SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Effect of thickeners and sweeteners on the release 1625 Aroma of blended aroma compounds in fat-free stirred headspace GC compounds yoghurt during shear conditions in yoghurt Intl Dairy Journal, 14, #9, 783-789 Decourcelle, N.; Lubbers, S.; Vallet, N.; Rondeau, P.; Guichard, E. Optimization of SPME for the analysis of volatile 1626 Volaitles from compounds in milk. headspace GC milk Journal of Dairy Science, 86, Supplement 1, 294 Clarkson, H.; Duncan, S.; O'Keefe, S. Volatile compounds and chemical changes in 1627 Volaitles from ultrapasteurized milk packaged in polyethylene headspace @ 5°C GC-MS milk terephthalate containers J of Food Science, 70. #6, C407-C412 Solano-Lopez, C.; Ji, T.; Alvarez, V. Quality control of raw cows' milk by headspace analysis 2808 Volaitles from Int. Dairy J. 18, #5, 506-513 (May 2008) headspace GC raw cow milk van Hooijdonk, A.C.M.; van Valenberg, H.J.F.; Hettinga, K.A. Development of a headspace SPME method combined 1628 Phthalate w/ GC-MS for the determination of phthalate esters 60min @ 90°C. GC-MS esters in in cow milk headspace cow milk Analytica Chimica Acta, 538, #1-2, 41-48 NaCl added Feng, Yong-Lai; Zhu, Jiping; Sensenstein, R. Analytical methods applied to the determination of heterocyclic 2814 Aromatic aromatic amines in foods Review article amines J Chromatogr B, 862, #1-2, 15-42 (FEB 1 2008) in food Sanz Alaejos, M.; Ayala, J. H.; Gonzalez, V.; Afonso, A. M. SPME coupled with HPLC for the analysis 1629 Aromatic of heterocyclic aromatic amines. 50µm CW-TPR LC-diode array amines J Chromatogr A, 1030, #1-2, 87-93 methanolic NaOH in food Cardenes, L.; Ayala, J.; Afonso, A.; Gonzalez, V. SPME-GC-MS analysis of horseradish (Armoracia rusticana) 1630 Isothiocynates Italian J Food Sci, 16, #4,487-490 GC-MS in horseradish D'Auria, M.; Mauriello, G.; Racioppi, R. Aroma profiles of five basil (Ocimum basilicum L.) cultivars grown 2451 Volatiles from under conventional and organic conditions headspace GC-ITMS basil cultivars FOOD CHEM. 107, #1, 464-472 (01 MAR 2008) GC-TOFMS Klimankova, E.; Holadova, K.; Hajslova, J.; Cajka, T.; Poustka, J.; Koudela, M. Volatile compounds in different cultivars of Apium 1631 Volatiles from graveolens L. headspace GC-MS cultivars Italian J Food Sci, 16, #4, 477-482 Tirillini, B.; Pellegrino, R.; Pagiotti, R.; Pocceschi, N.; Menghini, L. Tequila volatile characterization and ethyl ester determination 1632 Volatiles in by SPME-GC-MS analysis 100µm PDMS GC-MS tequila J Agri and Food Chem, 52, #18, 5567-5571 60min @ 40°C Vallejo-Cordoba, B.; Gonzalez-Cordova, A.; . immersed del Carmen Estrada-Montoya, M. Rapid determination of volatile compounds in grapes by 1633 Volatile aroma HS-SPME coupled with GC-MS 65µm DVB-PDMS GC compounds Talanta, 66, #5, 1152-1157 20 min @ 70°C in grapes Sanchez-Palomo, E.; Diaz-Maroto, A. ; Perez-Coello, A. headspace Stable isotope dilution analysis of wine fermentation products 1634 Fermentation by HS-SPME-GC headspace GC-MS products of Anal. Bioanal. Chem., 381, #4, 937-947 salt addition wines Capone, D.; Herderich, M.; Neuwohner, C.; Pardon, K.; Pollnitz, A.; Sefton, M; Skouroumounis, G.; Smyth, H.; Siebert, T. 1635 Monoter- Comparison of ultrasound-assisted extraction and direct immersion SPME method for the analysis of monoterpenoids immersion GC-MS penoids in in wine Ambient temperature, unless otherwise indicated. 54
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument wine Talanta, 67, #1, 129-135 Barciela, J.; Garcia-Martin, S.; Herrero, C.; Pena, R. 2873 Volatiles from Impact odorants of Chardonnay dry white wine from Changli County European Food Res and Tech 227, #1, 287-292 (May 2008) headspace GC/MS white wine Li, Hua; Tao, Yong-Sheng; Wang, Hua; Zhang, Li Dynamic changes in ester formation during chardonnay juice 2282 Ester compd in fermentations with different yeast inoculation and initial headspace GC-MS Chardonnay brix conditions juice. American J Enology and Viticulture 55 #3, 346-354 (2004) Lee, Seung-Joo; Rathbone, Da.; Asimont, S.; Adden, R.; Ebeler, S. Analytical method for determination of some 1636 Volatiles in aroma compounds on white wines by SPME-GC 50/30µm DVB/CAR GC white wine J of Food Sci, 68, #9, 2817-2820 Headspace Ferreira, A.; Guedes de Pinho, P. Analysis of methoxypyrazines in wine using 1637 Methoxy- headspace SPME with isotope dilution and Headspace GC-GC-NPD pyrazine comprehensive two dimensional GC GC-GC-TOFMS in wine J. Sep. Sci., 28, #9-10, 1075-1082 Allen, M.; Marriott, P.; Ryan, D.; Smith, J.; Watkins, P. GC profile of volatiles in cheese induced by 1638 Volatiles in different fat globule surface coatings. headspace GC cheese J of Dairy Science, 86, Supplement 1, 43 Everett, D. ; Crownshaw, J.; Ginestet, A.; Leus, M.; Dufour, J.. Flavor stability of skim and whole milk powder 1639 Flavors in J of Dairy Science, 86, Supplement 1, 40 GC milk products Whetstine, M.; Drake, M..; Karagul-Yuceer, Y.; Avsar, Y. GC-MS with SPME method for determination of 1640 Methyl methyl salicylate and other volatile compounds in 100µm PDMS GC-MS salicylate in leaves of Lycopersicon esculentum. Headspace tomato leaves Anal. Bioanal. Chem., 378, #2, 518-522 Deng, C; Zhang, X; Zhu, W; Qian, J SPME for flavor analysis in Harari Khat 1641 Flavors in (Catha edulis) stimulant. 100µm PDMS GC-MS Harari Khat J. Zhejiang Univ: Sci, 5, #4, 428-431 30min @ 20°C stimulant Abdulsalam, Al-Flahi; Yin, Xue-Feng; Zou, Jian-Kai Interactions between volatile and nonvolatile coffee 1642 Nonvolatiles components. Screening of nonvolatile components headspace GC from brewed J Agr Food Chem., 53, #11, 4417-4425 coffee Charles-Bernard, M.; Kraehenbuehl, K.; Rytz, A.; Roberts, D. Impact of "ecological" post-harvest processing on the volatile fraction 2649 Volatiles in of coffee beans: I. Green coffee headspace GC-MS coffee beans J. Food Compos. Anal. (UK) 20, #3-4, 289-96 (May 2007) Schorr-Galindo, S.; Gonzalez-Rios, O.; Suarez-Quiroz, M. L.; Boulanger, R.; Barel, M.; Guyot, B.; Guiraud, J.-P. Quality determination and group discrimination of shade grown 2517 Volatiles in coffee using solid phase microextraction headspace GC-FID coffee beans 21st International Conference on Coffee Science, Montpellier, France, 11-15 September, 2006 PP 306-309 Jackson, M.; Steiman, S.; Gautz, L.; Bittenbender, H.; Idol, T. Comprehensive multidimensional GC for the 1643 Volatiles in characterization of roasted coffee beans headspace GC-GC coffee beans J. Sep. Sci., 27, #5-6, 442-450 Casilli, A., Costa, R.; Dugo, G., Dugo, P.; Festa, S.; Mondello, L.; Tranchida, P. Analysis of roasted coffee bean volatiles by using 1644 Volatiles in comprehensive two-dimensional GC-TOF-MS headspace GC-GC-TOF-MS coffee beans J. Chromatogr. A, 1054, #1-2, 57-65 Casilli, A.; Marriott, P.; Mondello, L.; Ryan, D.; Shellie, R.; Tranchida, P. Ambient temperature, unless otherwise indicated. 55
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