SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1385 n-alkanes in soil. A new PVC-activated charcoal fibre coated on silver wire: application in determination of n-alkanes in the headspace of soil samples by SPME-GC. Analytical Sciences (2002) 18(1), 77-81. Farajzadeh, M.; Matin, A. A. Activated charcoal/PVC GC 1394 Hydrocarbons in soil. Determination of hydrocarbons in old creosote contaminated soil using headspace solid-phase microextraction and GC-MS. Chemosphere (2001) 44(7), 1641-1648. Eriksson, M.; Faeldt, J.; Dalhammar, G.; Borg-Karlson, A. -K. 30 µm PDMS GC-MS Headspace solid-phase microextraction of butyltin species in sediments and their gas chromatographic determination. Butyltin species in 1411 sediment. Journal of Separation Science (2001) 24(6), 459-464. Gui-bin, Jiang; Ji-yan, Liu; Ke-wu, Yang; Qun-fang, Zhou 100 µm PDMS Determination of chlorophenols in soil samples by microwave-assisted extraction coupled to headspace solid-phase microextraction and gas chromatography - Electron-capture detection 1446 Chlorophenols in soil Journal of Chromatography A (2003) 1012(2), 111-118 1461 Organophosphorus pesticides in soil 1462 Tributyltin in water and soil Jen, Jen-Fon; Wei, Ming-Chi Solid-phase microextraction coupled to gas chromatography- mass spectrometry for the study of soil adsorption coefficients of organophosphorus pesticides 85µm Polyacrylate, 1g soil in 6mL water, pH 2, 9mins. Headspace GC-ECD Journal of Environmental Monitoring (2002) 4(4), 477-481 GC-MS Zambonin, C. G.; Palmisano, F.; Losito, I.; Cilenti, A. Gas phase detection of tributyltin chloride arising from aqueous and solid matrices. Journal of Analytical Atomic Spectrometry (2002) 17(11), 1506-1510 GC-MS Bancon-Montigny, Chrystelle; Lam, Joseph W.; Maxwell, Paulette; Mester, Zoltan; Sturgeon, Ralph E.; Yang, Lu 1464 Aromatic acids in soil Separation and identification of aromatic acids in soil and the Everglades sediment samples using solid-phase microextraction followed by capillary zone electrophoresis. Journal of Chromatography A (2002) 979(1-2), 417-424 Deng, Yiwei; Fan, Xiaofang 85µm Polyacrylate CZE 1486 Monoaromatic hydrocarbons in soil Solid-phase microextraction-gas chromatographic determination of volatile monoaromatic hydrocarbons in soil. Fresenius' Journal of Analytical Chemistry (2002) 370(8), 1096-1099 100µm PDMS GC-MS Zygmunt, Bogdan; Namiesnik, Jacek Improvement in measurement precision with SPME by use of isotope dilution mass spectrometry and its application to the determination of tributyltin in sediment using SPME GC-ICP-MS. 1490 Tributyltin in sediment Journal of Analytical Atomic Spectrometry (2002) 17(8), 944-949 Yang, Lu; Mester, Zoltan; Sturgeon, Ralph E. 100µm PDMS, sodium tetraethylborate derivative Trace element speciation using solid phase microextraction 2243 Organometallic Spectrochimica Acta Part B: 60 #9-10, 1243-1269 (2005) Review article in water Mester, Zoltan; Sturgeon, Ralph Gas phase sampling of volatile (organo)metallic compounds above solid samples. GC-IDMS 1491 Organometallics in soil Journal of Analytical Atomic Spectrometry (2002) 17(8), 868-871 ICP-MS Mester, Zoltan Determination of tributyltin compounds in surface sediments of harbour by gas chromatography with headspace solid-phase microextraction Ambient temperature, unless otherwise indicated. 202
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument 1150 Tributyltin in sediment Fenxi Ceshi Xuebao (2003) 22 (2), 28-30. Lei, Z.; Huang, C. J.; Jia, L.; Shi, H. H. GC-FPD Removal of two polycyclic musks in sewage treatment plants: freely dissolved and total concentrations. Polycyclic musks in 1326 sewage. Environmental Science and Technology (2003) 37 (14), 3111-3116. Artola-Garicano, E.; Borkent, I.; Hermens, J. L. M.; Vaes, W. H. J. GC-MS SPME as a tool to predict internal concentrations 2097 Chloro- of soil contaminants in terrestrial organisms after 30µm PDMS GC benzenes exposure to a laboratory standard soil 1 day sample in soil Chemosphere, 54, #4, 561-568 headspace van der Wal, L.; van Gestel, C.; Hermens, J. Applicability of SPME combined with GC-MIP AED for the 2098 Butyltin in determination of butyltin compounds in sediment samples. ethylated derivative GC-MIP AED. sediment Analytical and Bioanalytical Chemistry, 380, #5-6, 853-857 headspace Carpinteiro, J.; Rodriguez, I. *; Cela, R. sonication Surface geochemical results complement 2099 Hydrocarbons conventional development approaches headspace GC in soil World Oil, 225, #12, 54-65 Quinlan, W.; Wood, James; Wylie, Albert Plant-assisted degradation of phenanthrene as 2100 Phenanthrene assessed by solid-phase microextraction (SPME) headspace GC-FID in soil Intl J of Phytoremediation, 6, #3, 253-268 Hynes, Russell K.; Farrell, Richard E.; Germida, James J. Determination of prometryn in soil by GC-MS using 2101 Prometryn microwave-assisted extraction associated with SPME microwave heated GC-MS in soil Fenxi Huaxue, 32, #6, 775-778 Yang, Y.; Luan, W.; Luo, X. J.; Li, G. K.* Soil volatile fungistasis and volatile fungistatic compounds 2102 Fungistasis Soil Biol. Biochem.,36, #12, 1997-2004 Headspace GC-MS in soil Chuankun, Xu; Keqin, Zhang; Leming, Zhang; Minghe, Mo Determination of benzene, toluene, ethylbenzene 2103 BTEX and xylenes in soils by multiple headspace SPME 75µm Carboxen GC-FID in soil J. Chromatogr. A, 1035, #1, 17-22 30min @ 30°C Ezquerro, O; Ortiz, G; Pons, B; Tena, M headspace over soil suspended in water Determination of the fungicides vinclozolin and 2104 Fungicides in dicloran in soils using ultrasonic extraction coupled 85µm polyacrylate GC-MS soil with SPME 5% acetone/water Anal. Chim. Acta, 514, #1, 125-130 Albanis, Triantafyllos A.; Lambropoulou, Dimitra A. Determination of pyrimethanil and kresoxim-methyl 2105 Fungicides in in soils by headspace SPME and GC-MS 85µm polyacrylate GC-MS, SIM in soil Anal. Bioanal. Chem., 379, #7-8, 1100-1105 headspace Araujo, L; Navalon, A; Prieto, A; Vilchez, J The moss Physcomitrella patens releases a 2106 Tetracyclic tetracyclic diterpene headspace GC-MS diterpene Plant Cell Rep., 22, #10, 780-786 from moss Kassner, H.; Schultze, W.; VonSchwartzenberg, K. Static headspace versus head space SPME for the 2107 Chlorinated for the determination of volatile organochlorine headspace GC-MS solvents in compounds in landfill leachates by GC Talanta, 63, #4, 809-814 Fernandez Martinez, E.; Fernandez Sanchez, M.; Florez Menendez, J.; Sanchez Uria, J.;Sanz-Medel, A. Optimization of microwave-assisted extraction 2108 Organics followed by SPME-GC-MS detection for the assay GC-MS in sebum of some semi-volatile organic J. Chromatogr.B, 825, #1, 11-20 Diaz-Vazquez, Liz; Garcia, Oscar; Marrero, I.; Rosario, Osvaldo; Velazquez, Zorangelys Ambient temperature, unless otherwise indicated. 203
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