SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument in swine manure J. Environ. Sci.Health, B34(4), 709-748 (1999) headspace, pH 2 Rizzuti, A., Cohen, A., Hunt, P., Vanotti, M. Headspace-SPME-GC as a tool to define an index that establishes the 2722 Ethyl esters retention capacity of the wine polymeric fraction towards ethyl esters headspace GC in wine J.Chromatogr. A 1150, #1-2, 155-161 (2007) Rocha, S. M.; Coutinho, P.; Delgadillo, I.; Coimbra, M. A. Analysis of esters in wines 966 Esters in wine J.Chromatogr. A (2002) 963(1-2), 213-223 Various GC Rodriguez-Bencomo, J.J.; Conde, J.E.; Rodriguez-Delgado, M.A.; Garcia- Montelongo, F.; Perez-Trujillo, J.P. Flavor and odor differences between fresh and preserved onions 967 Aroma in onions J.Chromatogr. A (2002) 963(1-2), 89-93 Polyacrylate GC-MS Mondy, N.; Duplat, D.; Christides, J.P.; Arnault, L.; Auger, J. Influence of crushing technique on composition of volatiles in olive oil 968 Volatiles in olive oil European Journal of Lipid Science and Technology (2002) 104(8), 483-489 65 um Carbowax/DVB GC-MS Servili, M.; Piacquadio, P.; de Stefano, G.; Taticchi, A.; Sciancalepore, V. 30 mins. Monitoring volatile compounds during the dry-cured ham ripening process 969 Volatiles in dry-cured ham J.Chromatogr. A (2002) 963(1-2), 83-88 Andres, A.I.; Cava, R.; Ruiz, J. Bisphenol type contaminants from food packaging materials in aqueous foods. 970 Bisphenol in food packaging J.Chromatogr. A (2002) 963(1-2), 375-380 Nerin, C.; Philo, M.R.; Salafranca, J.; Castle, L. HPLC 992 996 Development of headspace SPME, GC-MS method for the identification of odour causing volatile compounds in packaging materials. Odour compounds in food packaging materials J.Chromatogr. A (2002) 963(1-2), 381-392 75 um carboxen/PDMS GC-MS Ezquerro, O.; Pons, B.; Tena, M.T. Response surface models used for prediction of photooxidative quality changes of havarti cheese. Photooxidative quality changes of havarti cheese. European Food Research and Technology (2003) 216 (2), 93-98. GC-MS Stapelfeldt, Henrik; Mortensen, Grith; Sorensen, John. Solid phase micro-extraction technique and its applications in medical analysis. 997 Yaoxue Xuebao (2003) 38 (2), 153-158. Liu Zhen-ling; Wu Cai-ying. 999 Volatile compounds recovered by solid-phase microextraction from fresh adductor muscle and total lipids from sea scallop ( Placopecten magellanicus ) from Georges Bank (Nova Scotia). Volatile compounds from scallops Journal of Food Science (2002) 67 (6), 2032-2037. PDMS/DVB GC-MS Linder, M.; Ackman, R. G. 250 C, 2 minutes Headspace solid-phase microextraction in combination with gas chromatography-mass spectrometry for the rapid screening of organophosphorus insecticide residues in strawberries and cherries 1007 Insecticides in fruit J.Chromatogr. A (2003) 993(1-2), 197-203. GC-MS Albanis, Triantafyllos A.; Lambropoulou, Dimitra A. Solid phase microextraction capillary gas chromatography combined with furnace atomization plasma emission spectrometry for speciation of mercury in fish tissues 1012 Mercury in fish Spectrochmica Acta - Part B Atomic Spectroscopy (2003) 58 (3), 427-441. GC-FAPES Campos, Reinaldo C.; Grinberg, Patricia; Mester, Zoltan; Sturgeon, Ralph E. Ambient temperature, unless otherwise indicated. 26
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Headspace volatiles of Scutellaria californica A. Gray flowers 2781 Volatiles in J. Essent. Oil Res. 20, #2, 169-171 (March/April 2008) headspace GC-MS gray flowers Dao, Lan; Patterson, Robert; Rodriguez, David; Takeoka, G. Analysis of the volatile compounds of flowers and essential 2768 Volatiles in oils from Lavandula angustifolia cultivated in northeastern Italy Carboxen/DVB GC-MS lavender flowers by headspace SPME -GC-MS headspace Planta Medica 74, #2, 182-187 (FEB 2008) 50 min. Da Porto, Carla; Decorti, Deborha Use of SPME as a sampling technique for the characterization of 2470 Volatiles in volatile compounds emitted from Chinese daffodil flowers. headspace GC-MS daffodil flowers. J. Anal. Chem. (Transl. Zh. Anal. Khim.) 62, #7, 674-679 (2007-07) Song, G.; Xiao, J.; Deng, C.; Zhang, X.; Hu, Y. Volatile constituents of the leaves and flowers of Hypericum triquetrifolium Turra 1016 Volatiles in flowers Flavour and Fragrance Journal (2003) 18 (2), 91-94. GC-MS Bertoli, Alessandra; Mazzetti, Michele; Menichini, Francesco; Morelli, Ivano; Spinelli, Guido Evolution of volatile byproducts during wine fermentations using immobilized cells on grape skins. Volatile byproducts in 1017 wine Journal of Agricultural and Food Chemistry (2003) 51 (8), 2402-2408. Komaitis, Michael; Kanellaki, Maria; Koutinas, Athanasios; Mallouchos, Athanasios Analysis of terpenoids from hemlock (Tsuga) species by solid-phase microextraction/gas chromatography/ion-trap mass spectrometry. Terpenoids from 1018 hemlock Journal of Agricultural and Food Chemistry (2003) 51 (8), 2115-21120. Lagalante, Anthony F.; Montgomery, Michael E. GC-MS Volatile components associated with freshly cooked and oxidized off-flavours in turkey breast meat. 1027 Volatiles from meats Flavour and Fragrance Journal 2002) 17 (5), 327-334. GC-MS Brunton, N. P.; Cronin, D. A.*; Monahan, F. J. Analysis of volatile and semivolatile composition in cut tobacco and total particulate matter of cigarettes with SPME-GC-MS. Volatiles and semi- 1044 volatile in cigarettes. Fenxi Shiyanshi (2002) 21 (5), 31-35. Li, R.; Wang, L.; Li, Q.; Tong, X. D. 85 um Polyacrylate GC-MS Survey of 2-ethylhexanoic acid in baby food 2376 2-ethylhexanoic Food Additives and Contaminants 24, #7, 792-797 (JUL 2007) acid in baby food Ezerskis, Z.; Pastorelli, S.; Contini, C.; Simoneau, C. 1052 Comparison of mass spectrometry-based electronic nose and solid phase microextraction gas chromatography-mass spectrometry technique to assess infant formula oxidation. Oxidation of infant formula Journal of Agricultural and Food Chemistry (2003) 51 (9), 2790-2796. GC-MS Guy, Philippe A.; Fenaille, Francois; Fumeaux, Rene; Milo, Christian; Visani, Piero Formation of aroma compounds from ribose and cysteine during the maillard reaction. 1053 Aroma compounds Journal of Agricultural and Food Chemistry (2003) 51 (9), 2714-2721. GC-MS Cerny, Christoph; Davidek, Tomas A headspace-SPME-MS method for monitoring rapeseed oil autoxidation 2497 Volatile compounds J Am Oil Chemists' Society 84, #6, 509-517 (JUN 2007) headspace GC-MS rapeseed oil Jelen, H. H.; Mildner-Szkudlarz, S.; Jasinska, I.; Wasowicz, E Solid-phase microextraction for studies on the enantiomeric composition of filbertone in hazelnut oils. 1055 Volatile compounds Journal of Agricultural and Food Chemistry (2003) 51 (9), 2496-2500. hazelnut oil. Ruiz del Castillo, M. L.; Blanch, G. P.; Flores, G.; Herraiz, M. Ambient temperature, unless otherwise indicated. 27
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