SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />
Analyte / Extraction<br />
Matrix Literature Reference Conditions Instrument<br />
Nilsson, T., Ogaard-Madison, J., Montanrilla, L., Larsen, B., headspace<br />
Facchetti, S., Pelusioj, F. stirring<br />
685 MTBE<br />
Determination of MTBE in surface water by use of <strong>SPME</strong><br />
Environ, Sci.Technol. (2000), 34(7), 1359-1364 Carboxen/DVB/PDMS GC-MS<br />
in surface water Achten, C., Puettmann, W.<br />
Sensitive methods for measuring methyl tert-butyl-ether<br />
69 min<br />
25% NaCl, stirred<br />
935 MTBE in water Carboxen/DVB/PDMS GC-MS<br />
in surface water Umwelt-Technol. Aktuell (2000) 12(1), 22-25 69 min<br />
Achten, C., Puettmann, W. 25% NaCl, stirred<br />
686 MTBE, Ethanol, other<br />
Trace Analysis of Ethanol, MTBE, and related Oxygenate<br />
Compounds in Water using <strong>SPME</strong> and GC-MS Carboxen/DVB/PDMS GC-MS<br />
oxygenates in water Anal. Chem. 2000, 72, 4654-4658 25 min immersed<br />
Cassada, D., Zhang, Y., Snow, D., Spalding, R. stirred<br />
Sat. salt,<br />
910 MTBE, TBE, BTEX<br />
High levels of monoaromatic compounds limit the use of<br />
<strong>SPME</strong> of MTBE and Tert butyl alcohol 75µm Carboxen/PDMS Ion trap<br />
in water Environ Sci Technol, 2001, 35 (15) 3190-3192 65µm DVB/PDMS GC-MS<br />
Black, L., Fine, D.<br />
Analysis of Water Samples for Trace Levels of Oxygenated<br />
1-25min.<br />
saturated salt<br />
354 MTBE, EBE, BTEX and Aromatic Compounds Using Headspace <strong>SPME</strong> and 75µm Carboxen/PDMS GC-FID<br />
in water Comprehensive Two-Dimensional Gas Chromatography 40°C, 10 min<br />
J. Microcolumn Separations, 10 (7), 597-604 (1998) headspace<br />
Gaines, R., Ledford, E., Stuart, J. saturated salt<br />
952 MTBE<br />
Measurement of Henry's law constant for MTBE using <strong>SPME</strong><br />
Environ. Toxicol. Chem (2001), 20(8), 1625-1629<br />
in water Bierwagen, B.G.; Keller, A.A.<br />
Role of humic acids in the titanium oxide-photocatalysed<br />
15°-40°C<br />
headspace<br />
581 Tetrachloroethene degradation of tetrachloroethene in water. 100µm PDMS GC-MS<br />
in water Water-Res. Jun 1999; 33(8): 1827-1836<br />
Selli,-E; Baglio,-D; Montanarella,-L; Bidoglio,-G<br />
Using <strong>SPME</strong> with GC to assess trihalomethane content in water<br />
2331 Trihalomethanes Abstracts of Papers Am Chem Society (2004) 227 Part1, U456 GC<br />
in water Rizzuti, Anthony M.; Rogers, Lisa N.<br />
2829 Volatiles in<br />
Simultaneous analysis of 23 priority volatile compounds in water<br />
by <strong>SPME</strong>-GC-MS and estimation of the method's uncertainty 75µm Carboxen GC-MS<br />
in drinking water Int. J. Environ. Anal. Chem. 88, #3, 151-164 (March 2008) headspace<br />
Alpendurada, M.; Carvalho, J.; Goncalves, C.; Guimaraes, A. 15min @ 20°C<br />
Determination of trihalomethanes in drinking water of towns in<br />
2215 Trihalomethane the State of Minas Gerais, Brazil using headspace (HS)/<strong>SPME</strong> headspace GC-ECD<br />
in drinking water high resolution GC-ECD<br />
Ciencia Eng.) 11 #2, 57-62 (2002)<br />
Duarte, M.; Parreira, F; Rabelo De Carvalho, C.<br />
175 Trihalomethanes<br />
Detection and Quantification of Trihalomethanes in<br />
Drinking Water from Alexandria, Egypt<br />
in water Contam. Toxicol. 56: 397-404 (1996)<br />
Hassan, A., Benfenati, E., Fanelli, R.<br />
Analysis of dichlorobenzene in water by <strong>SPME</strong><br />
687 Dichlorobenzene J. Chin. Chem. Soc (2000) 47(2) 415-420 100um PDMS GC-ECD<br />
in water Liu, Y., Ho, W. 30 min<br />
813 Chloroform<br />
Analysis of chloroform in drinking water by<br />
headspace solid-phase microextraction and GC 85µm Polyacrylate GC-FID<br />
in water Fenxi Shiyanshi (2000), 19(5), 65-67 45°C<br />
Liu, Z. L.; Wang, C. H.; Wang, X headspace<br />
Ambient temperature, unless otherwise indicated. 149
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