SPME Applications Guide - Overbrook Scientific

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(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Determination of chromium(III) in water by SPME 1957 Chromium in w/ polyimide-coated fiber and GC-FPD polyimide fiber GC-FPD Water J. Chromatogr. A, 1062, #1, 49-55 TFA derivatives Ding, Tzuoo-Huei; Lin, Huang-Huei; Whang, Chen-Wen SPME: A powerful sample preparation tool prior to 1958 Organics mass spectrometric analysis review article GC-MS, LC-MS in water J. Mass Spectrom.(2004) 39(3), 233-254 Vas, Gyorgy; Vekey, Karoly Comparison between headspace and aqueous phase SPME 1959 Butyltin in method for speciation analysis of butyltin compounds headspace & GC sea water in sea water immersion sampling J Food and Drug Analysis, 12, #3, 205-211 Hsia, Meng-Pei; Hsu, Tau-Being; Liu, Shiu-Mei Multielemental speciation analysis of organometallic 1960 Hg,Pb,Tn compounds of mercury, lead, and tin in natural water Various fibers GC-MS in water & samples by headspace-SPME followed by GC-MS NaEt 4B derivatives seawater J. Chromatogr. A, 1034,#1-2, 191-197 headspace Centineo, G; Gonzalez, E; Sanz-Medel, A Reevaluation of headspace SPME-GC-MS for the 1961 MTBE in determination of methyl tert-butyl either in water samples headspace GC-MS water J. Chromatogr. A, 1021, #1-2, 157-164 Fang, Fu; Hong, Chia-Swee; Chu, S; Kou, W; Bucciferro, A Identification of 2,3-butanedione (diacetyl) as the 1962 Diacetyl Odor compound causing odor events at trace levels in the 75µm Carboxen GC-MS in water Llobregat River and Barcelona's treated water (Spain 30min @ 60°C J. Chromatogr. A, 1034, #1-2, 175-182 NaEt 4B derivative Diaz, A.; Galceran, Ma. Teresa; Ventura, F. Headspace Simultaneous determination of 22 volatile organic compounds, 1963 Odors/volatiles methyl-tert-butyl ether,1,4-dioxane, 2-methylisoborneol and 100µm PDMS GC-MS in water geosmgeosmin in water by headspace SPME-GC-MS headspace Anal. Chim. Acta, 548, #1-2, 79-85 Daishima, Shigeki; Nakamura, Sadao Determination of musty odorants, 2-methylisoborneol and geosmin, 2807 Geosmin and in environmental water by headspace GC-MS 65µm PDMS-DVB GC-MS 2-methyisoborneol J. Chromatogr. A, 1186, #1-2, 434-437 (Apr 4 2008) Headspace in water Kataoka, Hiroyuki; Okamura, Kota; Saito, Keita 70 °C for 30 min. Study of alkyl lead speciation by Head Space (HS)- 1964 Alkyl lead SPME coupled with GC-MS Headspace GC-MS in water Fenxi Shiyansh, 23, #2, 14-17 Shuai, Q.; Zheng, C; Shuai, Q.; Yang, W.; Zheng, Y. Effects of riboflavin-photo sensitization on the formation of volatiles 2666 Volatiles from in linoleic acid model systems with sodium azide or D2O Headspace GC-MS linoleic acid Food Chemistry 105, #4, 1375-1381 (2007) Yang, Seungk; Lee, JaeMin; Lee, JaeChul; Lee, JaeHwan Volatile fatty acids as malodorous compounds in 1965 C2-C7 Fatty wool scouring water and lanolin. Origin and headspace GC-CI-MS acids in characterization. water/lanolin Env Technology, 24, #12, 1465-1470 Jover, E.; Abalos, M.; Ortiz, L.; Bayona, J. SPME of volatile oxidation compounds in oil-in-water 1966 Volatile emulsions headspace GC-FID. oxidative Food Chemistry, 92, #3, 401-406 50°C for 20 min. products in Beltran, G; Aguilera, M; Gordon, Michael H. oil-water Full automation of derivatization:SPME-GC-MS 1967 Organometallic with dual-arm system for the determination of phenyl derivative GC-MS derivatives organometallic compounds in aqueous samples. headspace in water J Chromatogr A, 1025, #1, 77-84 Parkinson, D; Bruheim, I; Christ, I; Pawliszyn, J 1968 Methyl Determination of methylmercury and mercury(II) in a marine ecosystem using SPME--GC-MS headspace GC-MS mercury from Anal. Chim. Acta, 551, #1-2, 192-198 Na(C6H5) 4B seawater Bhalke, S.; Mishra, S.; Puranik, V.D.; Shukla, V.K.; Tripathi, R.M. derivative Ambient temperature, unless otherwise indicated. 172
(New references added to the 7th edition are in bold) SPME Fiber / Analyte / Extraction Matrix Literature Reference Conditions Instrument Speciation analysis of mercury by SPME and multicapillary 1969 Mercury GC hyphenated to ICP-TOF spectrometry. 75µm Carboxen ICP-TOF-MS from wate/ J Chromatogr A, 1055, #1-2, 197-207 NaEt 4B derivatives sediment Jitaru, P.; Adams, F. C.* headspace Diffusion-based calibration for SPMEof benzene, 1970 BTEX in toluene, ethylbenzene, p-xylene and chlorobenzenes headspace GC water from aqueous samples J Chromatogr A, 1025, #1, 11-16 Paschke, A.; Popp, P. Indirect determination of low vapour pressures using SPME - 1971 Chlorinated Application to tetrachlorobenzenes & trachlorbenyltoluenes minutes to hour GC benzenes J Chromatogr A, 1072, #1, 93-97 headspace Paschke, Albrecht; Schroter, Uwe; Schuurmann, Gerrit LC-MS-based procedures for monitoring of toxic organophosphorus 2890 Organo- compounds and verification of pesticide and nerve agent poisoning review article LC-MS phosphorus Anal. Bioanal. Chem. 391, #1, 97-116 (May 2008) compounds John, Harald; Thiermann, Horst; Worek, Franz Determination of organophosphorus pesticides in 1972 Organo- spiked river water samples using SPME-GC With immersed sampling GC-MS phosphorus EI-MS and ICP-MS detection GC-ICP-MS pesticides J Anal At Spectrom, 20, #9, 876-882 in water Blanco-Gonzalez, E; Fidalgo-Used, N; Montes-Bayon, M; Sanz-Medel, A SPME for the determination of pyrethroids in cucumber and watermelon 2404 Pyrethroids using HPLC combined with post-column photochemically induced HPLC-PIF-FD in cucumber fluorimetryderivatization and fluorescence detection 30 min @ 65°C and watermelon Anal. Chim. Acta 607, #1, 74-82 (21 JAN 2008) fluorimetry Vazquez, P. P.; Mughari, A. R.; Galera, M. M. derivatization Alternative sample preparation method for photochemical studies 2609 Pyrethroids based on SPME: Synthetic pyrethroid photochemistry headspace GC-MS photodegradation J. Chromatogr. A 1152, #1-2, 156-167 (Jun 8 2007) Cela, R.; Fernandez-Alvarez, M.; Garcia-Jares, C.; Llompart, M.; Lores, M.; Sanchez-Prado, L. The photochemical behaviour of five household pyrethroid insecticides 2591 Pyrethroids and a synergist as studied by photo-solid-phase microextraction headspace GC-MS photodegradation Anal. Bioanal. Chem. 388, #5-6, 1235-1247 (2007-07) 100µm PDMS Fernandez-Alvarez, M.; Lores, M. ; Llompart, M.; Garcia-Jares, C.; Cela, R Occurrence and bioavailability of pyrethroids in a mixed land 2625 Pyrethroids use watershed in sediment J. Environ. Qual. 36, #4, 1006-1012 (July/August 2007) Bondarenko, S.; Budd, R.; Gan, J.; Haver, D.; Kabashima, J. Analysis of pyrethroids in sediment pore water by SPME 2594 Pyrethroids Environ Toxicol Chem 26, #12, 2587-93 (2007 Dec) in sediment Bondarenko, Svetlana; Spurlock, Frank; Gan, Jianying Development of a SPME-GC with micro ECD detection method for 2865 Pyrethroids and a multiresidue analysis of pesticides in bovine milk 65µm PDMS-DVB GC-ECD organochlorinated Anal. Chim. Acta 617, #1-2, 37-50 (Jun 9 2008) 30min @ 100°C pesticides in Cela, Rafael; Dagnac, Thierry; Fernandez-Alvarez, Maria; stirred bovine milk Garcia-Jares, Carmen; Lamas, J.: Pablo; Llompart, Maria; Lores, M. Effects of sample pretreatment and storage conditions in the 2537 Pyrethroids etermination of pyrethroids in water samples by SPME-GC-MS headspace GC-MS in water Anal Bioanal Chem 387, #5, 1841-1849 (2007) 40°C Casas, V.; Llompart, M.; Garcia-Jares, C.; Cela, R.; Dagnac, T Determination of enantiomers of synthetic 1973 Pyrethroids pyrethroids in water by SPME GC in water enantioselective gas chromatography. J Agrl Food Chem, 52, #4, 736-741 Liu, W. P.; Gan, J. J.* Ultrasound-assisted emulsification-microextraction of emergent Ambient temperature, unless otherwise indicated. 173
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