SPME Applications Guide - Overbrook Scientific

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1390 (New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Volatile fingerprinting (SPME-GC-FID) to detect and discriminate diseases of potato tubers. Conditions Instrument Volatiles in potato tubers Plant Disease (2002) 86(2), 131-137 Kushalappa, A. C.; Chen, C. R.; Lee, B.; Lui, L. H. GC-FID Fast extraction, clean-up and detection methods for the rapid analysis and screening of seven indicator PCBs in food matrices. 1399 PCBs in food. Trends in Analytical Chemistry (2002) 21(1), 39-52 Anklam, E.; von Holst, Christoph; Bjorklund, E. Optimization of solid phase microextraction analysis of aroma compounds in a Portuguese muscatel wine must. 1401 Aroma from wine must. Journal of Microcolumn Separations (2001) 13(6), 236-242. 85 um polyacrylate Relva, A. M.; Freire, Luis M. T. Vaz; Freitas, A. M. Costa Monitoring of lipid degradation products by solid-phase microextraction Lipid degeneration 1402 products in oils Journal of Microcolumn Separations (2001) 13(6), 215-220. Doleschall, Fruzsina; Kemeny, Zsolt; Kovari, Katalin; Recseg, Katalin 100 um PDMS GC-FID Optimization of solid-phase microextraction analysis for studying change of headspace flavor compounds of banana during ripening. 1403 Volatiles in bananas Journal of Agricultural and Food Chemistry (2002) 50(4), 653-657 Liu, Tai-Ti; Yang, Tsung-Shi Solid phase microextraction and gas chromatography-olfactometry analysis of internal volatiles from intact citrus fruits and their aroma activity 1414 Volatiles from fruit. Abstracts of Papers American Chemical Society (2001) 222(1-2), AGFD142. GC-O Rouseff, Russell L.; Lin, Jianming SPME GC-MS-based testing for monitoring off-flavor development in processed milk. 1415 Off-flavors from milk Abstracts of Papers American Chemical Society (2001) 222(1-2), AGFD27. Marsili, Ray T. 1418 1420 1421 Volatiles in soybean and corn oils Solid phase microextraction of volatile soybean oil and corn oil compounds. Journal of Food Science (2002) 67(1), 71-76 Various fibers compared GC-MS Min, D. B.; Lee, J. H.; Steenson, D. F. Polydimethylsiloxane solid-phase microextraction-gas chromatography method for the analysis of volatile compounds in wines. Its application to the characterization of varietal wines. Volatile compounds in wine. Journal of Chromatography A (2001) 922(1-2), 267-275. PDMS GC Polo, M. C.; Martin-Alvarez, P. J.; Pozo-Bayon, M. A.; Pueyo, E. Determination of organochlorine pesticides and chlorobenzenes in strawberries by using accelerated solvent extraction combined with sorptive enrichment and gas chromatography/mass spectrometry. Pesticides in strawberries. Journal of AOAC International (2001) 84(4), 1194-1201. Wennrich, Luise; Breuste, Juergen; Koeller, Gabor; Popp, Peter Analysis of volatile compounds released from embryogenic cultures and somatic embryos of sweet oranges by head space SPME Volatile compounds 1422 from oranges. Plant Cell Tissue and Organ Culture (2001) 66(1), 31-34. Del Bosco, S. Fatta; Alonzo, G.; Saiano, F.; Tusa, N. GC-MS The effects of temperature and pressure on the performance of Carboxen/PDMS fibres during solid phase microextraction ( SPME ) of headspace volatiles from cooked and raw turkey breast. Volatiles from turkey 1423 breast. Flavour and Fragrance Journal (2001) 16(4), 294-302. Carboxen/PDMS Ambient temperature, unless otherwise indicated. 40
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Cronin, D. A.; Brunton, N. P.; Monahan, F. J. Conditions Instrument Headspace-SPME analysis of volatiles of the ridge gourd (Luffa acutangula) and bitter gourd (Momordica charantia) flowers. Volatiles of gourd 1424 flowers. Flavour and Fragrance Journal (2001) 16(4), 289-293. Grun, I. U.; Fernando, L. N. GC-MS Changes in the aroma of a strawberry drink during storage. Aroma of strawberry 1426 drink. Journal of Agricultural and Food Chemistry (2001) 49(7), 3244-3252. Siegmund, Barbara; Derler, Karin; Pfannhauser, Werner Truffle aroma characterization by headspace solid-phase microextraction 1440 Truffle aroma Journal of Chromatography A (2003) 1017(1-2), 207-214 Diaz, P.; Ibanez, E.; Reglero, G.; Senorans, F.J Analysis of total propionic acid in feed using headspace solid-phase microextraction and gas chromatography 1441 Propionic acid in feed Journal of Chromatography A (2003) 1017(1-2), 161-166 Ibanez, Carlos 1442 1448 Volatiles in Italian Vinegars Garlic flavor components Quantitative analysis of 2-furfural and 5-methylfurfural in different Italian vinegars by headspace solid-phase microextraction coupled to gas chromatography-mass spectrometry using isotope dilution Journal of Chromatography A (2003) 1017(1-2), 141-149 Calabrese, Roberto; Davoli, Enrico; Giordano, Lucia; Rotilio, Domenic Comparative study of extraction techniques for determination of garlic flavour components by gas chromatography-mass spectrometry. Analytical and Bioanalytical Chemistry (2003) 377(4), 749-756 Lee, S. N.; Kim, N. S.; Lee, D. S. 50/30um DVB/Carboxen PDMS headspace 13.6 mins. 85um Polyacrylate headspace 50/30um DVB/Carboxen PDMS headspace 50/30um DVB/Carboxen PDMS, headspace GC-MS GC-FID, GC-MS GC-MS GC-MS 2731 Volatiles in Comparative study of different extraction techniques for the analysis of virgin olive oil aroma headspace GC-MS Olive Oil Food Chemistry 105, #3, 1171-1178 (2007) Vichi, S.; Guadayol, J.; Caixach, J.; Lopez-Tamames, E.; Buxaderas, S. 1451 Volatiles in Olive Oil Solid-phase microextraction in the analysis of virgin olive oil volatile fraction: Characterization of virgin olive oils from two distinct geographical areas of northern Italy. Journal of Agricultural and Food Chemistry (2003) 51(22), 6572-6577 Lopez-Tamames, Elvira; Buxaderas, Susana; Conte, Lanfranco S.; Pizzale, Lorena; Vichi, Stefania GC-FID, GC-MS Solid-phase microextraction in the analysis of virgin olive oil volatile fraction: Modifications induced by oxidation and suitable markers of oxidative status. 1452 Volatiles in Olive Oil Journal of Agricultural and Food Chemistry (2003) 51(22), 6564-6571 Lopez-Tamames, Elvira; Buxaderas, Susana; Conte, Lanfranco S.; Pizzale, Lorena; Vichi, Stefania GC-FID, GC-MS 1453 Free fatty acids in ewe cheese Quantification of short-chain free fatty acids in "Terrincho" ewe cheese: Intravarietal comparison. Journal of Dairy Science (2003) 86(10), 3102-3109 Ferreira, I. M. P. L. V. O.; Ferreira, M. A.; Pinho, O. Evaluation of two commercial solid-phase microextraction fibres for the analysis of target aroma compounds in cooked beef meat Ambient temperature, unless otherwise indicated. 41 85um Polyacrylate 65 degrees C, 45 mins. Headspace GC-FID
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