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SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />

Analyte / Extraction<br />

Matrix Literature Reference Conditions Instrument<br />

Usobiaga, Aresatz; Zuloaga, Olatz NaBEtr derivative<br />

2244 Organotin in<br />

Organotin speciation in Bizerte lagoon (Tunisia)<br />

Science of the Total Environment 349, #1-3, 211-222 (2005) headspace GC-PFPD<br />

marine sediments Mzoughi, N.; Lespes, G.; Bravo, M.; Dachraoui, M.; Potin-Gautier, M.<br />

Preconcentration and Determination of Sn- and Pb-Organic<br />

NaEt4B<br />

derivatives<br />

153 Organo Sn, Pb Species in Environmental Samples by <strong>SPME</strong> and GC-AED GC-AED<br />

in water Fresenius’ J. Anal. Chem. 354: 587-91 (1996)<br />

Tutschiku, S., Mothes, S., Wennrich, R.<br />

Determination of Organotin Compounds in Water Samples<br />

215 Organotin by Solid-Phase Microextraction (<strong>SPME</strong>) and GC-MS GC-MS<br />

in water Ann. Chim. (Rome) 87: 497-504 (1997)<br />

Guidotti, M., Vitali, M.<br />

152 Methyltin<br />

Rapid Determination of Methyltin Compounds in Aqueous<br />

Samples Using <strong>SPME</strong> and Capillary GC Followed by 100µm PDMS GC-FPD<br />

in water in situ Derivatization with Sodium Tetraethylborate 29°C, 2-35 min<br />

J. High Res. Chromatogr. 18: 767 (1995) headspace<br />

Morcillo, Y., Cai, Y., Bayona, J.<br />

Determination of Tetraethyllead and Inorganic Lead in Water<br />

stirring<br />

NaBEtr derivative<br />

161 Lead derivatives by <strong>SPME</strong>-GC 100µm PDMS GC-MS<br />

in water Anal. Chem. 68: 3008 (1996) 10 min<br />

Gorecki, T., Pawliszyn, J. headspace<br />

683 Lead derivatives<br />

Determination of Tetraethyllead by <strong>SPME</strong>-thermal desorption<br />

quartz furnace atomic absorption spectrometry AA<br />

in water J. Anal. At. Spectrom. 2000, 15(16), 705-709<br />

Sandra Fraguairo, M, AlavapMoreno, F., Isela, B.<br />

10 min, headspace<br />

Rapid Determination of Butyl, Phenyl and Cyclohexyl Tin<br />

23 Organotin compounds Compounds in Aqueous Samples Using <strong>SPME</strong> and 100µm PDMS GC-FPD<br />

in water Capillary Gas Chromatography Following in situ Derivatization 30 min<br />

with Sodium Tetraethylborate immersion<br />

CID-CSIC Jordi Girona, 18-26, E-8034, Barcelona, Spain stirring<br />

Morcillo, Y., Cai, Y., Porte, C., Bayona, J. NaBEt4 derivative<br />

503 Organo-tin, -lead,<br />

Determination of organometallic compounds in surface<br />

water and sediment samples with <strong>SPME</strong>-CGC-ICPMS 100µm PDMS GC-ICPMS<br />

-mercury Mikrochim. Acta (1999), 130(4), 241-251 10 min<br />

in water De Smaele, T., Moens, L., Sandra, P., Dams, R. headspace<br />

235 Rare earth elements<br />

Separation of Cerium from Other Rare-Earth Elements with<br />

Application to Samarium-Neodymium and Lanthanum-<br />

Cerium Chronometry<br />

Nucl. Instrum. Methods Phys.Res.Sect.B 117: 201-208 (1996)<br />

Rehkaemper, M., Gaertner, M., Galer, S., Goldstein, S.<br />

2742 Selenite and<br />

Comparison of two derivatizing agents for the simultaneous.<br />

determination of selenite and organoselenium species immersed vs GC-MS<br />

organoselenium by GC and atomic emission . headspace (20min)<br />

J. Chromatogr. A 1165, #1-2, 191-199 (Sep 21 2007) piazselenol<br />

Campillo, N.; Penalver, R.; Hernandez-Cordoba, M.; Perez-Sirvent, C.;<br />

Martinez-Sanchez, M. -J.<br />

derivative<br />

580 Selenite, selenate<br />

Selective determination of selenite and selenate using<br />

<strong>SPME</strong> and GC-MS GC-MS<br />

in water J-High-Resolut-Chromatogr. Jul 1999; 22(7): 414-416 35 min, agitation<br />

Guidotti,-M; Ravaioli,-G; Vitali,-M<br />

Compound-specific nitrogen and carbon isotope analysis of<br />

piazselenol derivative<br />

immersed<br />

2752 Nitroaromatics nitroaromatic compounds in aqueous samples using <strong>SPME</strong>-GC/IRMS GC/IRMS<br />

in water ANAL. CHEM. 79, #6, 2386-2393 (15 MAR 2007)<br />

Berg, M.; Bolotin, J.; Hofstetter, T. B.<br />

Ambient temperature, unless otherwise indicated. 147

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