SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Zhang, W. Y.; Wang, C. Y.; Yang, Z. J. SPME coupled with HPLC w/ fluorimetric detection 1994 Bisphenol in for the determination of bisphenol A, 4-n-nonylphenol and 50µm CW-TPR HPLC-Fluorimetric water 4-t-octylphenol in environmental water samples. Analytical Letters, 37, #4, 739-753 Cai, Y. Q.; Jiang, G. B.*; Liu, J. F.; Liang, X.; Yao, Z. W.; Liu, J. M.; Liu, J. Y.; Zhou, Q. X. Electronic nose technology for the detection of microbial 1995 Volatiles from and chemical contamination of potable water headspace @ 25°C GC Bacteria Sens Actuators, B Chem, 106, #1, 3-6 in water Canhoto, O.; Magan, N. On-fibre silylation following SPME for the determination of 1996 Herbicides acidic herbicides in water samples by GC 85µm polyacrylate GC-MS in water Anal. Chim. Acta, 537, #1-2, 259-266 MTBSTFA derivative Cela, R.; Gonzalez, R.; Quintana, J.; Rodriguez, I.; Rubi, E. stirred Analysis of the chloroacetanilide herbicides in water using 1997 Herbicides SPME with CAR/PDMS and GC/ECD 75µm Carboxen GC-ECD in water J of AOAC Intl, 88, #4, 1236-1241 immersed sampling Hwanc, Ying-Ming; Wong, Yih-Gang; Ho, Wu-Hsiung Sonochemical degradation of triclosan in water and wastewater 2790 Triclosan in Ultrason. Sonochem.15, #5, 689-694 (July 2008) GC-ECD water Barro, R.; Garcia-Jares, C.; Kalogerakis, N.; Llompart, M.; Lores, M.; GC-MS Mantzavinos, D.; Petrakis, C.; Psillakis, E.; Sanchez-Prado, L. 2171 Triclosan in Further research on the photo-SPME of triclosan Anal. Bioanal. Chem.384, #7-8, 1548-1557 (2006) PDMS fiber GC-MS water Cela, R.; Fernandez-Alvarez, M.; Garcia-Jares, C.; Llompart, M.; Lores,Marta; Sanchez-Prado, L. Optimization of SPMEconditions for the determination of 1998 Triclosan in triclosan and possible related compounds in water samples 85µm polyacrylate GC-MS water J Chromatogr A, 1072, #1, 107-115 MTBSTFA derivative Canosa, P.; Rodriguez, I.; Rubi, E.; Cela, R. 30min extraction immersed sampling Application of strategic sample composition to the screening 1999 Anti- of anti-inflammatory drugs in water samples using SPME 85µm polyacrylate GC-MS inflamatory Anal. Chim. Acta, 524, #1-2, 63-71 silylated esterfication drugs in Carpinteiro, J.; Carro, A.; Cela, R.; Lorenzo, R.; headspace water Martinez, E.; Quintana, J.; Rodriguez, I. Determination of anti-inflammatory drugs in water samples, by in situ 2793 Anti-inflamatory derivatization, SPME-GC-MS 100µm PDMS GC-MS drugs in Talanta 75, #1, 111-115 (MAR 15 2008) headspace water Araujo, L.; Wild, J.; Villa, N.; Camargo, N.; Cubillan, D.; Prieto, A. dimethyl sulphate, derivatives Recently developed GC/MS and LC/MS methods for determining 2499 Anti-inflamatory NSAIDs in water samples LC-MS drugs in Anal Bioanal Chemistry 387, #4, 1203-1214 (FEB 2007) derivatives GC-MS water Farre, M.; Petrovic, M.; Barcelo, D. A combination of statistical and analytical evaluation methods as 2784 Phamaceutical a new optimization strategy for the quantification of pharmaceutical GC-MS-MS resideu in sewage residues in sewage effluent 2.5-7 pH effluent Anal. Chim. Acta, 613, #2, 169-176 (Apr 21 2008) Budziak, D.; Carasek, E.; Costa, L..; Martendal, E.; Suchara, E. Applicability of SPME followed by on-fiber silylation for the 2000 Estrogens in determination of estrogens in water samples by GC-MS-MS 85µm polyacrylate GC-MS-MS sewage J Chromatogr A, 1056, #1-2, 179-185 MSTFA derivatives water Carpinteiro, J.; Carro, A.; Cela, R.; Lorenzo, R.A.; immersed sampling Quintana, J.; Rodriguez, I. Determination of odorous mixed chloro-bromoanisoles in 2001 Chloro-brom- water by SPME-GC-MS headspace GC-MS anisole in J Chromatogr A, 1064, #1-2, 97-106 100µm PDMS water Diaz, A.; Ventura, F.; Galceran, M. Estimation of measurement uncertainty for the Ambient temperature, unless otherwise indicated. 176
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 2002 Nonylphenol determination of nonylphenol in water GC-MS in water using SPME and SPME procedures. Analytica Chimica Acta, 506, #1, 71-80 Diaz, A.; Vazquez, L.; Ventura, F.; Galceran, M. Predicting organic contaminant concentrations in sediment porewater 2523 Organics in using solid-phase microextraction sediment Chemosphere 66, #8, 1408-1414 (JAN 2007) Yang, Ze-Yu; Zeng, Eddy Y.; Maruya, Keith A.; Mai, Bi-Xian; Ran, Yong Validation, using a chemometric approach, of GC- 2003 Organotin inductively coupled plasma-atomic emission GC-ICP-AES in water and spectrometry (GC-ICP-AES) for organotin determination sediment Anal. Bioanal. Chem., 376, #2, 226-235 Aguerre, S.; Lespes, G.; Pecheyran, C. Development of a novel SPME element for 2004 Bethrodine thermal desorption GC analysis 30µm PDMS GC-MS herbicide in J. Chromatogr. A, 1035, #2, 277-279 water Hosaka, A.; Ohtani, H.; Tsuge, S.; Wang, L.; Watanabe, C. Application of SPME for the determination of soil fumigants 2005 Fumigants in water and soil samples soil headspace or GC/ECD/NPD in soil/water Journal of Separation Science, 28, #1, 98-103 immersed in water Fuster, S.; Beltran, J.; Lopez, F. J.; Hernandez, F. Impurity analysis of 1,4-dioxane in nonionic surfactants and 2006 Surfactants cosmetics using headspace SPME coupled w/GC & GC-MS headspace GC, GC-MS in water J. Chromatogr. A, 1071, #1-2, 141-145 Fuh, C. Bor; Lai, M.; Tsai, H. Y.; Chang, C. M. Rapid screening for trace nonyl-phenyl 2007 Surfactants polyethylene glycol ether in water by SPME 14 hour SALDI-MS in water combining with laser desorption ionization MS polycrystaline Proc. 50th ASMS Conf. Mass Spectrom. Allied Top. graphite coated fiber 2002, p597-599 Chen, Yu-Chie; Sun, Mei-Chuan Analysis of methylamine by SPME and HPLC after 2008 Methylamine on-fiber derivatization with 9-fluorenylmethyl chloroformate 9-fluorenylmethyl HPLC in water Anal. Chim. Acta, 513, #2, 425-433 chloroformate Campins-Falco, P.; Chafer-Pericas, C.; Herraez-Hernandez, R derivative immersion sampling A new selective method for dimethylamine in water analysis 2009 Methylamine by LC using SPME and two-stage derivatization with 50µm CW-TPR HPLC in water o-phthalaldialdehyde and 9-fluorenylmethyl chloroformate 9-fluorenylmethyl Talanta, 66, #5, 1139-1145 chloroformate Chafer-Pericas, C; Herraez-Hernandez, R.; Campins-Falco, P derivative immersion sampling Determining leaching of bisphenol A from plastic 2010 Bisphenol A containers by SPME-GC-MS 85µm polyacrylate GC-MS from water Anal. Chim. Acta, 539, #1-2, 41-47 50min @ 65°C Chang, Chia-Min; Chou, Chi-Chi; Lee, Maw-Rong BSTFA derivative headspace Determination of trace bisphenol-A in leachate by 2011 Bisphenol A SPME coupled with HPLC HPLC-UV from water Fenxi Kexue Xuebao, 20, #5, 461-464 Deng, L.; Zhang, W. H.; Feng, X. H.; Deng, N. S.* Fibre selection based on an overall analytical feature comparison for the 2426 Trihalomethanes solid-phase microextraction of trihalomethanes from drinking water 65µm PDMS-DVB GC-MS in drinking water J. Chromatogr., A 1139, #1, 27-35 (2007-01-12) headspace San Juan, P. M.; Carrillo, J. D.; Tena, M. T. 40°C, 0.36 g mL salt Novel analytical methods for the determination of fuel oxygenates 2857 Fuel oxygenates in water review article in water HANDBOOK OF ENVIRONMENTAL CHEMISTRY pp1-30 (2007) Jochmann, Maik A.; Schmidt, Torsten C. Measurement of fuel oxygenates in tap water using SPME-GC-MS 2758 Fuel oxygenates J Chrom Sci, 46, #5, 381-387 (MAY-JUN 2008) headspace GC-MS in tap water Cardinali, Frederick L.; Blount, Benjamin C.; Schmidt, Rachael; Morrow, J. 2012 THM & TBE Measurement of trihalomethanes and methyl tertiary-butyl ether in tap water using SPME-GC-MS. headspace GC-MS Ambient temperature, unless otherwise indicated. 177
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