SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference
Volatiles from apple (Malus domestica) eliciting antennal
Conditions Instrument
889 Volatile attractants antennal responses in female codling moth Cydia pomonella GC-Electrofrom
apples (L.) (Lepidoptera: Tortricidae): Effect of plant injury and s
sampling technique
Zeitschrift fuer Naturforschung Sec C (2001) 56(3-4) 262-268
Backman, A; Bengtsson, M; Karlsson, A; Liblikas, I; Witzgall, P
antennography
636 Pyrazine
Headspace SPME method for determining 3-akyl-2 methoxypyrazine
in musts by PDMS fibers 100µm PDMS/DVB GC-NPD
in Must J Chromatogr. Sci (2000), 880(1+2), 93-99 4 hr.@30°C
Sala, C., Mestres, M, Marit, M., Busto, O., Guasch, J.
Development of a SPME-GC-ECD methodology for
headspace
NaCl added
892 Pesticides selected pesticides in must and wine samples GC-ECD
in must & wine Fresenius' J Anal Chem) 369(7-8) 647-651
Alves, A; Correia, M; Delerue-Matos, C
Headspace SPME and Gas Chromatography with
211 Musk compounds Atomic-Emission Detection 100µm PDMS GC-AED
in cosmetic products Chromatographia 45: 138-144 (1997) 80°C, 30 min
Struppe, C., Schaefer, B., Engewald, W. headspace
835 Volaitles from
SPME-GC-MS analyses of hazelnut creams
Lab. 2000 (2000) 14(7), 86-88 GC-MS
hazelnut creams Saba, A.; Cuzzola, A.; Raffaelli, A.; Salvadori, P.
821 Fragrances
A novel technology to study the emission of
fragrance from the skin 100µm PDMS GC-MS
on skin Perfumer& Flavorist, vol. 23 (1998) 1-11 30-60min
Mookherjee, B., Patel, S., Trenkle, R., Wilson, R. headspace
637 Volatiles
Analysis of headspace constituents of Gardenia flower by
GC-MS with SPME and dynamic headspace sampling 100µm PDMS GC-MS
in Gardenia flower Sepu, (2000-09) 18(5) 425-455 60 min @ 28°C
Liu, B., Gao, Y. headspace
Composition of the volatiles from flowers of Bystropogon
2811 Volatiles moderensis Webb by SPME
in flower Planta Medica 73, #9, 949-950 (AUG 2007)
Castilho, P. C.
2568 Fragrance in
Analysis of volatile compounds emitted from fresh Syringa oblata
flowers in different florescence by headspace SPME-GC-MS 65µm PDMS/DVB GC-MS
Syringa oblata Anal. Chim. Acta 576, #1, 43-49 (2006-08-18) headspace
flowers Li, Z. G.; Lee, M. R.; Shen, D. L. 30 min @ 25°C
882 Fragrance
On-site field sampling and analysis of fragrance from living
Lavender (Lavandula angustifolia L.) flowers by SPME 100µm PDMS GC-MS
in Lavender flowers coupled to GC and io-trap mass spectrometry 10 min @ 28°C
J. chromatogr. A 917(2001) 245-250
An, M., Haig, T., Hatfield, P.
headspace
2555 Furfural in
Diffusive sampling of airborne furfural by SPMEdevice with on-fiber
derivatization 65µm PDMS/DVB GC-MS
Air J. Chromatogr., A 1129. #1, 29-33 (2006-09-29) 25°C
Tsai, S. W.; Kao, K. Y. PFBHA derivative
2469 Aroma volatiles
Application of headspace-SPME-HPLC for the analysis of the aroma
Volatile components of treacle and determination of its content headspace HPLC
from treacle of 5-hydroxymethylfurfural (HMF).
Food Chemistry 104, #3, 1310-1314 (2007)
Edris, A. E.; Murkovic, M.; Siegmund, B.
2428 Fragrance
Isolation and characterization of the volatile aroma compounds
from the concrete headspace and the absolute of Jasminum 100µm PDMS GC-MS
in flowers sambac (L.) Ait. (Oleaceae) flowers grown in Egypt
Eur. Food Res. Technol. 226, #3, 621-626 (January 2008)
headspace
Ambient temperature, unless otherwise indicated. 78