SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Pawliszyn, J. and conditions Applications of Solid Phase Microextraction 731 Reference book Edited by Janusz Pawliszyn RSC Chromatography Monographs 732 Overview Theory of solid phase microextraction J. Chromatogr. Sci. (2000), 38(7), 270-278 Pawliszyn, J. 35 applications described Researchers are giving SPME a second look 733 R&D Magazine, February 1999, 44-45 Sample Preparation and Solid-Phase Extraction 30:50 Carboxen/DVB/PDMS headspace GC-FID 251 Overview LC-GC 15: 1106, 1108, 1110-1113, 1116-1117 (1997) no fibers or Majors, R., Raynie, D. conditions shown 252 Formaldehyde, Recent Advances in Solid Phase Microextraction LC-GC May Supplement, ppS41-S46 (1998) 65µm PDMS/DVB, GC-MS, surfactants in Lord, H., Pawliszyn, J. Carbowax/TPR fiber HPLC-UV air and water varied conditions 2494 VOCs in air and Sample preparation for the analysis of volatile organic compounds in air and water matrices review article water matrices J. Chromatogr. A 1153, #1-2, 130-144 (JUN 15 2007) Demeestere, Kristof; Dewulf, Jo; De Witte, Bavo; Van Langenhove, H. 2495 Review article Sample handling strategies for the determination of persistent trace organic contaminants from biota samples sample handling ANAL. CHIM. ACTA 590, #1, 1-16 (02 MAY 2007) methods Fidalgo-Used, N.; Blanco-Gonzalez, E.; Sanz-Medel, A. 255 Thiophenes Application of SPME/GC-MS to Characterize Metabolites in the Biodesulfurization of Organosulfur Model Compounds 85µm polyacrylate GC-MS in water in Gitumen 20 min Environ. Sci. Technol. 32 (3): 421-426 (1998) immersion MacPherson, T., et al. pH 2 Construction of an Interface for SPME-PC-SFC 256 J. High Resolut. Chromatogr. 34 (10): 275-277 (1997) Medvedovici, A., Sandar, P. Automated In-Tube SPME Coupled to HPLC 257 Phenylurea pesticides Anal. Chem., Vol. 69, No. 16, August 15, 1997, 3140-3147 Omegawax 250 HPLC-UV, in water Eisert, R., Pawliszyn, J. 25µL, 10 flush cycles 245nm 258 PAHs Effect of Heating the Interface on Chromatographic Performance of SPME Coupled to HPLC 100µm PDMS HPLC-UV, in water Anal. Commun. 34 (11): 365-369 (1997) 60 min 254nm Daimon, H., Pawliszyn, J. Effect of Heating the Interface on Chromatographic immersion heat desorb 22-180°C 259 PAHs Performance of SPME Coupled to HPLC 100µm PDMS HPLC-UV, in water Analyst (Cambridge) 122 (11): 365-369 (1997) 60 min 254nm Daimon, H., Pawliszyn, J. immersion heat desorb 22-180°C Development of an improved heated interface for coupling SPME to 2181 Heated interface high-performance liquid chromatography for HPLC J. Chromatogr. A, 1105, #1-2, 208-212 (2006) Alves, C.; Contadori, A..; Fernandes, C.; Lancas, F.; Neto, A. Santos; R., Jose C. SPME Combined with HPLC for the Determination of Metal Ions Ambient temperature, unless otherwise indicated. 218
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 260 Hg (II) ion Using Crown Ether as Selective Extracting Reagent polypropylene hallow HPLC-UV, in water J. Microcolumn Sep. 167-173 (1998) fiber, 30 min 254nm Jia, C., Luo, Y., Pawliszyn, J. immersion derivative: dibenzo-18-crown-6 734 Dopamine in Analysis of biogenic amines by SPME and HPLC with electrochemical detection Carbowax-TPR HPLC biological matrix J. Chromatogr. A, (2000) 873, 396 Auger, J., Boulay, R., Jaillais, B., Delion-Vancassel, S. electrochem 368 Aromatic amines SPME Coupled with HPLC for the Determination of Aromatic Amines 50µm Carbowax/TPR, HPLC-UV, in wastewater Anal. Chem., Vol. 71, No. 2, January 15, 1999, 310-316 65µm PDMS/DVB, 280nm Wu, Y., Huang, S. 30 min or 20 min Na2SO4 buffer added Automated In-Tube SPME Coupled to HPLC 407 Phenylurea pesticides Anal. Chem., Vol. 69, No. 16, August 15, 1997, 3141-3147 Omegawax 250 UV, 245nm in water Eisert, R., Pawliszyn, J. 25uL, 10 flush cycles 2695 Pesticides in Headspace SPME in pesticide residues analysis: 2. Apple samples. Pesticidi i Fitomedicina 22, #2, 173-176 (2007) 100µm PDMS GC-MS apple samples Durovic, R.; Milinovic, J.; Markovic, M.; Markovic, D. 60 min @ 60°C headspace 2177 Carbamate Behaviour of carbamate pesticides in GC and their determination with SPE and SPME as preconcentration steps 85µm polyacrylate GC-MS pesticides J SepSci. 28, #16, 2130-2138 (2005) Carabias-Martinez, R.; Garcia-Hermida, C.; Rodriguez-Gonzalez, E.; Ruano-Miguel, Luis 735 Carbamate Automated in-tube SPME-HPLC for Carbamate pesticide analysis Intube capillaries HPLC pesticides J. Chromatogr. A, (2000) 873(1), 137-147 in water Gou, Y, Eisert, R., Pawliszyn, J. 736 Carbamate In-tube SPME coupled to capillary LC for Carbamate analysis in water samples Intube capillaries HPLC pesticides Anal. Chem. 2000, 72(13), 2774-2779 in water Gou, Y., Pawliszyn, J. 737 Carbamate On-line coupling of in-tube SPME to HPLC for analysis of carbamates in water samples: comparison of Intube capillaries HPLC pesticides two commercially available autosampler in water J. Microcolumn Sep. (2000), 12(3), 125-134 Gou, Y., Tragas, C., Lord, H., Pawliszyn, J. 789 Development of effective sample pretreatment by in-tube SPME and its application Chromatography (2000) 21(4), 276-279 Kataoka, Hiroyuki; Wu, Jingcun; Lord, Heather L.; Pawliszyn, J. Intube capillaries Sample preparation technique using fiber-in-tube SPME 810 Chromatography (2000), 21(4), 284-285 Jinno, K; Kawazoe, M; Saito, Y; Hayashida, M 571 175 references On-line combination of aqueous-sample preparation and capillary gas chromatography various references of review J-Chromatogr,-A. 21 May 1999; 842(1-2): 391-426 Louter,-AJH; Vreuls,-RJJ; Brinkman,-UAT SPME & SPE 552 Solid phase microextraction turned inside out Che. Aust. 1999, 66(6), 9-11 Tan, D., Marriott, P., Lee,H., Morrison, P. Intube capillaries Ambient temperature, unless otherwise indicated. 219
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