SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Bensoam, J., Cicolella, A., Durjardin, R. immersed 516 Amines/alcohols Evaluation of SPME for the anlaysis of hydophilic compounds 75µm Carboxen/PDMS in water J. Exposure Anal.Environ. Epidemiol. 1999, 9(3) 181-191 Shoemaker, J. Munch, J., Behmer, T. 517 Polar volatiles SPME of volatile polar compounds in water J. High Resolut. Chromatogr. (1999), 22(2), 109-115 85µm polyacrylate GC-MS in water Matisova, E, Sedlakova, J., Slezackova, M., Welsch, T. On-Site Sampling for Volatiles and Pesticides, Using SPME 50°C headspace 290 VOCs, pesticides Amer. Environ. Lab. 10 (2): 21-22 (1998) 100µm PDMS, GC-MS in water and air Shirey, R., Mani, V, Mindrup, R. 75µm Carboxen/PDMS 2-3 min, headspace stirring, salt added 291 Petroleum Solvent-Free and Rapid Determination of Petroleum Hydrocarbons in Water by SPME hydrocarbons UFZ-Ber. Optimierung Umweltvertiraeglicher in water Analysenverfahren fuer Mineraloelkohlenwasserstoff IM Boden 12: 14-17 (1997) Christall, B. Partition Infrared Method for Total Gasoline Range Organics 367 C3-C16 hydrocarbons in Water Based on SPME 130µm Teflon film IR 4000-2690 in water Environ. Sci. Technol, 1999, 33, 814-819 30 min cm-1 Stahl, D., Tilotta, D. immersion 518 MMT in Determination of methylcyclopentadienylmanganese tricarbonyl (MMT) in aqueous samples by SPME-GC-AED 100µm PDMS GC-AED water Analyst (Cambridge, UK), (1999), 124(1), 71-73 15 min @ 20°C Yang, F., Chau, Y. headspace SPME combined with GC-AED for the determination of cyclopentadienyl- 2665 MMT in manganese tricarbonyl and (methylcyclopentadienyl)manganese headspace GC-AED water tricarbonyl in soils and seawaters J. Chromatogr. A 1173, #1-2, 139-145 (Nov 30 2007) Campillo, N.; Hernandez-Cordoba, Manuel; Penalver, Rosa 849 MMT in Determination of methylcyclopentadienylmanganesel tricarbonyl by SPME-direct thermal desorption-quartz GC-AED water furnace atomic absorption spectrometry Spectrochim. Acta, Part B (2001) 56B(2) 215-222 Fragueiro, M. S.; Alava-Moreno, F.; Lavilla, I.; Bendicho, C Uncertainty associated to the analysis of organochlorine pesticides in 2706 Organochlorine water by SPME-GC-ECD-Evaluation using two different approaches headspace GC-ECD pesticides in Analytica Chimica Acta; Vol. 573-574, 202-208 (2006-07-28) water Ratola, Nuno Analytical methods for PCBs and organochlorine pesticides in 2852 Review article environmental monitoring and surveillance: A critical appraisal Anal. Bioanal. Chem. 386, #4, 769-789 (October 2006) Muir, Derek; Sverko, Ed 2409 Pesticides, PCBs Simultaneous analysis of PCBs and organochlorine pesticides in water by headspace SPME with GC-MS 100µm PDMS GC-ECD from water J. Chromatogr., A 1138, #1-2, 231-243 (2007-01-05) Derouiche, A.; Driss, M. R.; Morizur, J. -P.; Taphanel, M. -H. headspace 519 VOCs, BTEX, Efficiency of direct SPME from water: Comparison of different fiber types including a new C8-coating variety of fibers Ambient temperature, unless otherwise indicated. 158
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument pesticides, PCBs Chromatographia, 1999, 49(11/12), 686-690 from water Popp, P., Paschke, A. 904 pesticides Analysis of fire ant pesticides in water by SPME and GC-MS and LC-MS GC-MS & in water Analytica Chimica Acta 2001, 436(1) 11-20 Reyzer, M., Brodbelt, J. LC-MS Optimisation and validation of a SPME method for simultaneous 2413 Pesticides determination of different types of pesticides in water by GC-MS 60µm PDMS/DVB GC-MS in water J. Chromatogr., A 1141, #2, 165-173 (2007-02-09) Beceiro-Gonzalez, E. ; Concha-Grana, E.; Guimares, A.; Goncalves, C.; Muniategui-Lorenzo, S.; Alpendurada, M. 45 min @ 60°C 770 Chlorine, nitrogen Multiresidual method for determination of chlorine, nitrogen, and phosphorus containing pesticides in surface GC/ECD/NPD phosphorus and drinking water by SPME and GC/ECD/NPD pesticides Boll. Chim. Ig., Parte Sci. (2000) 51(S3), 99-103 in water de Luca, Giuseppe; Mura, Michele (in Italian) 512 Iodinated THMs SPME for the determination of iodinated trihalomethanes in drinking water 65µm CW/DVB/PDMS GC-ECD in drinking water J. Chromatogr., A (1999), 841(2), 197-206 10 min @ 20°C Cancho, B., Ventura, G., Galceran, M. NaCl used 292 Iodinated organics Solid Phase Microextraction and Analysis of Iodinated Organic Compounds 85µm polyacrylate GC-ECD in water Avail. UMI, Order No. DA9812871 from: Diss. Abstr. Int., B 58 (10): 5364 (1998) Frazey, P. 288 Iodinated volatiles SPME with Temperature-Programmed Desorption for the Analysis of Iodinated Disinfection Byproducts 85µm polyacrylate GC-ECD in water Anal. Chem. 70 (3): 638-644 (1998) 15 min Frazey, P., Barkley, R., Siever, R. Simultaneous determination of cyanogen chloride and immersion stirring 694 Cyanogen chloride cyanogen bromide in treated water at sub-ug/L levels by a Carboxen/DVB/PDMS GC-ECD in water new SPME-GC-ECD method 15 min, headspace J. Chromatogr. A 897(2000) 307-315 Cancho, B., Ventura, F., Galceran, M. 2-3pH, 25% salt added Determination of acetic acid in aqueous samples, by 695 Acetic acid water-phase derivatization, SPME, and GC 85µm Polyacrylate GC-FID in water J. Chromatogr. A., (2000), 874(2), 225-234 headspace Wittmann, G., Van Langenhove, H., Dewulf, J. benzenal bromide derv. Determinationof Chlorinated Acetic Acids in Drinking 411 Chloroacetic acids Water by in-situ Derivatization-SPME in water Interri J. Environ. Anal. Chem. 66: 215-224 (1997) Aikawa, B., Burk, R. SPME coupled with GC-ion trap mass spectrometry for the 520 Haloacetic acids analysis of haloacetic acids in water GC-Iontrap in water J. Chromatogr., A 1999, 859(2), 159-172 MS Sarridon, M., Santos, F., Galceran, M. 696 Haloacetic acids In situ derivatization/SPME for the determination of haloacetic acids in water Carboxen/PDMS GC-ITMS in water Anal. Chem. 2000 Oct. 15, 72(20), 4865-4873 Sarrion, M. Santos, F., Galceran, M. Using SPME to Determine Partition Coefficients to Humic Acids headspace dimethyl sulfate derv. 353 Chlorobenzenes and Bioavailable Concentrations of Hydrophobic Chemicals 7µm PDMS GC-FID in water Environ.Sci Technol, 1998, 32, 3430-3435 20 min Ramos, E., Meijer, S., Vaes, W., Verhaar, H., Hermens, J. SPME-capillary GC determination of chlorobenzene immersion pH 7 Ambient temperature, unless otherwise indicated. 159
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SPME Literature Literature No. Titl
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