SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Mateo-Vivaracho, L.; Ferreira, V. ; Cacho, J. Gas phase post derivitization following SPME for rapid analysis of polyphenols in wine by GC-MS. pentafluorobenzyl bromide 1558 Polyphenols in wine. Zhongshan Daxue Xuebao, Ziran Kexueban 40(1) 54-57. Luan, Tian-gang; Li, Gong-ke; Zhang, Zhan-xia. Chinese Fast screening determination of some ubiquitous 2078 Pesticides pesticides with SPME in water samples 85µm polyacrylate GC-MS in water Analytical Letters, 37, #7, 1427-1436 immersion sampling Moreira Vaz, J.; Komatsu, E. Multiresidue method using SPME for the determination 2079 Pesticides in of various pesticides with different volatility in 100µm PDMS GC-MS air confined atmospheres 40min Anal and Bioanal Chemistry, 379, #3, 476-483 dynamic air sampling Ferrari, F; Sanusi, Ad; Millet, M; Montury, M Pesticides analysed in rainwater in Alsace region (Eastern France): 2855 Pesticides in Comparison between urban and rural sites 100µm PDMS GC-MS/MS rainwater Atmospheric Environment 41, #34, 7241-7252 (NOV 2007) 65µm PDMS-DVB Scheyer, Anne; Morville, Stephane; Mirabel, Philippe; Millet, Maurice PFBBr derivatives Development of an SPME-GC-MS/MS method for the determination 2241 Pesticides in of pesticides in rainwater: Laboratory and field experiments GC-MS/MS rainwater Environ. Pollut. 139 #1, 133-142 (2006) Mirabel, Philippe; Sauret-Szczepanski, Nathalie; Wortham, Henri Analysis of trace levels of pesticides in rainwater using SPME and 2223 Pesticides in GC tandem mass spectrometry PDMS GC-MS-MS rainwater Anal. Bioanal. Chem. 384, #2, 475-487 (2006) Millet, Maurice; Mirabel, Philippe; Morville, Stephane; Scheyer, Anne Analysis of trace levels of pesticides in rainwater by SPME and 2467 Pesticides in GC-tandem mass spectrometry after derivatisation with PFBBr. 65µm PDMS-DVB GC-MS rainwater Anal Bioanal Chem 387, #1, 359-68 (2007 Jan) headspace Scheyer, A.; Briand, O.; Morville, S.; Mirabel, P.; Millet, M. PFBBr derivative 60 min at 68°C Interactions of chlorpyrifos with colloidal materials 2080 Chlorpyrifos in aqueous systems GC from water J of Environmental Quality, 33., #5, 1765-1770 Wu, Jigang; Laird, David A. SPME-GC-(tandem) MS as a tool for pesticide residue 2081 Pesticides in analysis in water samples at high sensitivity and 65µm PDMS-DVB GC-MS-MS water selectivity w/ confirmation capabilities immersed fiber J Chromatogr A, 1026, #1-2, 239-250 Goncalves, C.; Alpendurada, M. F. Transport and fate of dieldrin in poplar and willow 2082 Dieldrin in trees analyzed by SPME headspace GC trees Chemosphere, 61, #1,, 85-91 Anderson, Larry G.; Ramaswami, Anu; Skaates, S. Pesticide residue analysis in waters by SPME 2083 Pesticides coupled to GC-tandem mass spectrometry. 100µm PDMS GC-MS-MS in water Analytical Letters, 37, 1, 99-117 65µm PDMS-DVB Arrebola, F. ; Cortes Aguado, S.; Sanchez-Morito, N.; Garrido Frenich, A.; Martinez Vidal, J. Determination of pesticides and some metabolites in 2084 Pesticides different kinds of milk by SPME and low-pressure GC-MS-MS headspace/ immersed GC-MS-MS in milk Anal. Bioanal. Chem., 381, #1, 164-172 acidified sample Frenich, A. Garrido; Gonzalez-Rodriguez, M.J.; Liebanas, F. J. Arrebola; Lopez, F. J. Sanchez; Vidal, J. L. Martinez Evaluation of SPME conditions for the determination of chlorophenols 2741 Chlorophenol in honey samples using gas chromatography 100µm PDMS GC-AED in honey J Chromatogr A, 1125, #1, 31-37 (2006-08-25) headspace Campillo, N.; Penalver, R.; Hernandez-Cordoba, M. 15 min @ 75°C acetylation Comparison of SPME and stir bar sorptive 2085 Organo- extraction for determining six organophosphorus 100µm PDMS LC-MS phosphorus insecticides in honey by LC-MS insecticides J Chromatogr A, 1030, #1-2, 77-85 Ambient temperature, unless otherwise indicated. 194
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument in honey Blasco, C.; Fernandez, M.; Pico, Y.; Font, G. Application of SPME for the determination of pyrethroid 2086 Pyrethroid residues in vegetable samples by GC-MS immersion sampling GC/MS In vegetables Anal. Bioanal. Chem., 376, #4, 502-511 Beltran, J.; Hernandez, F.; Lopez, F.J.; Peruga, A.; Pitarch, E. Water quality and presence of pesticides in a 2087 Pesticides in tropical coastal wetland in southern Mexico immersion sampling GC water Mar. Pollut. Bull., 48, #11-12, 1130-1141 Bello-Mendoza, R; Hernandez-Romero, A.; Malo, E.; Tovilla-Hernandez, C 2348 p,p'-DDT Spatial and temporal variations and possible sources of (DDT) and a its metabolites in rivers in Tianjin, Chin GC in water Chemosphere 68, #1,10-6 (May-2007) Tao, S; Li, B G; He, X C; Liu, W X; Shi, Z Determination of dichlorodiphenyltrichloroethane in 2088 p,p'-DDT water using automated SPME-GC-ECD 100µm PDMS GC-ECD in water Fenxi Huaxue, 32, #4, 500-502 immersion sampling Luan, T. G.; Lan, C. Y.; Zhou, H. L.; Wong, M. H. Evaluation of an SPME and GC-MS method for 2089 Fluazifop analysis of fluazifop in water. 100µm PDMS GC-MS in water Acta Chromatographica, 14, #1, 231-236 stirring Olszewska, E. Cost analysis of ELISA, solid-phase extraction, and 2090 Pesticides SPME for the monitoring of pesticides in water comparison of cost GC in water Environmental Research, 98, #1, 143-150 Dalvie, M.; Sinanovic, E.; London, L; Cairncross, E; Solomon, A.; Adam, H. Advanced method using microwaves and SPME 2091 Prethroid coupled w/GC-MS for the determination of pyrethroid 100µm PDMS GC-MS residue on residues in strawberries 30min immersed strawberries J. Chromatogr. A, 1046, #1-2, 35-40 water/acetornitrile Guillet, Valerie; Montury, Michel; Sanusi, Astrid preextraction Analysis of pesticide residues in juice and beverages "review" 2092 Pesticides in Crit. Rev. Anal. Chem., 34, #2, 121-131 Review article GC-MS beverages Albero, B; Gonzalez, L; Sanchez-Brunete, C; Tadeo, J. Combining SPME and on-line preconcentration-capillary 2093 Pesticides electrophoresis sensitive analysis of pesticides in foods CE-UV in water Electrophoresis, 26, #4-5, 980-989 Hernandez-Borges, J.; Cifuentes, A.; Garcia-Montelongo, F.; Rodriguez-Delgado, M. Highly sensitive analysis of multiple pesticides in foods 2094 Pesticides in combining SPME, capillary electrophoresis-MS & chemometrics NH 2HCO 3 buffer CE-MS food Electrophoresis, 25, #13, 2065-2076 pH 4 CE-UV Hernandez-Borges, Javier; Rodriguez-Delgado, M.; Garcia-Montelongo, Francisco J.; Cifuentes,A. Application of SPME to the study of the photochemical 2095 Pesticides behaviour of five priority pesticides: "On-fiber" 100µm PDMS GC-MS in water and aqueous photodegradation 30min extract J. Chromatogr. A, 1047, #2, 271-279 immersion sampling Sanchez-Prado, Lucia; Llompart, Maria; Lores, Marta; Garcia-Jares, Carmen; Cela, Rafael Applicability of headspaceSPME to the determination 2096 Pesticides in of multi-class pesticides in waters. 30µm polyacrylate GC-MS water J Chromatogr A, 1028, #1, 63-74 30° to 100°C Sakamoto, Mitsushi; Tsutsumi, Taizou headspace Soil Application of SPME and GC with Electron-Capture and Mass 36 HexachlorocyclohexaneMass Spectrometric Detection for the Determination of 100µm PDMS GC-ECD, in soil Hexachlorocyclohexanes in Soil Solutions 20-30 min GC-MS J. Chromatogr. 687: 133-140 (1994) immersion Ambient temperature, unless otherwise indicated. 195
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