SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
1356 Volatiles in wines
Classification of Nebbiolo-based wines from Piedmont (Italy) by means of solidphase
microextraction-gas chromatography-mass spectrometry of volatile
compounds.
Journal of Chromatography A (2002) 943(1), 123-137
Aceto, Maurizio; Marengo, Emilio; Maurino, Valter
GC-MS
Determination of cyclopiazonic acid in cheese samples using solid-phase
microextraction with high performance liquid chromatography.
Cyclopiazonic acid in
1362 cheese. Food Chemistry (2001) 75(2), 249-254.
Zambonin, C. G.; Monaci, L.; Aresta, A. *
Carbowax/TPR HPLC
2-Methyl-3-furanthiol and methional are possible off-flavours in stored orange
juice: aroma-similarity, NIF/SNIF GC-Olfactometry, and GC analyses.
Off flavours in orange
1367 juice. Journal of Agricultural and Food Chemistry (2001) 49(11), 5425-5432.
Bezman, Y.; Rouseff, R. L.; Naim, M. *
GC-O
Headspace solid phase microextraction ( SPME ) analysis of flavour compounds
in wines. Effect of the matrix volatile composition in the relative response factors
in a wine model.
Flavour compounds in
1368 wine. Journal of Agricultural and Food Chemistry (2001) 49(11), 5142-5151.
Rocha, S.; Ramalheira, V.; Barros, A.; Delgadillo, I.; Coimbra, M. A.
GC
New device for direct extraction of volatiles in solid samples using SPME
1370 Volatiles in solid foods. Journal of Agricultural and Food Chemistry (2001) 49(11), 5115-5121. GC-MS
Ruiz, J.; Ventanas, J.; Cava, R.
The use of an electronic aroma-sensing device to assess coffee differentiation.
Comparison with SPME gas chromatography-mass spectrometry aroma
patterns.
1372 Coffee aroma Journal of Food Composition and Analysis (2001) 14(5), 513-522. 100 um PDMS GC-MS
Costa Freitas, A. M.; Parreira, C.; Vilas-Boas, L.
1377 PAH in rice.
Dynamics analysis for the distribution of PAH in rice.
Journal of Health Science (2001) 47(5), 446-451.
Liu, X. X.; Korenaga, T.
GC-MS
1378 Fatty acids in milk.
Quantitative determination of short-chain free fatty acids in milk using solidphase
microextraction and gas chromatography.
Journal of Agricultural and Food Chemistry (2001) 49(10), 4603-4608.
Gonzalez-Cordova, A. F.; Vallejo-Cordoba, B. *
Polyacrylate GC
Comparison of simultaneous distillation extraction and solid-phase
microextraction for the determination of volatile flavour components.
Volatile flavour
1382 compounds. Journal of Chromatography, A (2001) 930(1-2), 1-7.
Cai, J. B.; Liu, B. Z.; Su, Q. D.*
GC-MS
Solid-phase microextraction ( SPME ) technique for measurement of generation
of fresh cucumber flavour compounds.
Cucumber flavour
1387 compounds Journal of Agricultural and Food Chemistry (2001) 49(9), 4203-4207.
Palma-Harris, C.; McFeeters, R. F.*; Fleming, H. P.
PDMS GC
Characterization of volatiles in different dry gins
2330 Volatile fraction of J Ag Food Chem 53, #26, 10154-10160 (2005) headspace GC/MS
distilled gins Vichi, S.; Riu-Aumatell, M.; Mora-Pons, M.; Buxaderas, S.;
Lopez-Tamames, Elvir
1389 Scotch whiskies
Headspace congeners of blended scotch whiskies of different product
categories from SPME analysis.
Journal of the Institute of Brewing (2001) 107(5), 315-332.
Lee, K. -Y. M.; Paterson, A. *; Birkmyre, L.; Piggott, J. R
PDMS, polyacrylate GC-FID
Ambient temperature, unless otherwise indicated. 39