SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Use of the SPME-GC-MS technique to study the thermal degradation 2822 Thermal of isotactic polypropylene: Effects of temperature and reaction time, heaspace GC-MS byproducts of and analysis of the reaction mechanism polypropylene E-Polymers Jan 30 2008 Bortoluzzi, J.; Carasek, E.; Cristiano, R.; Gallardo, H..; Soldi, V. SPME to concentrate volatile products from thermal 1763 Thermal degradation of polymers 100µm PDMS, GC-MS byproducts of Polym Degradation Stab, 89, #1, 33-37 75µm Carboxen polypropylene Bortoluzzi, J.; Carasek, E; Pinheiro, E.; Soldi, V 2880 Degradation Comparison of extraction methods for sampling of low molecular compounds in polymers degraded during recycling headspace GC products of Eur Polym J 44, #6, 1583-1593 (June 2008) polymers Karlsson, Sigbritt; Moller, Johanna; Stromberg, Emma Emission of possible odourous low molecular weight 1764 Odours from compounds in recycled biofibre/polypropylene composites heaspace GC-MS polypropylene monitored by head-space SPME-GC-MS composites Polym Degradation Stab, 90. #3, 555-562 De Las Heras, Luis A.; Espert, Ana; Karlsson, Sigbritt Development and analytic of odor absorber 1765 Odor Tenside Surfactants Deterg, 41, #6, 282-286 headspace GC removal by Bohmer, Thomas; Muller, Felix; Peggau, Jorg Zn ricinoleate Headspace-SPME-GC-MS identification of volatile organic 1766 Volatiles from compounrds released from expanded polystyrene 75µm Carboxen GC-MS polystyrene J. Polym. Environ., 12, #2, 83-87 headspace Knupp, Gerd; Kusch, Peter Correlation between emitted and total amount of 1767 2-cyclopentyl- 2-cyclopentyl- cyclopentanone in polamide 6.6 headspace GC-MS cyclo- allows rapid assessment by Head Space and HS-SPME . GC-RI pentanone in under non-equilibrium conditions polamide 6.6 J. Chromatogr. A, 1052, #1-2, 151-159 Groning, Mikael; Hakkarainen, Minna Identification and migration of degradation compounds from irradiation 2864 Degradation of multilayer polyamide 6 films for meat foodstuffs and cheese 100µm PDMS GC-MS compounds Anal. Bioanal. Chem. 391, #3, 847-857 (June 2008) 20 min, 80 °C of Polamide 6 Felix, J.S.; Manzoli, J.E.; Monteiro, M.; Nerin, C.; Padula, M.; Pezo, D.; Romero, J. Multiple headspace SPMEof 2-cyclopentyl- cyclopentanone 1768 2-cyclopentyl- in polyamide 6.6: Possibilities and limitations in the headspace GC-MS cyclopentanone headspace analysis of solid hydrogen-bonding matrices in polamide 6.6 J. Chromatogr. A, 1052, #1-2, 61-68 Groning, Mikael; Hakkarainen, Minna Chemical characterization of oil-based asphalt release agents 2308 Volatiles from and their emissions headspace GC/MS Asphalt release Fuel 85 #9, 1232-1241 (2006) agents Isacsson, Ulf; Tang, Bing Determination of aromatic hydrocarbons in asphalt release 1769 Hydrocarbons agents using headspace SPME-GC-MS headspace GC-MS from asphalt J Chromatogra, A, 1069, #2, 235-244 Isacsson, Ulf; Tang, Bing Natural Products 401 Volatiles Analysis of Tobacco Volatiles with SPME Dr. W.D. Koller, Federal Research Centre for Nutrition, 100µm PDMS GC-MS in tobacco Institute of Process Engineering, Engesserstr. 20, 10 min 76131 Karlsruhe/Deutschland headspace 402 Pesticides in A Simple Screening for Pesticide Residues in Tobacco Dr. W.D. Koller, Federal Research Centre for Nutrition, 100µm PDMS GC-MS water/MeOH extract Institute of Process Engineering, Engesserstr. 20, 10 min 76131 Karlsruhe/Deutschland immersion Ambient temperature, unless otherwise indicated. 72
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 102 Flavor additives Qualitative and Quantitative Analysis of Flavor Additives on Tobacco Products Using SPME-GC-MS 65µm Carbowax/DVB GC-FID in tobacco J. Agric. Food Chem. 45: 844-849 (1997) 95°C, 15 min Clark, J., Bunch, J. KCl added 430 Alkaloids Determination of Tobacco Alkaloids Using SPME and GC-NPD Chromatographia (1998), 47(7/8), 443-448 100µm PDMS GC-NPD in tobacco Yang, S., Smetena, I. 12 min, immersed 627 Acetates Quantitative analysis of acetates in cigarette tobacco using SPME-GC-MS GC-MS in cigarette tobacco J. Chromatogr. Sci (2000), 38(4), 137-144 Watson, C., Ashley, D. headspace 2554 Volatile Organics Analysis of volatile organic compounds in mainstream cigarette smoke ENVIRON. SCI. TECHNOL. 41, #4, 1297-1302 (15 FEB 2007) headspace GC-MS found in cigarette smoke Polzin, G. M.; Kosa-Maines, R. E.; Ashley, D. L.; Watson, C. H. Identification and determination of mainstream and sidestream 2434 Organics found in smoke components in different brands and types of cigarettes GC-MS cigarette smoke by means of SPME-GC-MS J. Chromatogr. A 1180, #1-2,138-150 (Feb 8 2008) Bartolucci, G.; Furlanetto, S.; Giannini, I.; Moneti, G.; Orlandini, S.; Pieraccini, G.; Pinzauti, S. 137 Phenols in Quantitative Determination of Phenols in Mainstream Smoke with SPME-GC-Selected Ion Monitoring Mass Spectrometry 85µm polyacrylate GC-FID cigarette smoke J. Chromatogr. Sci. 34: 272-275 (1996) 60 min Clark, J., Bunch, J. stirring 2863 Formaldehyde in Determination of particulate-bound formaldehyde from burning incense by solid phase microextraction 65µm PDMS/DVB GC-ECD incense smoke Bull. Environ. Contam. Toxicol. 80, #4, 324-328 (April 2008) headspace Chen, C.Y.; Lin, J.M.; Liou, S.W.; Yang, T.T. PFBHA derivative 2652 Volatiles in Characterization of incense smoke by SPME - Comprehensive twodimensional (GC x GC) 65µm PDMS/DVB GC-GC-FID incense smoke Atmospheric Env 41, #27, 5756-5768 (SEP 2007) Tran, Tin C.; Marriott, Philip J. headspace 628 Azo dyes Study on determination of prohibited azo dyes by SPME Fenxi Deshi Xuebao (2000), 19(1), 76-78 GC-MS in leather & textiles Xu, H., Tong, H. reduced to aromatic amines w/Na2SO4 Development of a SPME method for detection of the use of Azo dyes banned Azo dyes in coloured tectiles and leather in leather & textiles Rapid Commun.Mass Spectrom. 13, pp1833-1837 Cioni, G., Bartolucci, G., Pieraccini, G., Meloni, S., Moneti, G. 916 Hexachlorobenzene Rapid Quantification of hexachlorbenzene in the color additives D&C Red Nos. 27 & 28 (phloxine B) using SPME GC-MS 100µm PDMS GC-MS in color additives J Chromatogr A (1999) 863(1) 37-46 25min @ 26°C Andrezejewski, D., Weisz, A. Derivatization Solid-Phase Microextraction Gas immersed stirred 210 Solvents in Chromatographic Mass Spectrometric Determination of 65µm Carbowax/DVB GC-FID water-based coatings Organic Acids in Tobacco 5 min J. Chromatogr. Sci. 35 (5): 209-212 (1997) headspace Clark, T., Bunch, J. stirring salt added 836 Biproducts from Screening of biotransformation products of carvone enantiomers by headspace-SPME/GC-MS headspace GC-MS Ambient temperature, unless otherwise indicated. 73
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