SPME Applications Guide - Overbrook Scientific

(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
Determination of chromium(III) in water by SPME
1957 Chromium in w/ polyimide-coated fiber and GC-FPD polyimide fiber GC-FPD
Water J. Chromatogr. A, 1062, #1, 49-55 TFA derivatives
Ding, Tzuoo-Huei; Lin, Huang-Huei; Whang, Chen-Wen
SPME: A powerful sample preparation tool prior to
1958 Organics mass spectrometric analysis review article GC-MS, LC-MS
in water J. Mass Spectrom.(2004) 39(3), 233-254
Vas, Gyorgy; Vekey, Karoly
Comparison between headspace and aqueous phase SPME
1959 Butyltin in method for speciation analysis of butyltin compounds headspace & GC
sea water in sea water immersion sampling
J Food and Drug Analysis, 12, #3, 205-211
Hsia, Meng-Pei; Hsu, Tau-Being; Liu, Shiu-Mei
Multielemental speciation analysis of organometallic
1960 Hg,Pb,Tn compounds of mercury, lead, and tin in natural water Various fibers GC-MS
in water & samples by headspace-SPME followed by GC-MS NaEt 4B derivatives
seawater J. Chromatogr. A, 1034,#1-2, 191-197 headspace
Centineo, G; Gonzalez, E; Sanz-Medel, A
Reevaluation of headspace SPME-GC-MS for the
1961 MTBE in determination of methyl tert-butyl either in water samples headspace GC-MS
water J. Chromatogr. A, 1021, #1-2, 157-164
Fang, Fu; Hong, Chia-Swee; Chu, S; Kou, W; Bucciferro, A
Identification of 2,3-butanedione (diacetyl) as the
1962 Diacetyl Odor compound causing odor events at trace levels in the 75µm Carboxen GC-MS
in water Llobregat River and Barcelona's treated water (Spain 30min @ 60°C
J. Chromatogr. A, 1034, #1-2, 175-182 NaEt 4B derivative
Diaz, A.; Galceran, Ma. Teresa; Ventura, F. Headspace
Simultaneous determination of 22 volatile organic compounds,
1963 Odors/volatiles methyl-tert-butyl ether,1,4-dioxane, 2-methylisoborneol and 100µm PDMS GC-MS
in water geosmgeosmin in water by headspace SPME-GC-MS headspace
Anal. Chim. Acta, 548, #1-2, 79-85
Daishima, Shigeki; Nakamura, Sadao
Determination of musty odorants, 2-methylisoborneol and geosmin,
2807 Geosmin and in environmental water by headspace GC-MS 65µm PDMS-DVB GC-MS
2-methyisoborneol J. Chromatogr. A, 1186, #1-2, 434-437 (Apr 4 2008) Headspace
in water Kataoka, Hiroyuki; Okamura, Kota; Saito, Keita 70 °C for 30 min.
Study of alkyl lead speciation by Head Space (HS)-
1964 Alkyl lead SPME coupled with GC-MS Headspace GC-MS
in water Fenxi Shiyansh, 23, #2, 14-17
Shuai, Q.; Zheng, C; Shuai, Q.; Yang, W.; Zheng, Y.
Effects of riboflavin-photo sensitization on the formation of volatiles
2666 Volatiles from in linoleic acid model systems with sodium azide or D2O Headspace GC-MS
linoleic acid Food Chemistry 105, #4, 1375-1381 (2007)
Yang, Seungk; Lee, JaeMin; Lee, JaeChul; Lee, JaeHwan
Volatile fatty acids as malodorous compounds in
1965 C2-C7 Fatty wool scouring water and lanolin. Origin and headspace GC-CI-MS
acids in characterization.
water/lanolin Env Technology, 24, #12, 1465-1470
Jover, E.; Abalos, M.; Ortiz, L.; Bayona, J.
SPME of volatile oxidation compounds in oil-in-water
1966 Volatile emulsions headspace GC-FID.
oxidative Food Chemistry, 92, #3, 401-406 50°C for 20 min.
products in Beltran, G; Aguilera, M; Gordon, Michael H.
oil-water
Full automation of derivatization:SPME-GC-MS
1967 Organometallic with dual-arm system for the determination of phenyl derivative GC-MS
derivatives organometallic compounds in aqueous samples. headspace
in water J Chromatogr A, 1025, #1, 77-84
Parkinson, D; Bruheim, I; Christ, I; Pawliszyn, J
1968 Methyl
Determination of methylmercury and mercury(II) in a marine
ecosystem using SPME--GC-MS headspace GC-MS
mercury from Anal. Chim. Acta, 551, #1-2, 192-198 Na(C6H5) 4B
seawater Bhalke, S.; Mishra, S.; Puranik, V.D.; Shukla, V.K.; Tripathi, R.M. derivative
Ambient temperature, unless otherwise indicated. 172