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SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />

Analyte / Extraction<br />

Matrix Literature Reference Conditions Instrument<br />

Popp, P., Kalbitz, K., Opperman, G. stirring<br />

74 Diesel fuel<br />

Solid Phase Microextraction-GC for Analysis of Diesel Fuel<br />

Residues in Soil 100µm PDMS GC-FID<br />

in soil Request from Dept. Soil Science, University of Manitoba 55°C, 30 min<br />

Winnipeg, MB, Canada R3T 2N2.<br />

Graham, K., Webster, B., Sarna, L.<br />

headspace<br />

716 THF, methanol<br />

Analysis of THF and methanol in distillation residue<br />

samples by automated headspace <strong>SPME</strong>-GC with FID 65µm PDMS/DVB GC-FID<br />

in distillate J Chromatogr. Sci. (2000), 38(3), 117-121 9min.<br />

Gavlick, W. headspace<br />

870 PAHs in<br />

The use of <strong>SPME</strong> and GC-MS for the chemical characterization<br />

and assessment of PAH pollution in aqueous<br />

environmental environmental samples<br />

samples Int. J. Environ. Anal. Chem (2000) 78(3-4) 205-221<br />

Havenga, Willem J.; Rohwer, Egmont R<br />

717 PAHs<br />

Solid Phase Microextraction of PAHs from soil<br />

Chem. Ana., 2000 (45 No.6) 835-842<br />

in soil Sedukiene, I., Vickackaite, V., Kazlauskas, R.<br />

567 PAHs<br />

Chemical characterization and screening of hydrocarbon<br />

pollution in industrial soils by headspace <strong>SPME</strong> 100µm PDMS GC-MS<br />

in soil J-Chromatogr,-A. 2 Jul 1999; 848(1-2): 279-295 40 min<br />

Havenga,-WJ; Rohwer,-ER headspace<br />

865 PAHs<br />

Solid phase microextraction of PAHs from soil<br />

Chemia Analityczna (Warsaw) (2000) 45(6) 835-842<br />

in soil Seduikiene, I.; Vickackaite, V.; Kazlauskas, R.<br />

Extraction of Pesticides by Solid Phase Microextraction<br />

30min @ 60°C<br />

heaspace<br />

75 Pesticides (from Soil) 100µm PDMS GC-ECD, -NPD<br />

in soil Request from: Dept. Environmental Assessment, Swedish immersed,<br />

University of Agricultural Sciences, PO Box 7050,<br />

Uppsala, Sweden<br />

Bengsson, S., Berglof, T.<br />

water solution<br />

Distribution coefficients of aliphatic alcohols, carbonyl compounds<br />

2336 Alcohols, esters, and esters between air and Carboxen/PDMS fiber coating Carboxen/PDMS GC/MS<br />

carbonyls in air Anal. Chim. Acta. 560 #1-2, 103-109 (2006) air sample<br />

Isidorov, V.; Modzelewska, A.; Purzynska, A.; Serowiecka, M. 15-30°C<br />

2149 Amides in Air<br />

Analysis of amides in the air by sampling with <strong>SPME</strong> and detection<br />

by GC-FID passive air sampling GC-FID<br />

J. Sep. Sci., 29, #3, 346-350 (2006) 65µm PDMS-DVB<br />

de Lourdes Cardeal, Z.; de Souza Bergo, P.; Parreira, F.;<br />

Rabelo de Carvalho, C.<br />

90min @25°C<br />

2718 Triazine<br />

On-fibre <strong>SPME</strong> coupled to conventional HPKC versus in-tube<br />

<strong>SPME</strong> coupled to capillary LC screening analysis of triazines 65µm PDMS-DVB LC<br />

in water in water samples.<br />

J. Chromatogr., A 1125, #2, 159-171 (2006-09-01)<br />

Chafer-Pericas, C.; Herraez-Hernandez, R.; Campins-Falco, P.<br />

855 Triazine, amides<br />

Determination of triazines and amides in water using<br />

solid-phase microextraction coupled with GC-MS. GC-MS<br />

in water Chromatographia (2001) 53(5-6), 306-310<br />

Hu, R.; Elia, D.; Berthion, J. -M.; Poliak, S.<br />

529 Triazines,<br />

Determination of polar pesticides in soil by <strong>SPME</strong> couple to<br />

HPLC-MS 85µm polyacrylate HPLC-MS<br />

carbamates Fresenius'J. Anal. Chem. (1999), 363(7), 680-685 salt added<br />

in soil leachates Moder, M., Popp, P., Eisert, R., Pawliszyn, J.<br />

Ambient temperature, unless otherwise indicated. 196

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