SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
in water Anal. Chem. 68: 130-133 (1996) min to 20 hr
Dean, J., Tomlinson, W., Makovskaya, V., Cumming, R.,
Hetheridge, M., Comber, M.
immersion, stirring
546 PAHs
Solubility and partitioning studies with PAHs using an
optimized SPME procedure 100µm SPME GC-MS
in water and Fresenius' J. Anal. Chem. (1999), 363(4), 426-428 stirred
octanol-water Paschke, A., Popp, P., Schueuermann, G.
728 PAHs
Determination of PAHs in waste water by off-line coupling
SPME with column liquid chromatography 100µm PDMS HPLC
in waste water J. Chjromtogr. A, 897(2000) 153-159
Popp, P., Bauer, C., Moder, M., Paschke, A.
60 min fluorescence
547 Pesticides in
Extracted amounts by SPME: a realistic approach to the
partition coefficient K.
water J. Chromtogr. Sci. 1999, 37(8), 277-282
Urruty, L., Montury, M
548 Volatiles
Determination of Henry's law coefficient by combination of
the equilibrium partitioning in closed systems and 100µm PDMS GC-FID
in water SPME techniques
J. Chromatogr, A., (1999), 830(2), 353-363
Dewulf, J., Van Langenhove, H., Everaert, P
30 min @ varied temp.
237 Organics in
Partitioning of Organic Chemicals to Polyacrylate-Coated
Solid-Phase Microextraction Fibers: Kinetic Behavior and 85µm polyacrylate GC-FID, -ECD
water and air Quantitative Structure-Property Relationships immersion GC-MS
Anal. Chem. 68: 4458-4462 (1996)
Vaes, W., Hamwik, C., Ramos, E., Verhaar, H., Hermens, J.
stirring
Solid Phase Microextracting Using Fused-Silica Fibers Coated
84 with Graphitized Carbon Black
Chromatographia 41: 678-684 (1995)
Mangani, R., Cenciarini, R.
88 Overview
New Direction in Sample Preparation for Analysis of
Organic Compounds
Trends Anal. Chem. 14 (3): 113-122 (1995)
Pawliszyn, J.
Multiple applications
121 Eugenol,
Solid Phase Microextraction for Quantitative Analysis in
Nonequilibrium Situations 85µm polyacrylate GC-MS
2,4-dimethylphenol, Anal. Chem. 69: 1230-1236 (1997) 1-160 min
2-phenylethanol Ali, J. immersion, stirring
in water
SPME in Headspace Analysis, Dynamics in Non-Steady State
salt added
360 2-Octanol Mass Transfer 85µm polyacrylate, GC-MS
in water Anal. Chem., 70: 4822-4826, (1998) 100µm PDMS
Ali, J. headspace
2623 Volatiles from
Analysis of volatile compounds from Malaysian durians (Durio zibethinus)
using headspace SPME coupled to fast GC-MS headspace GC-MS
Malaysian durians J. Food Compos. Anal. (UK) 20, #1, 31-44 (Feb. 2007)
Nazimah, S.; Chin, S.; Quek, S.; Man, Y.; Rahman, R.; Hashim, D. M.
2637 Volatiles from
Characterization of volatile compounds in selected citrus fruits from
Asia. Part I: freshly-squeezed juice headspace GC-MS
citrus fruit Flavour and Fragrance J. 22, #3, 228-232 (MAY-JUN 2007)
Dharmawan, Jorry; Kasapis, Stefan; Curran, Philip; Johnson, Jeffrey R.
2725 Volatiles from
Postharvest survey of volatile compounds in five tropical fruits
using headspace-solid phase microextraction (HS-SPME). headspace GC-MS
tropical fruit HortScience 42, #2, 309-314 (2007)
Natta Laohakunjit; Orapin Kerdchoechuen; Matta, F.; Silva, J.; Holmes, W.
sat. salt
Ambient temperature, unless otherwise indicated. 214