SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Organophosphorous Literature Reference Application of solid-phase microextraction for the determination of organophosphorus pesticides in aqueous samples by gas chromatography with flame photometric detector. Conditions Instrument 1364 pesticides Talanta (2001) 55(4), 807-814. Yao, Z. W.; Jiang, G. B.*; Liu, J. M.; Cheng, W. Various GC-FID Focused microwave assistance for extracting some pesticide residues from strawberries into water before their determination by SPME/HPLC/DAD. Pesticides in 1369 strawberries. Journal of Agricultural and Food Chemistry (2001) 49(11). Falqui-Cao, C.; Wang, Z.; Urruty, L.; Pommier, J. -J.; Montury, M. * 60µm PDMS/DVB HPLC 1395 Pesticides Analysis of acidic pesticides using in situ derivatization with alkylchloroformate and solid-phase microextraction ( SPME ) for GC-MS. Chemosphere (2001) 44(7), 1531-1539. Henriksen, T.; Svensmark, B.; Lindhardt, B.; Juhler, R. K. PDMS GC-MS 1406 Pesticides Formation of volatile halogenated by-products during chlorination of isoproturon aqueous solutions. Chemosphere (2001) 45(3), 269-274. Lopez, A.; Ciannarella, R.; Mascolo, G.; Tiravanti, G. 85 µm polyacrylate GC-MS Factors affecting multiresidue determination of priority herbicides when using solid-phase microextraction. 1439 Herbicides in water Journal of AOAC International (2002) 85(2), 486-493 1445 1459 1483 Organochlorine pest. In water Methyl parathion in apples triazole in wine and strawberries 1494 Organochlorine pesticides in water 1495 Pesticides in bee products Albanis, Triantafyllos A.; Konstantinou, Ioannis K.; Lambropoulou, Dimitra A. Determination of organochlorine pesticides in water using microwave assisted headspace solid-phase microextraction and gas chromatography 100µm PDMS and 85µm Polyacrylate GC-FID, GC-MS Journal of Chromatography A (2003) 1012(2), 129-137 Various fibers compared GC-ECD Jen, Jen-Fon; Li, Gwo-Chen; Li, Hong-Ping Field study for degradation of methyl parathion in apples cultivated with integrated crop management system. Bulletin of Environmental Contamination and Toxicology (2002) 69(6), 771- 778 Tsatsakis, A. M.; Danis, T. G.; Nikitovic, D. P.; Stratis, I. A.; Toutoudaki, M.; Tsakiris, I. N. Solid-phase microextraction and gas chromatography-mass spectrometry for the rapid screening of triazole residues in wine and strawberries. Journal of Chromatography A (2002) 967(2), 255-260 Zambonin, C. G.; Cilenti, A.; Palmisano, F. Determination of organochlorine pesticides in ground water using solid-phase microextraction followed by dual-column gas chromatography with electroncapture detection. Journal of Chromatography A (2002) 964(1-2), 21-33 30µm PDMS GC-ECD Tomkins, Bruce A.; Barnard, Angela R. Analytical methods for pesticide residue determination in bee products. Journal of Food Protection (2002) 65(9), 1502-1511 Fernandez, M.; Manes, J.; Pico, Y. Identification of dimethylchloroarsine near a former herbicide factory by headspace solid-phase microextraction gas chromatography-mass spectrometry. 1505 Dimethylchloroarsine Chemosphere (2002) 48(9), 1003-1008 Aldstadt, Joseph H., III; Killelea, Daniel R. Ambient temperature, unless otherwise indicated. 192 85µm Carboxen PDMS Stableflex GC-MS
1522 1531 1554 1551 (New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Chlorinated pesticides in water Organophosphorus pesticides in cherry and strawberry juice Determination of chlorinated pesticides in water by SPME/GC. Water Research (2002) 36(7), 1909-1911 100µm PDMS GC-ECD Boussahel, R.; Baudu, M.; Bouland, S.; Montiel, A.; Moussaoui, K. M. Headspace solid phase microextraction applied to the analysis of organophosphorus insecticides in strawberry and cherry juices. Journal of Agricultural and Food Chemistry (2002) 50(12), 3359-3365 Various fibers compared GC-MS Albanis, Triantafyllos A.; Lambropoulou, Dimitra A. Evaluation of Solid Phase Microextraction-gas chromatography in the analysis o some pesticides with different mass spectrometric techniques: Application to environmental waters and food samples. Pesticides in water and Analytical Letters (2002) 35(2), 327-338 food Benfenati, E.; Natangelo, M.; Tavazzi, S. GC-ITMS Pesticides in human blood Headspace solid-phase microextraction in combination with gas chromatography and tandem mass spectrometry for the determination of organochlorine and organophosphorus pesticides in whole human blood. Journal of Chromatography B (2002) 769(1), 65-77 GC-MS Hernandez, F.; Beltran, J.; Lopez, F. J.; Pitarch, E. 1386 Herbicides Applications of solid-phase microextraction ( SPME ) in the determination of residues of certain herbicides at trace levels in environmental samples. Journal of Environmental Monitoring (2001) 49(9), 505-508. Ramesh, A.; Ravi, P. E. 65µm Carobwax/DVB GC-ECD Determination of tebufenpyrad and oxadiazon by solid-phase microextraction and gas chromatography-mass spectrometry. Tebufenpyrad and 1384 oxadiazon. Chromatographia (2001) 54(5-6), 377-382. Navalon, A.; Prieto, A.; Araujo, L.; Vilchez, J. L.* 100µm PDMS GC-MS 2550 2-aminoaceto- Analysis of 2-aminoacetophenone by direct-immersion SPME-GC-MS and its sensory impact in Chardonnay and Pinot gris wines. immersion GC-MS phenone Food Chemistry 105, #3, 1144-1150 (2007) in wine Wenlai Fan; I-Min Tsai; Qian, M. C. 2815 Phthalates Determination of phthalates in wine by headspace SPME followed by GC-MS use of deuterated phthalates as internal standards headspace GC-MS in wine J Chromatography A 1181, #1-2, 125-130 (FEB 15 2008) Carrillo, J. D.; Martinez, M. P.; Tena, M. T. 2535 Phthalates Determination of phthalates in wine by headspace SPME followed by . GC-MS. Fibre comparison and selection 65µm PDMS-DVB GC-MS in wine J Chromatography A 1164, #1-2, 248-261 (2007) Carrillo, J. D.; Salazar, C.; Moreta, C.; Tena, M. T. headspace 2746 guaiacols, phenols Determination of Brett character responsible compounds in wines by using multiple headspace solid-phase microextraction 65µm CW-DVB GC-MS in wine J Chromatography A 1143, #1-2, 176-181 (2007) Pizarro, C.; Perez-del-Notario, N.; Gonzalez-Saiz, J. M. headspace 2526 Ethylphenols Determination of ethylphenols in wine by in situ derivatisation and headspace solid-phase microextraction-GC-MS 50/30 DVB/CAR GC-MS in wine Anal Bioanal Chem 387, #7, 2547-2558 (2007) headspace Carrillo, J. D.; Tena, M. T. Automated analysis of 2-methyl-3-furanthiol and 3-mercaptohexyl . 70C for 70 min acetic anhydride 2573 Polyfunctional acetate at ng L minus 1 level by headspace SPME with on-fibre . 65µm PDMS-DVB GC-MS thiols in wine derivatisation.and GC-negative chemical ionization MS determination headspace J. Chromatogr., A 1121, #1, 1-9 (2006-07-14) 5 min Ambient temperature, unless otherwise indicated. 193
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