(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber / Analyte / Extraction Matrix Literature Reference Analysis of nitroaromatic compounds in complex samples using <strong>SPME</strong> Conditions Instrument 2640 Nitroaromatics and isotope dilution quantification GC-electron negative ionisation MS GC-MS in water J. Chromatogr. A 1164, #1-2, 65-73 (Sep 14 2007) van Bavel, B.; Gustavsson, L.; Jonsson, S 49 Nitroaromatics Enrichment of Nitroaromatic Compounds from Water Samples by <strong>SPME</strong> in water GIT Spex Chromatogr. 14: 85-87 (1995) Schaefer, B., Engewald, W. 809 Nitroarenes Analysis of nitroarenes by <strong>SPME</strong>/GC-Ion trap MS Chromatography (2000) 21(2),123-124 Kataoka, Hiroyuki; Lord, Heather L.; Pawliszyn, Janusz GC-MS 160 Hetero aromatics Trace Analysis of Hetero Aromatic Compounds in Water by <strong>SPME</strong> 85µm polyacrylate GC-MS in water J. High Res. Chromatogr. 19(11): 627-632 (1996) 60-200 min Johansen, S., Pawliszyn, J. stirring pH 8, salt added 218 BTEX Determination of Benzene Derivatives in Water by <strong>SPME</strong> Anal. Chim. Acta 343: 101-108 (1997) in water Huang, S., Cheng, C., Sung, Y. Enrichment of Nitrophenols from Water by Means of <strong>SPME</strong> 50 Nitrophenols Fresenius’ J. Anal. Chem. 352(5): 535-6 (1995) 100µm PDMS GC-NPD in water Schafer, B., Engewald, W. 5 min stirring pH
(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Nilsson, T., Ogaard-Madison, J., Montanrilla, L., Larsen, B., headspace Facchetti, S., Pelusioj, F. stirring 685 MTBE Determination of MTBE in surface water by use of <strong>SPME</strong> Environ, Sci.Technol. (2000), 34(7), 1359-1364 Carboxen/DVB/PDMS GC-MS in surface water Achten, C., Puettmann, W. Sensitive methods for measuring methyl tert-butyl-ether 69 min 25% NaCl, stirred 935 MTBE in water Carboxen/DVB/PDMS GC-MS in surface water Umwelt-Technol. Aktuell (2000) 12(1), 22-25 69 min Achten, C., Puettmann, W. 25% NaCl, stirred 686 MTBE, Ethanol, other Trace Analysis of Ethanol, MTBE, and related Oxygenate Compounds in Water using <strong>SPME</strong> and GC-MS Carboxen/DVB/PDMS GC-MS oxygenates in water Anal. Chem. 2000, 72, 4654-4658 25 min immersed Cassada, D., Zhang, Y., Snow, D., Spalding, R. stirred Sat. salt, 910 MTBE, TBE, BTEX High levels of monoaromatic compounds limit the use of <strong>SPME</strong> of MTBE and Tert butyl alcohol 75µm Carboxen/PDMS Ion trap in water Environ Sci Technol, 2001, 35 (15) 3190-3192 65µm DVB/PDMS GC-MS Black, L., Fine, D. Analysis of Water Samples for Trace Levels of Oxygenated 1-25min. saturated salt 354 MTBE, EBE, BTEX and Aromatic Compounds Using Headspace <strong>SPME</strong> and 75µm Carboxen/PDMS GC-FID in water Comprehensive Two-Dimensional Gas Chromatography 40°C, 10 min J. Microcolumn Separations, 10 (7), 597-604 (1998) headspace Gaines, R., Ledford, E., Stuart, J. saturated salt 952 MTBE Measurement of Henry's law constant for MTBE using <strong>SPME</strong> Environ. Toxicol. Chem (2001), 20(8), 1625-1629 in water Bierwagen, B.G.; Keller, A.A. Role of humic acids in the titanium oxide-photocatalysed 15°-40°C headspace 581 Tetrachloroethene degradation of tetrachloroethene in water. 100µm PDMS GC-MS in water Water-Res. Jun 1999; 33(8): 1827-1836 Selli,-E; Baglio,-D; Montanarella,-L; Bidoglio,-G Using <strong>SPME</strong> with GC to assess trihalomethane content in water 2331 Trihalomethanes Abstracts of Papers Am Chem Society (2004) 227 Part1, U456 GC in water Rizzuti, Anthony M.; Rogers, Lisa N. 2829 Volatiles in Simultaneous analysis of 23 priority volatile compounds in water by <strong>SPME</strong>-GC-MS and estimation of the method's uncertainty 75µm Carboxen GC-MS in drinking water Int. J. Environ. Anal. Chem. 88, #3, 151-164 (March 2008) headspace Alpendurada, M.; Carvalho, J.; Goncalves, C.; Guimaraes, A. 15min @ 20°C Determination of trihalomethanes in drinking water of towns in 2215 Trihalomethane the State of Minas Gerais, Brazil using headspace (HS)/<strong>SPME</strong> headspace GC-ECD in drinking water high resolution GC-ECD Ciencia Eng.) 11 #2, 57-62 (2002) Duarte, M.; Parreira, F; Rabelo De Carvalho, C. 175 Trihalomethanes Detection and Quantification of Trihalomethanes in Drinking Water from Alexandria, Egypt in water Contam. Toxicol. 56: 397-404 (1996) Hassan, A., Benfenati, E., Fanelli, R. Analysis of dichlorobenzene in water by <strong>SPME</strong> 687 Dichlorobenzene J. Chin. Chem. Soc (2000) 47(2) 415-420 100um PDMS GC-ECD in water Liu, Y., Ho, W. 30 min 813 Chloroform Analysis of chloroform in drinking water by headspace solid-phase microextraction and GC 85µm Polyacrylate GC-FID in water Fenxi Shiyanshi (2000), 19(5), 65-67 45°C Liu, Z. L.; Wang, C. H.; Wang, X headspace Ambient temperature, unless otherwise indicated. 149