SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
SPME Applications Guide - Overbrook Scientific
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(New references added to the 7th edition are in bold) <strong>SPME</strong> Fiber /<br />
Analyte / Extraction<br />
Matrix Literature Reference Conditions Instrument<br />
hormones in J. Chromatogr. A, 1104, #1-2, 23-32 (2006) immersion<br />
biological Lan, Chongyu; Luan, Tiangang; Yang, Lihua derivatization<br />
samples<br />
113 Estrogen, steroids in<br />
Analysis of Steroids from Human Serum by <strong>SPME</strong> with<br />
Headspace Derivatization & GC 85µm polyacrylate GC-MS<br />
water/biological fluids J. High Res. Chromatogr. 20: 171-173 (1997) 30 min<br />
Okeyo, P., Rentz, S., Snow, N.<br />
Analysis of Estrogens and Anabolic Steroids by <strong>SPME</strong> with<br />
immersion, stirring<br />
BSTFA derivative<br />
373 Estrogen, steroids in On-Fiber Derivatization and GC-MS 85µm polyacrylate GC-MS<br />
water/biological fluids J. Microcolumn Separations, 10(7) 551-556 (1998) 30 min<br />
Okeyo, P., Snow, N.<br />
On-Fiber Derivatization for Analysis of Steroids by <strong>SPME</strong>-GC-MS<br />
immersion, stirring<br />
BSTFA derivative<br />
404 Estrogen, steroids in Book chapter 60µm Carbowax/DVB GC-MS<br />
water/biological fluids Snow, N. 60°C, 30 min<br />
immersion<br />
stirring<br />
BSTFA derivative<br />
200 Ethanol, acetone,<br />
Solid Phase Microextraction for the Analysis of Human Breath<br />
Anal. Chem. 69 (4): 587-596 (1997) 100µm PDMS GC-MS<br />
isoprene in Grote, C., Pawliszyn, J. 10-60 sec<br />
human breath<br />
Determination of isoprene in human expired breath using<br />
headspace<br />
659 Isoprene <strong>SPME</strong> with GC-MS Carboxen/PDMS GC-MS<br />
in human breath J. Chromatogr, B. Biomed Appl. 739(1), 183-190 10 min @ 40°C from<br />
Hyspler, R, Crhova, S. Gasparic, J., Cizkova, M.,<br />
Balasova, V., Zadak, Z.<br />
tedlar bag sample<br />
322 Chloroethenes<br />
Determination of Chloroethenes in Environmental Biological<br />
Samples Using GC Coupled with <strong>SPME</strong><br />
in biological fluids Chromatographia 42 (5/6): 313-317 (1996)<br />
Xu, N., Vadegrifts, S., Sewell<br />
660 Halothane<br />
Rapid analysis of halothane in biological samples<br />
using headspace <strong>SPME</strong> and GC-MS - GC-MS<br />
in biological samples a case of double homicide<br />
J. Anal. Toxicol. (2000), 24(5), 372-376<br />
Musshoff, G., Junker, H., Madea, B.<br />
867 4-Heptanone<br />
Urine 4-heptanone: A beta-oxidation product of<br />
2-ethylhexanoic acid from plasticisers GC-MS<br />
in urine Clinica Chimica Acta (2001) 306(1-2) 51-61<br />
Walker, Valerie; Mills, Graham A<br />
491 Clozapine in<br />
<strong>SPME</strong> for the assay of clozapine in human plasma<br />
Fresenius' J. Anal. Chem, 1999, 364(7), 654-655 100µm PDMS<br />
human plasma Kruggel, S., Ulrich, S.<br />
<strong>SPME</strong> for the assay of levomepromazine in human plasma<br />
30 min<br />
pH adj. NaOH<br />
843 Levomepromazine Therapeutic Drug Monitoring (2000) 22(6), 723-728 100µm PDMS GC-NPD<br />
in human plasma Kruggel, S., Ulrich, S.<br />
Determination of homocysteine and its related compounds<br />
30 min @30°c<br />
chloramitriptyline added<br />
0. 1 M -NaOH<br />
575 Homocysteine in by <strong>SPME</strong>-gas chromatography-mass spectrometry. 85µm polyacrylate GC-MS<br />
plasma/water J-Chromatogr,-B:-Biomed-Appl. 30 Apr 1999; 727(1-2): 1-8 30 min immersed<br />
Myung,-S-W; Kim,-M-S; Min,-H-K; Yoo,-E-A; Kim,-K-R pH 3<br />
906 Ranitidine<br />
Automated in-tube <strong>SPME</strong>-LC-electrospray ionization mass<br />
spectrometry for the determination of ranitidine.<br />
J. Chromatogr.B (1999), 731(2), 353-359<br />
Kataoka, H., Lord, H., Pawliszyn, J.<br />
LC-MS<br />
Ambient temperature, unless otherwise indicated. 121
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