SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference SPME and GC-MS for determination of monoaromatic Conditions Instrument 495 BTEX in hydrocarbons in blood and urine. Application to people 75µm Carboxen/PDMS GC-MS in urine & blood exposed to air pollutants Chromatographia, 1999, 50(3/4), 167-172 Andreoli, R., Manini, P. Bergamaschi, E., Brustolin, A., Mutti. A. headspace 591 BTEX in Headspace solid-phase micro-extraction for the determination of BTEX in urine. 100µm PDMS GC-EMIS urine J-Chromatogr,-B:-Biomed-Appl. 19 Feb 1999; 723(1-2): 105-115 15 min @ 30°C Fustinoni,-S; Giampiccolo,-R; Pulvirenti,-S; Buratti,-M; Colombi,-A headspace 662 Toluene The comparison of toluene determination between headspace SPME and Headspace methods in glue 100µm PDMS in blood sniffer's blood and urine samples J. Forensic Sci. (2000), 45(3), 702-707 Kim, N., Park, S. 496 Toluene, xylene Method for analyzing urinary toluene and xylene by SPME and its application to workers using organic solvents 100µm PDMS GC-FID in urine Bull. Environ, Contam. Toxicol. (1999), 62(2), 109-116 5 min, Asakawa, F., Jitsunari, F., Choi, J., Suna, S., Takeda, N., Kitamado, T. NaCl, stirring 497 Toluene, benzene Biomonitoring of benzene and toluene in human blood by headspace SPME 65µm Carboxen/PDMS GC-MS in human blood Fresenius' J. Anal. Chem. (1999), 363(1)m 88-91 30 min @ 20°C Schimmiing, E., Levsen, K., Koehme, C., Schuermann, W. headspace 332 Erythromycin A Study of Erythromycin A Decomposition Products in Aqueous Solution by SPME-LC-MS 65µm PDMS/DVB LC-MS in water Rapid Commun. Mass Spectrom. 10 (2): 225-234 (1998) 15 min Volmer, D., Hui, J. Rapid Determination of Corticosteroids in Urine by Combined immersed 50% MeOH extr. 333 Corticosteroids SPME-LC-MS LC-MS in urine Rapid Commun. Mass Spectrom. 11 (17): 1926-1934 (1997) Volmer, D., Hui, J. Polypyrrole coated capillary in-tube SPME coupled 663 Beta blockers with HPLC electrospray ionization MS for the Polypyrrole capillary LC-ESI-MS in urine, serum determination of beta blockers in urine and serum samples J. Microcolumn Sep. (2000) 12(4), 255-266 Wu, J., Lord, H., Pawliszyn, J., Kataoka, H. 334 Flavor compounds Evaluation of SPME for Analysis of Volatile Metabolites Produced by Staphylococci 100µm PDMS, GC-FID in staphylococci J. Agric. Food Chem. 46 (1): 228-234 (1998) 85µm polyacrylate Vergnaise, L., Masson, F., Montel, M., Berdague, J., Talon, R. Evaluation and identification of potential organic nematicidal headspace stirring, salt added pH 3 for esters 2576 Volatiles from volatiles from soil bacteria headspace GC-MS soil bacteria Soil Biology & Biochem 39, #10, 2567-2575 (OCT 2007) Gu, Ying-Qi; Mo, Ming-He; Zhou, Jun-Pei; Zou, Chang-Song; Zhang, K. Application of SPME to measure volatile metabolites 498 Aldehydes, esters produced by Staphylococcus carnosus and 100µm PDMS, 85µm polyacrylate GC-FID from bacteria Staphylococcus xylosus 15 min, stirring Book- Applied SPME, 1999, 364-371 Royal Society of esters @ 80°C, Chemistry, Cambridge, UK Coden: 67TUA8 aldehydes @ 25°C Talon, R, Montel, M. headspace 392 Volatile metabolites Application of Head-Space SPME for the Analysis of Volatile Metabolites Emitted by Penicillium Species 100µm PDMS, GC-MS in penicillium fungi J. Microbiological Methods, 25 (1996) 245-255 85µm polyacrylate Nilsson, T., Larsen, T., Montanarrella, L., Madsen, J. 25°C, 30 min (PDMS), 50 min (PA) Ambient temperature, unless otherwise indicated. 124
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Biotransformation of (R)-(+)- and (S)-(-)-limonene by Conditions Instrument 895 Volatile metabolites fungi and the use of SPME for screening. from limonen Phytochemistry (Oxford) (2001) 57(2) 199-208 Demyttenaere, J.; De Kimpe, N; Van Belleghem, K 2730 Volatile Fungal biotransformation of monoterpenes found in agro-industrial residues from orange and pulp industries into : headspace GC metabolites from aroma compounds screening using SPME monoterpenes Food Sci Biotech 16, #1, 37-42 (2007) Marostica, M. R., Jr.; Onoyama Mota, N.; Baudet, N.; Pastore, G. M. 802 Volatile metabolites Biotransformation of geraniol, nerol and citral by sporulated surface cultures of Aspergillus niger and Penicillium sp. in penicillium fungi Phytochemistry (2000) 55(4), 363-373 Demyttenaere, J.,del Carmen Herrera, M.; De Kimpe, N 393 Volatiles in Use of Digital Aroma Technology and SPME GC-MS to Compare Volatile Compounds produced by Bacteria Isolated from 100µm PDMS GC-MS bacteria on poultry Processed Poultry 37°C, 30 min J. Sci Food Agric. 1998, 78, 343-348 Arnold, J., Senter, S. headspace 664 Volatiles in Evaluation of SPME for the Isotopic Analysis of volatile compounds produced during fermentation by lactic 70µm Carboxen/PDMS GC-C-IRMS lactic acid bacteria acid bacteria 10 min J. Agric Food Chem. 2000, 48, 2222-2227 headspace Goupry, S., Rochut, N., Robins, R., Gentil, E. salt added 570 Fatty acid esters Headspace SPME with l-pyrenyldiazomethane in-fiber derivatization for analysis of fecal short-chain fatty acids 85µm polyacrylate GC-EMIS in faeses J-Chromatogr,-B:-Biomed-Appl. 25 Jun 1999; 730(1): 113-122 15 min Mills,-GA; Walker,-V; Mughal,-H Determination of Cannabinoids in Water and Human Saliva by 1-pyrenyldiazomethane derivative 335 Cannabinoids SPME and Quadrupole Ion Trap GC-MS 30µm PDMS GC-MS in water/saliva Anal. Chem. 70 (9): 1788-1796 (1998) 10 min Hall, B., Satterfield-Doeerr, M., Parikh, A., Brodbelt, J. immersion 665 Dibenzylamine Direct comparison of SPE and SPME for the GC determination of dibenzylamine in artificial saliva 85µm polyacrylate GC-MS in saliva leachates from baby bottle teats Anal Chim Acta 2000, 414(1-2), 133-140 Niessner, G., Klampfl, C. pH 10 Extraction and analysis of different Cannabis samples by 2185 Cannabinoids headspace SPME combined with GC-MS headspace GC-MS from Cannabis J SepSci. 28, #17, 2293-2300 (2005) samples Ilias, Y.; Rudaz, S.; Mathieu, P.; Christen, P.; Veuthey, Jean 340 Cannabinoids Solid-Phase Microextraction for Cannabinoids Analysis in Hair and Its Possible Application to Other Drugs 30µm PDMS GC-MS in hair J. Anal. Toxicology, Vol. 23, Jan./Feb. 1999 15 min, immersion Strano-Rossi, S., Chiarotti, M. Use of headspace SPME in hair analysis for hair digested with 1N NaOH 666 Lipophilic drugs organic compounds in hair Forensic Sci. Int. (2000), 107(1-3), 129-148 headspace Sporkiert, F., Pragst, F. hair digested with 4% NaOH 941 Lipophilic drugs Analysis of hair by headspace SPME and GC-MS. Chromatogr Separation Tech (2001), 17(2), 4-8 headspace in hair Pragst, F SPME in Forensic Toxicology hair digested with 4% NaOH 336 Review of use Jpn. J. Forensic Toxicol. 16 (1): 1-15 (1998) various fibers Ambient temperature, unless otherwise indicated. 125
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