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SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />

Analyte / Extraction<br />

Matrix Literature Reference Conditions Instrument<br />

1122 Chlorophenols in water Chromatographia (2002) 55(9-10), 595-600<br />

Bianchi, F.; Careri, M.; Mucchino, C.; Musci, M.<br />

65um DVB/PDMS,<br />

pentafluorobenzoyl<br />

chloride derivatization<br />

GC-ECD<br />

MultiSimplex optimization of the solid-phase microextraction-gas<br />

chromatography-mass spectrometric determination of polycyclic aromatic<br />

hydrocarbons, polychlorinated biphenyls and phthalates from water samples.<br />

PAH, PCB and<br />

1151 phthalates in water. Journal of Chromatography, A (2002) 978 (1-2), 165-175.<br />

Cortazar, E.; Zuloaga, O. *; Sanz, J.; Raposo, J. C.; Etxebarria, N.; Fernandez,<br />

L. A.<br />

PDMS GC-MS<br />

1153 Endosulfan in water.<br />

Optimization of solid-phase extraction and solid-phase microextraction for the<br />

determination of small alpha - and small beta -endosulfan in water by gas<br />

chromatography-electron-capture detection.<br />

Journal of Chromatography, A (2002) 976 (1-2), 293-299.<br />

Lopez-Blanco, M. C.; Reboreda-Rodriguez, B.; Cancho-Grande, B.; Simal-<br />

Gandara, J. *<br />

GC-ECD<br />

1154 PAH's in water<br />

Application of the novel benzo-15-crown-5 sol-gel coating for solid-phase<br />

microextraction in rapid determination of trace PAHs in water at non-equilibrium<br />

situations.<br />

Fenxi Kexue Xuebao (2003) 19 (2), 109-112.<br />

Wang, D. H.; Xing, J.; Wu, C. Y.*<br />

GC<br />

Application of time-resolved luminescence methodology to the determination of<br />

phthalate esters.<br />

1155 Phthalate esters Analytical Letters (2003) 36 (5), 1017-1027.<br />

Casas-Hernandez, A. M.; Aguilar-Caballos, M. P.; Gomez-Hens, A. *<br />

2549 Butyltin in<br />

Headspace <strong>SPME</strong>-GC-ion trap tandem mass spectrometry method for<br />

butyltin analysis in sediments: Optimization and validation headspace GC-MS<br />

sediments Microchemical Journal 87, #2, 147-153 (DEC 2007)<br />

Carvalho, P.; Pinto, L.; Basto, A..; Vasconcelos, A..<br />

1164 Butyltin<br />

<strong>SPME</strong>-GCMS for speciation of butyltin compounds in marine environment<br />

Journal De Physique. IV : JP (2003) 107 (II), 1313-1316.<br />

Mahapatra, S.; Puranik, V.D.; Sadasivan, S.; Tripathi, R.M.<br />

PDMS GC-MS<br />

Fibre introduction mass spectrometry: fully direct coupling of solid-phase<br />

microextraction with mass spectrometry.<br />

VOC, SVOC in<br />

1071 aqueous solutions. Analytical Chemistry (2002) 74 (21), 5688-5692.<br />

Meurer, E. C.; Tomazela, D. M.; Silva, R. C.; Augusto, F.; Eberlin, M. N.*<br />

PDMS FIMS<br />

Extractions with superheated water.<br />

1072 Journal of Chromatography, A (2002) 975 (1), 31-46.<br />

Smith, R. M.<br />

1112 Organotin<br />

Rapid determination of organotin compounds by headspace solid-phase<br />

microextraction<br />

Journal of Chromatography A (2003) 999 (1-2), 123-134.<br />

Le Gac, Marjorie; Lespes, Gaetane; Potin-Gautier, Martine<br />

GC<br />

Determination of siloxane-water partition coefficients by capillary extraction-highresolution<br />

gas chromatography. Study of aromatic solvents.<br />

1228 BTEX Journal of Chromatography, A (2003) 985 (1-2), 39-45.<br />

Nardi, L.<br />

1167 Glycol ethers<br />

Optimization of the headspace solid-phase microextraction for determination of<br />

glycol ethers by orthogonal array designs.<br />

Journal of Chromatography, A (2002) 977(1), 11-15<br />

Huang, C. T.; Su, Y. Y.; Hsieh, Y. Z.<br />

75µm Carboxen PDMS GC-FID<br />

Simultaneous determination of oestrogenic short ethoxy chain nonylphenols<br />

and their acidic metabolites in water by an in-sample derivatization/solid-phase<br />

microextraction method.<br />

Ambient temperature, unless otherwise indicated. 165

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