SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
J. Chemical Ecology, Vol. 23, No., 12, 1997, 2897-2915 headspace
Robacker, D., Bartelt, R.
Pheromone analysis using capillary GC techniques
470 Pheromones J. Chromatogr., A 1999, 843(1+2), 199-236 review of use of SPME GC
Jones, G., Oldham, N.
124 Pheromones
Solid Phase Microextraction Technique Used for Collecting
Semiochemicals, Identification of Volatiles Released by 100µm PDMS GC-MS
in insects Individual Signaling Phylionorycter sylvella Moths 1-3 hr
Z. Nturforsch. C: Giosci. 51: 599 (1996)
Karlson-Borg, A., Mozuaitis, R.
headspace
2484 Pheromones
The scent of the waggle dance
PLoS Biology 5, #9, 1862-1867 (SEP 2007) headspace GC/MS
in honey bees Thom, Corinna; Gilley, David C.; Hooper, Judith; Esch, Harald E.
Use of SDS page, SPME, and GC-MS for chemical analysis of
2332 Phermones temporal gland secretions from African elephants. GC/MS
African elephant Abstracts of Papers Am Chem Society (2004) 227 Part1, U443
Freyaldenhoven, D.; Kopper, R.; Goodwin, T.; Lichti, C.;Rasmussen, L.
Chemical analysis of urine from male african elephants by SDS PAGE,
2333 Urine from SPME, and GC-MS. GC/MS
African elephant Abstracts of Papers Am Chem Society (2004) 227 Part1, U425
Carver, A.; Davis, B.; Kopper, R.; Goodwin, T.; Lichti, C.;
Rasmussen, L..; Hollister-Smith, Julie; Alberts, S.
410 Pheromones in
Purification, Identification, Concentration and Bioactivity
of (Z)-7-dodecen-1-yl acetate: Sex Pheromone of the GC-MS
elephant urine Female Asian Elephant, Elephas maximus
Chem. Senses 22: 417-437
Rasmussen, L.E.L., Lee, T.D., Zhang, A., Roelofs, W.L.,
and Daves Jr., G.D.
773 Fungal volatiles
Application of SPME for the determination of fungal
volatile metabolites
Prog. Biotechnol (2000) 17, 369-377
Jelen, H.; Wasowicz, E
394 Free fatty acids
Sampling Techniques for GC-MS Analysis of Long-Chain
Free Fatty Acids from Insect Exocrine Glands 100µm PDMS, GC-MS
in exocrine secretions J. Chromatogr. A 816 (1998) 169-175 65µm Carbowax/DVB
Maile, R., Dani, F., Jones, G., Morgan, D., Orthius, D.
Attractants from Stryphylococcus aureus Cultures from
140°C, 30 min
headspace
382 Volatile attractants Mexican Fruit Fly, Anastrepha ludens 100µm PDMS GC-MS
in cultures J. Chemical Ecology, Vol. 21, No. 11, 1861-1874 (1995) 5 min - 24 hr
Robacker, D., Flath, R. headspace
471 Volatile attractants
Volatiles of bracket fungi Fomtopsis pinicola
and Fomes fomentarius and their functions as GC-MS
in bracket fungi insect attractants
J. Chem. Ecol. (1999), 25(3), 567-590
Faldt, J., Jonsell, M., Norlander, G., Borg-Karlson, A.
Volatiles from Fusarium verticillioides (Sacc.) Nirenb.
584 Alcholols, aldehydes and their attractiveness to Nitidulid beetles. 100µm PDMS GC-FID/MS
in air J-Agric-Food-Chem. Jun 1999; 47(6): 2447-2454 30 min
Bartelt,-RJ; Wicklow,-DT
472 Volatile attractants
Identification of a new blend of apple volatiles
attractive to the apple maggot, GC-FID
from apples Rhagoletis pomonella
J. Chem. Ecol., 1999, 25(6), 1221-1232
Zhang, A., Linn, C., Wright, S., Prokopy, R.
Reissig, W., Roelogs, W.
Ambient temperature, unless otherwise indicated. 77