SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
Determination of clenbuterol in urine using headspace SPME or
2247 Clenbuterol liquid-liquid-liquid microextraction headspace GC/MS
in urine Analytica Chimica Acta 552 #1-2, 67-75 (2005) HMDS derivatives
Melwanki, Mahaveer B.; Hsu, Wei-Hsun; Huang, Shang-Da
1169 Clenbuterol in urine
Quick analysis of small beta -agonists in urine by solid-phase microextraction
with headspace derivatization and gas chromatography-mass spectrometry.
Fenxi Huaxue (2003) 37 (3), 326-328.
Liang, Y. L.; Yin, B. Z.; Hu, X. Z.*; Yu, J. X.; Liu, H. W.; Lin, Y. F.; Wu, T.
Polyacrylate GC-MS
Simple and rapid analysis of endocrine disruptors in liquid medicines and
intravenous injection solutions by automated in-tube solid-phase
microextraction/high performance liquid chromatography.
Endocrine disruptor
1279 contaminants. Journal of Pharmaceutical and Biomedical Analysis (2003) 32 (3), 469-478.
Mitani, K.; Narimatsu, S.; Izushi, F.; Kataoka, H. *
HPLC
1308 Drug analysis
Solid-phase microextraction and liquid chromatography/mass spectrometry in
drug analysis
Analytica Chimica Acta (2003) 492 (1-2), 49-67.
Kumazawa, Takeshi; Lee, Xiao-Pen; Sato, Keizo; Suzuki, Osamu
LC-MS
Determination of pharmaceutical process impurities by solid phase
microextraction gas chromatography
Pharma process
1312 impurities Journal of Separation Science (2003) 26 (12-13), 1097-1103.
Frost, Richard P.; Hussain, Mumtaz S.; Raghani, Anil R.
Carboxen/PDMS/DVB GC
In vivo sampling with solid phase microextraction
2445 Drugs in J. Biochem. Biophys. Meth. 70, #2, 181-193 (2007-03-10)
biological fluids Musteata, F. M.; Pawliszyn, J.
Development and evaluation of a solid-phase microextraction probe for in vivo
pharmacokinetic studies
1336 Analytical Chemistry (2003) 75 (19), 5103-5115. polypyrrole
Fahie, Brian; Grant, Russell P.; Incledon, Bev; Lord, Heather L.; Pawliszyn,
Janusz B.; Walles, Markus
1361
Automated sample preparation using in-tube solid-phase microextraction and
its applications long dash a review.
Drugs in biological
fluids Analytical and Bioanalytical Chemistry (2002) 373(1-2), 31-45.
Kataoka, H.
LC-MS
Comparison of SPME and liquid-liquid extraction in 96-well format for
2753 Drugs in the determination of a drug compound in human plasma by LC-MS LC-MS
plasma J. PHARM. BIOMED. ANAL. 45, #4, 599-608 (30 NOV 2007)
Xie, W.; Pawliszyn, J.; Mullett, W. M.; Matuszewski, B. K.
2562 Asarones
Development of GC-MS following headspace SPME for fast .
determination of asarones in plasma headspace GC-MS
in plasma Rapid Commun. Mass Spectrom.20, #14, 2120-2126 (2006-06-09)
Deng, C. H.; Lin, S.; Huang, T. M.; Duan, G. L.; Zhang, X. M.
2905 Nitromethane
Method for quantifying nitromethane in blood as a potential biomarker
of halonitromethane exposure headspace GC/MS
in blood Environ. Sci. Technol. 42, #7, 2522-2527 (Apr 1 2008)
Alwis, K. ; Blount, Be.; Loose, K; Silva, Lalith K.; Smith, M.
SPME method for carbon isotopic analysis of volatile carboxylic acids in
2561 Carboxylic acid human plasma byGC/combustion/isotope ratio mass spectrometry. 75µm Carboxen GC/C/IRMS
in plasma Rapid Commun. Mass Spectrom. 20, #23, 3573-3578 (2006-11-13)
Ferchaud-Rocher, V.; Albert, C.; Champ, M.; Krempf, M.
headspace
Simultaneous determination of selegiline and desmethylselegiline in
Ambient temperature, unless otherwise indicated. 93