; Colmsjo, A. dibutylamine derivative 752 VOC, formaldehyde Field air analysis with SPME device Analytica Chimiera Acta 400 (1999) 153-162 varied fibers GC-FID in air Koziel, J., Jia, M., Khaled, A., Noah, J., Pawliszyn, J. Field Sampling and Determination of Formaldehyde in Indoor 1-75 min air samples 753 VOC, formaldehyde Air with SPME and On-Fiber Derivatization 65µm DVB/PDMS GC-FID in air Environ Sci Technol 2001, Vol 35, pg. 1481-1486 10min. Headspace Koziel, J., Noah, J., Pawliszyn, J. PFBHA Derivative 2702 Aromatic VOCs Field analysis of benzene, toluene, ethylbenzene and xylene in water by portable GC-micro-FID combined with headspace SPME 65µm DVB/PDMS GC-FID in water Talanta 69, #4, 894-899 (2006-06-15) Ji, J.; Deng, C. H.; Shen, W. W.; Zhang, X. M. 1min. Headspace sat. salt 755 Aromatic VOCs Design of Validation of Portable SPME devices for rapid field air sampling and diffusion-based calibration 65µm DVB/PDMS GC-FID in Indoor air Anal. Chem. 2001,73(3), 481-486 Augusto, F., Koziel, J., Pawliszyn, J. 30 sec air sampling 759 VOCs Fast field sampling/sample preparation and quantification of volatile organic compounds in indoor air by SPME 65µm DVB/PDMS GC-FID in Indoor air and portable GC Field Analytical Chem. And Tech 4(2-3): 73-84,2000 Jia, M., Koziel, J., Pawliszyn, J. 1min. Headspace 545 Volatile organics Analysis of volatile organic compounds in the ambient air of Algiers by GC with a beta-cyclodextrine capillary column in air J. Chromatogr A, 1999, 846(1+2), 287-293 Yassaa, N., Meklati, B., Cecinato, A. 984 VOC's in air Dynamic versus static sampling for quantitative analysis of VOC's in air. J.Chromatogr. A (2002) 963(1-2), 49-56 Tuduri, L.; Desauziers, V.; Fanlo, J.L. PDMS/carboxen 1062 Volatile organics from steel. Analysis of airborne volatile organic compounds of a steel industry by solid phase microextraction and gas chromatography/mass spectrometry. Bulletin of Environmental Contamination and Toxicology (2003) 70 (5), 957- 963. GC-MS de Lourdes Cardeal, Z.; de Carvalho, C. R.; Parreira, F. V. Solid phase microextraction with analysis by gas chromatography to determine short term hydrogen cyanide concentrations in a field setting. Hydrogen cyanide in 1070 air Journal of Separation Science (2002) 25 (14), 917-921. Smith, P. A.; Sheely, M. V.; Kluchinsky, T. A, Jr. GC-NPD 1114 Development of a quantification method for the analysis of malodorous sulphur compounds in gaseous industrial effluents by solid-phase microextraction and gas chromatography-pulsed flame photometric detection Malodorous sulphur compounds in effluents Journal of Chromatography A (2003) 999 (1-2), 71-80. PDMS/carboxen GC-PFPD Desauziers, Valerie; Fanlo, Jean-Louis; Lestremau, Francois; Roux, Jean- Claude Ambient temperature, unless otherwise indicated. 207
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