SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Namera, A., Yashiki, M., Kojima, T., Fukunaga, N. and conditions 337 Acylcarnitines Determination of Urinary Acylcarnitines by ESI-MS Coupled with SPME ESI-MS in urine J. Mass Spectrom. 32 (11): 1195-1204 (1997) Mioder, M., Loster, H., Hraschuh, R., Popp, R. 499 Methylxanthines Extraction of methylxanthines from human body fluids by SPME 65µm Carbowax/DVB GC-NPD in blood/urine Anal. Chim. Acta., 1999, 387(1), 53-60 1 hr @ 40°C Kumazawa, T., Seno, H., Lee, X., Ishii, A. 1ml of 1M HCl04 414 Organic acid esters Urinary Organic Acid Screening by SPME of the Methyl Esters J. Chromatogr. B: Biomed Sci. Appl. (1998), 713(2), 427-432 85µm polyacrylate GC-FID, -MS in urine Liebich, H., Gesele, E., Woll, J. Validation of negligible depletion SPME as a tool to 20 min immersion w/stirring trimethyloxonium tetrafluoroborate 667 Semivolatile determine tissue/blood partition coefficient for semivolatiles in tissue/blood and nonvolatile organic chemicals Toxicol. Appl. Pharmacol. (2000), 166(2), 138-144 Garicano, E., Vaes, W., Hermens, J. 415 New Mass Spectrometric Methods for the Fast Analysis of Biomedical-Relevant Substances CLB Chem. Labor Biotech. (1998), 49(11), 414-420 Volmer, D. GC-MS 417 Verpamil & SPME-HPLC Determination of Verpamil and Norverpamil Enantiomers in Urine HPLC norverapamil J. Mass Spectrom. (1997), 32(11), 1195-1204 in urine Asafu-Adjaye, E., Shiu, G. 971 Pesticides in water Pesticide toxicity assessment using an electrochemical biosensor. Analytical and Bioananalytical Chemistry (2002) 373(8), 696-703 Farre, M.; Goncalves, C.; Lacorte, S.; Barcelo, D.; Alpendurada, M.F. GC-MS Absorption through porcine skin exposed to various doses of jet fuel marker components determined with GC-FID using head space SPME fiber. 1034 Jet fuel in porcine skin. Toxicological Sciences (2003) 72 (S-1), 383. 1050 PAH Xia, X. R.; Riviere, J. E.; Muhammad, F.; Monteiro-Riviere, N. A.; Baynes, R. E. Determination of selected monohydroxy metabolites of 2-, 3- and 4-ring polycyclic aromatic hydrocarbons in urine by solid-phase microextraction and isotope dilution gas chromatography-mass spectrometry. Journal of Chromatography, B: Analytical Technologies in the Biomedical and Life Sciences (2002) 778 (1-2), 157-164. GC-MS Smith, C. J.; Walcott, C. J.; Huang, W. L.; Maggio, V.; Grainger, J.; Patterson, D. G., Jr. 1294 Biomimetic solid-phase microextraction to predict body residues and toxicity of chemicals that act by narcosis. Environmental Toxicology and Chemistry (2002) 21(2), 229-234 Leslie, Heather A.; Busser, Frans J. M.; Hermens, Joop L. M.; Kraak, Michiel H. S.; Oosthoek, Annelies J. P. GC-MS 1349 Fatty acid ethyl esters in hair as markers of alcohol consumption. Segmental hair analysis of alcoholics, social drinkers, and teetotalers. Fatty acid ethyl esters in hair Clinical Chemistry (2001) 47(12), 2114-2123. Auwaerter, V.; Sporkert, F.; Hartwig, S.; Pragst, F. *; Vater, H.; Diefenbacher, A. GC-MS Ambient temperature, unless otherwise indicated. 126
1381 (New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Sample preparation with fibre-in-tube solid-phase microextraction for capillary electrophoretic separation of tricyclic antidepressant drugs in human urine. Tricyclic antidepressants in urine. Electrophoresis (2001) 22(17), 3785-3790. Jinno, K.; Kawazoe, M.; Saito, Y.; Takeichi, T.; Hayashida, M. Analysis of fatty acid ethyl esters in hair as possible markers of chronically elevated alcohol consumption by headspace solid-phase microextraction (HS SPME ) and gas chromatography-mass spectrometry (GC-MS). Fatty acid ethyl esters 1391 in hair. Forensic Science International (2001) 121(1-2), 76-88. Pragst, F.; Auwaerter, V.; Sporkert, F.; Spiegel, K. 65 um PDMS/DVB GC-MS Pollution prevention screening of simulated Hanford waste for polychlorinated biphenyls by solid phase microextraction/GC-ECD. 1417 Abstracts of Papers American Chemical Society (2001) 222(1-2), ANYL118. Okemgbo, Asopuru A.; Metcalf, Steven G. 1438 Methylene chloride in urine Monitoring of occupational exposure to methylene chloride: Sampling protocol and stability of urine samples. Journal of Toxicology Clinical Toxicology (2003) 41(5), 735-735 Tabak, A.; Scherb, I.; Hoffer, E.; Bentur, Y.; Weiner, A. 2755 Fentanyl in Determination of fentanyl in human plasma by head-space SPME-GC-MS J. PHARM. BIOMED. ANAL. 43, #5, 1763-1768 (11 APR 2007) headspace GC-MS human plasma Bagheri, H.; Es-haghi, A.; Khalilian, F.; Rouini, M. -R. 1489 1501 Fentanyl and midazolam in plasma Simultaneous determination of fentanyl and midazolam in plasma using direct solid-phase microextraction before gas chromatography-mass spectrometry analysis. Analytical Letters (2002) 35(9), 1575-1590 65um PDMS/DVB Dufresne, C.; Bureau, J.; Favetta, P.; Gonin, R.; Guitton, J. Fully automated determination of amphetamines and synthetic designer drugs in hair samples using headspace solid-phase microextraction and gas chromatography-mass spectrometry. Amphetamines and designer drugs in hair Journal of Chromatographic Science (2002) 40(6), 359-364 Musshoff, Frank; Junker, Heike P.; Kroener, Lars; Lachenmeier, Dirk W.; Madea, Burkhard GC-MS 2351 GHV, MAMP, A validated SPME-GC-MS method for simultaneous quantification of club drugs in human urine. 100µm PDMS GC-MS KET, MDMA Forensic Sci Int 71, #2-3, 142-50 (2007 Sep 13) 20 min @ 90°C in urine Brown, Stacy D; Rhodes, Daniel J; Pritchard, Boyd J hexylchloroformate/ pyridine derivative Detection and identification of illicit drugs including GHB, Rohypnol, Ketamine, and Psilocybin by refocused Solid Phase Microextraction High Performance Liquid Chromatography Mass Spectrometry, (SPME/HPLC/MS). 1511 Drugs of abuse Abstracts of Papers American Chemical Society (2002) 223(1-2), ANYL 54 HPLC-MS 1021 Sabucedo, Alberto; Furton, Kenneth G.; Benson, Andrew; Almirall, Jose A fatal human intoxication with the herbicide allyl alcohol (2-propen-1-ol). allyl alcohol (2-propen- Journal of Analytical Toxicology (2002) 26(1), 55-57 1-ol) Toennes, S. W.; Schmidt, K.; Fandino, A. S.; Kauert, G. F. GC-MS Ambient temperature, unless otherwise indicated. 127
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