SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument essential oils Lopez, P.; Sanchez, C.; Batlle, R.; Nerin, C. Determination of microbial volatile organic compounds from 2217 Volatile organics Staphylococcus pasteuri against Tuber borchii using SPME-GC-MS GC-MS in bacteria Rapid Communications Mass Spectrometry 19 #22, 3411-3415 (2005) Barbieri, E.; Gioacchini, A. M.; Zambonelli, A.; Bertini, L.; Stocchi, V. 2372 poly(3-hydroxy Use of headspace solid-phase microextraction for the quantification of poly(3-hydroxybutyrate) in microbial cells headspace GC-FID -butyrate) J. Chromatogr., A 1154, #1-2, 34-41 (2007-06-22) in microbial cells Monteil-Rivera, F.; Betancourt, A.; van Tra, H.; Yezza, A.; Hawari, J 811 Volatile hydrocarbon Development of a method for the application of SPME to monitor biodegradation of volatile hydrocarbons GC-FID from bacterial during bacterial growth on crude oil 45min @ 30°C growth J Indus Microb & Biotech (2000) 25(3), 155-162 Van Hamme, J. D.; Ward, O headspace Solid-phase microextraction of volatile compounds from the chopped leaves of three species of Eucalyptus. Volatile compounds 1054 from Eucalyptus. Journal of Agricultural and Food Chemistry (2003) 51 (9), 2679-2686. Pawliszyn, Janusz; Caramao, Elina B.; Christensen, Eva; Zanin, Kelen D.; Zini, Claudia A. Sampling and sample preparation for analysis of aromas and fragrances. 1082 Aromas and fragrances Trends in Analytical Chemistry (2003) 22 (3), 160-169. Augusto, Fabio; Leite e Lopes, Alexandre; Zini, Claudia Alcaraz Localization and speciation of selenium and mercury in Brassica 2169 Selenium, mercury juncea - Implications for Se-Hg antagonism headspace GC-ICP-MS in plants J Anal At Spectrom 21, #4, 404-412 (2006) GC-TOFMS Caruso, J.; Meija, J.; Mounicou, S.; Shah, M.; Shann, J.; Vonderheide,A. Simultaneous monitoring of volatile selenium and sulfur species from Se accumulating plants (wild type and genetically modified) by gas chromatography mass spectrometry and gas chromatography-inductively coupled plasma mass spectrometry using solid-phase microextraction for sample introduction. Selenium and sulfur 1092 from plants. Analytical Chemistry (2002) 74 (22), 5837-5844. Meija, J.; Montes-Bayon, M.; Le Duc, D. L.; Terry, N.; Caruso, J. A.* GC-ICP MS Use of solid-phase micro-extraction as a sampling technique in the determination of volatiles emitted by flowers, isolated flower parts and pollen 1120 Volatiles from flowers Journal of Chromatography A (2003) 1000 (1-2), 229-233. Cioni, Pier Luigi; Flamini, Guido; Morelli, Ivano 2598 Volatile organics Enantiomeric purity of (+/-)-methyl jasmonate in fresh leaf samples and commercial fragrances headspace GC/MS. from Jasminum J. Sep. Sci.30, #13, 2117-2122 (August 2007) leaves Blanch, Gracia P.; Ruiz del Castillo, Maria Luisa Composition and antimicrobial activity of Anemopsis 2220 Volatiles californica leaf oil GC from califonica leaf J Ag Food Chem, 53, #22, 8694-8698 (2005) Medina, A.; Lucero, M.; Holguin, F.; Estell, R.; Posakony, J.; Simon,J.; O'Connell, M The composition of dalea formosa oil determined by steam 2228 Volatile organics distillation and SPME 100um PDMS GC-FID and in dalea J. Essent. Oil Res. 17 #6, 645-647 (2005) GC/MS. formosa oil Estell, Rick E.; Lucero, Mary E.; Sedillo, Ruth L. Identification and quantification of methyl jasmonate in leaf volatiles of Arabidopsis thaliana using solid-phase microextraction in combination with gas chromatography and mass spectrometry. Ambient temperature, unless otherwise indicated. 80
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1121 Methyl jasmonate Phytochemical Analysis (2003) 14 (3), 155-159. Dubery, Ian A.; Meyer, Riaan; Rautenbach, George F. GC-MS Identification of sulcatol, a potential pheromone of the ambrosia beetle Gnathotrichus materiarius (Col., Scolytidae). 1139 Sulcatol from beetles Journal of Applied Entomology (2003) 127 (4), 189-194. Flechtmann, C. A. H.; Berisford, C. W. 1165 Mercury and tin Elevated lead levels: A possible factor behind the forest die back of Montane forests in Sri Lanka? Journal De Physique. IV : JP (2003) 107 (II), 1439. Dissanayake, C.B.; Ranasinghe, P.N. PDMS GC-MIP/AES 2902 Methanol from Determination of methanol in biodiesel by headspace SPME Bioresour. Technol. 99, #13, 5901-5905 (September 2008) 75µm Carboxen GC-FID 1170 biodiesel Alley, E.; Armbrust, K.; French, W.; Hernandez, R.; Paraschivescu, M. headspace Ethanol from wood pulp Determination of methanol released from wood and mechanical pulp by headspace solid-phase microextraction J Pulp Pap Sci (2002) 28(6), 199-203 Eckerman, C.; Holmbom, B.; Pranovich, A.V. 2377 Chlorophenols in Focused microwave-assisted micellar extraction combined with SPME-GC-MS to determine chlorophenols in wood samples GC-MS wood samples Anal. Chim. Acta 582,#1, 10-18 (2007-01-16) Pino, V.; Ayala, J. H.; Gonzalez, V.; Afonso, A. M. 2504 Pentachlorophenol Removal of 2,4-dichlorophenol and pentachlorophenol from waters by sorption using coal fly ash from a Portuguese thermal power plant 2,4-dichlorophenol J Hazardous Materials 143, #1-2, 535-540 (MAY 8 2007) in water Estevinho, B.; Martins, Isabel; Ratola, Nuno; Alves, Arminda; Santos, L. GC-ECD Development of a SPME method for direct determination of 2264 Pentachlorophenol pentachlorophenol in paper and board samples: Comparison with PDMS & PA GC-ECD in paper samples conventional extraction method J. Chromatogr. A, 1095 #1-2, 8-15 (2005) Domeno, C.; Munizza, G.; Nerin, C. 2661 Pentachlorophenol Development of a SPME-GC-MS method for the determination of pentachlorophenol in human plasma using experimental design. headspace GC-MS in plasma Chemosphere 70, #2, 256-62 (2007 Dec) Zhou, Ying; Jiang, Qingwu; Peng, Qian; Xuan, Dongliang; Qu, Weidong acetylation 2604 Volatiles from The composition of volatiles from tatami mats containing hinoki (Chamaecyparis obtusa) wood-wool and its decline over the long term headspace GC tatami mats J. Wood Sci. 53, #6, 529-532 (December 2007) Hiramatsu, Y.; Imai, Y.; Matsui, N.; Miyazaki, Y.; Ohira, T. 1171 Volatiles in wood On-line wood species sensor Process Control News Pulp Paper Industry (2002) 22(1), 10-11 Fuhr, B.; Henry, D.; Sedgwick, G.; Smith, G.; Woolley, J. GC Reevaluation of the chemical secretion of the sternal glands of Polistes social wasps (Hymenoptera Vespidae). 1173 Ethology Ecology & Evolution (2003) 15 (1), 73-82. Dani, F. R.; Jones, G. R.; Morgan, E. D.; Turillazzi, S. 1181 Characterization of Citrus unshiu ( C. unshiu Marcov. forma Miyagawa-wase ) blossom aroma by solid-phase microextraction in conjunction with an electronic nose. Journal of Agricultural and Food Chemistry (2003) 51 (2), 418-423. Choi, H. S. GC-MS Ambient temperature, unless otherwise indicated. 81
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