SPME Applications Guide - Overbrook Scientific

1530
(New references added to the 7th edition are in bold) SPME Fiber /
Analyte / Extraction
Matrix Literature Reference Conditions Instrument
Residual solvents in
cocaine
Forensics
Gas chromatographic-mass spectrometric analysis of residual solvent trapped
into illicit cocaine exhibits using head-space solid-phase microextraction
Journal of Chromatography B (2002) 772(2), 249-256 headspace GC-MS
Chiarotti, Marcello; Marsili, Remo; Moreda-Pineiro, Antonio
748 Review
The use of SPME-GC in forensic analysis
J. Chromatogr. Sci. (2000), 38(7), 297-306
Furton, K., Wang, J., Hsu, Y. Walton, J, Almirall, J.
500 Gasoline
The detection and analysis of ignitable liquid residues
extracted from human skin using SPME-GC 100µm PDMS GC-FID
on skin Almirall, J., Wang, J., Lothridge, K, Furton, K.
Characterization of SPME-GC for the analysis of gasoline tracers
15 min
headspace
2733 Gasoline volatiles in different microenvironments. 75µm Carboxen GC-FPD
in varied matries J Air Waste Manag Assoc 57, #3, 355-65 (2007 Mar) 10min
Ceballos, Diana; Zielinska, Barbara; Fujita, Eric; Sagebiel, John air samples
SPME samping of fire debris resideus in the presence of
2385 Fire debris radionuclide surrogate metals headspace GC-MS
from surrogate Journal of Chromatography A 2007-03-23 22°C
metals Duff, M., Crump, S., Keisha M.
2630 Ignitable liquids
Forensic application of GC-differential mobility spectrometry with
two-way classification of ignitable liquids from fire debris headspace GC-MS
in fire debris Anal. Chem. 79, #17, 6752-6759 (Sep 1 2007)
Harrington, Peter B.; Lu, Yao
85 Accelerants
A Simple, Inexpensive, Rapid, Sensitive and Solventless
Technique for the Analysis of Accelerants in Fire 100µm PDMS GC-FID
in fire debris Debris Based on SPME 40°C, 20 min
J. High Res. Chromatogr. 18: 625-629 (1995)
Furton, K., Bruna, J., Almirall, J.
headspace
105 Gasoline, kerosene
Forensic Application of the SPME Method to the Analysis
of Gasoline and Kerosene 100µm PDMS GC-NPD
in fire debris Kaneko, T., Nakada, M. 22°C for 1 hr, or
80°C for 5 min
headspace
Multivariate pattern recognition of petroleum-based accelerants by
2430 Accelerants SPME-GC with flame ionization detection. headspace GC-FID
Identification Anal. Chim. Acta 589, #2, 247-254 (2007-04-25)
Bodle, E. S.; Hardy, J. K.
114 Accelerants
Novel Method for Analysis of Gasoline from Fire Debris Using
Headspace Solid Phase Microextraction 100µm PDMS GC-FID
in fire debris J. Forensic Sci. 41: 12-22 (1996)
Furton, K., Almirall, J., Bruna, J.
40°C, 20 min
The Recovery of Accelerants in Aqueous Samples from Fire
115 Accelerants Debris Using SPME 100µm PDMS GC-FID
in liquid residue Science & Justice 36 (4): 283-287 (1996) 20 min @ 40°C
Almirall, J., Furton, K., Bruna, J.
143 Accelerants
Determination of Liquid Accelerants in Arson Suspected Fire
Debris Using Headspace SPME 100µm PDMS GC-FID
in fire debris Anal. Commun. 33: 129 (1996)
Steffen, A., Pawliszyn, J.
A comprehensive sample preparation scheme for a
15 min @ 70°C
headspace
594 Accelerants accelerants in suspect arson cases. GC, GC-MS
in fire debris J-Forensic-Sci. May 1999; 44(3): 504-515
Ren,-QL; Bertsch,-W
Immersion mode SPME ECD/GC and TEEM-GC/MS for analysis of
Ambient temperature, unless otherwise indicated. 128